CN206300830U - Can light irradiation, the heater of controlled atmosphere - Google Patents
Can light irradiation, the heater of controlled atmosphere Download PDFInfo
- Publication number
- CN206300830U CN206300830U CN201621358547.XU CN201621358547U CN206300830U CN 206300830 U CN206300830 U CN 206300830U CN 201621358547 U CN201621358547 U CN 201621358547U CN 206300830 U CN206300830 U CN 206300830U
- Authority
- CN
- China
- Prior art keywords
- bell jar
- transparent bell
- base
- heating plate
- transparent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
The utility model provide it is a kind of can light irradiation, the heater of controlled atmosphere.Its structure includes base and the heating plate being arranged on the base and transparent bell jar, and the transparent bell jar is the open hollow cavity structure in lower end, and the transparent bell jar buckle closure is on the base so that the inner chamber of transparent bell jar is closing space；The heating plate is located in the inner chamber of the transparent bell jar, is used to place sample to be heated in the heating plate；Through-thickness is provided with inflation inlet and vacuum interface with the transparent bell jar intracavity inter-connection on the base；The inner chamber of the transparent bell jar can be vacuumized by vacuum interface to required atmosphere is passed through in the inner chamber of the transparent bell jar by inflation inlet；External light source can carry out light irradiation by transparent bell jar to the sample to be heated in heating plate.The utility model simple structure, simple operation is light harvesting irradiation, atmosphere is controllable, calorify the device of one, is very suitable for heating and/or the light irradiation experiment of organic film.
Description
Technical field
The utility model is related to technical field of film preparation, specifically it is a kind of can light irradiation, the heating of controlled atmosphere
Device.
Background technology
The organic film prepared using chemical method needs heated baking in most cases, the solvent remained on film is volatilized
Or make film crystallization.But organic film suffers from the influence of dioxygen oxidation or moisture attack, should not directly in an atmosphere
It is heated.Currently, a kind of device for being called glove box is widely used, and it is a kind of closed container for being filled with inert gas,
Size is larger, is easy to built-in function.But, can not be vacuumized in glove box, light irradiation experiment can not be carried out, while hand
Casing is nor the firing equipment of specialty.
Utility model content
The purpose of this utility model be just to provide it is a kind of can light irradiation, the heater of controlled atmosphere, it is existing to solve
Glove box and non-professional firing equipment, and do not possess vacuumize and light irradiation experiment problem.
What the purpose of this utility model was realized in：It is a kind of can light irradiation, the heater of controlled atmosphere, including base
And heating plate and transparent bell jar on the base are arranged on, the transparent bell jar is the open hollow cavity structure in lower end, institute
Transparent bell jar buckle closure is stated on the base so that the inner chamber of the transparent bell jar is closing space；The heating plate is located at institute
State in the inner chamber of transparent bell jar, be used to place sample to be heated in the heating plate；Through-thickness is provided with the base
With the inflation inlet and vacuum interface of the transparent bell jar intracavity inter-connection；Can be in the transparent bell jar by the inflation inlet
Required atmosphere is passed through in chamber, the inner chamber of the transparent bell jar can be vacuumized by the vacuum interface；External light source can
Light irradiation is carried out to the sample to be heated in heating plate by transparent bell jar.
The open position being in contact with the base in the lower end of the transparent bell jar is provided with sealing ring.
Through-thickness is provided with the pressure tap with the transparent bell jar intracavity inter-connection on the base, by the survey
Pressure mouth can be measured to the pressure of the transparent bell jar inner chamber.
Control outside the binding post that the heating plate is connected on the base by wire and wearing and the transparent bell jar
Power electric connection processed.
The supporting plate for being supported to the heating plate is provided with the base, the supporting plate adds with described
Support column is provided between hot plate；Temperature probe, the temperature probe are provided between the heating plate and the supporting plate
By wire and wear the binding post being connected on the base and electrically connected with the thermometer outside the transparent bell jar.
The utility model makes the inner chamber of transparent bell jar form a sky for closing by setting transparent bell jar on base
Between, heating plate is placed on base and in transparent bell jar inner chamber, and sample to be heated is placed on hot plate, by heating
Plate can be heated to sample to be heated；The inflation inlet and vacuum interface with transparent bell jar intracavity inter-connection are opened up on base,
Can be to being passed through required atmosphere in transparent bell jar by inflation inlet（Such as inert gas）, can be to transparent bell jar by vacuum interface
Inner chamber is vacuumized, it is of course also possible to so that inflation and vacuumize while carry out, so, you can the transparent bell jar inner chamber of guarantee
In sample to be heated heated under required atmospheric condition, be particularly suited for easily being influenceed not by dioxygen oxidation or moisture attack
Suitable organic film heated in an atmosphere.And, external light source can be by transparent bell jar to the sample to be heated in heating plate
Carry out light irradiation experiment.
It is provided by the utility model can light irradiation, the heater of controlled atmosphere, it is possible to achieve in vacuum or various gas
To the heating of sample under atmosphere, light irradiation experiment can also be realized under vacuum or controlled atmosphere, and light irradiation can be with
Carried out simultaneously with heating, i.e., illumination and heating are carried out simultaneously to sample under different atmosphere or vacuum condition, this is right
The carrying out of the techniques such as photocatalysis, vacuum heat, atmosphere heat treatment and related experiment is with great effect.
The utility model simple structure, simple operation is light harvesting irradiation, atmosphere is controllable, calorify the device of one, very
It is suitable to the heating of organic film and/or light irradiation experiment.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
In figure：1st, base, 2, transparent bell jar, 3, heating plate, 4, supporting plate, 5, sealing ring, 6, pressure tap, 7, inflation inlet,
8th, vacuum interface, 9, support feet, 10, binding post.
Specific embodiment
As shown in figure 1, it is provided by the utility model can light irradiation, the heater of controlled atmosphere, its structure specifically wraps
Include base 1, transparent bell jar 2 and heating plate 3.
Base 1 is circular flat plate structure in the present embodiment, and three support feets 9 are uniformly arranged below with base 1.Heating
Plate 3 is placed on the base 1, is used to place sample to be heated, such as organic film in heating plate 3（Certainly, substrate is contained）.
The lower section of heating plate 3 is provided with the supporting plate 4 for being supported to heating plate, heating plate 3 and supporting plate 4 are relative up and down
Circular flat plate structure.It is connected by support column between supporting plate 4 and base 1, it is same logical between heating plate 3 and supporting plate 4
Support column is crossed to be connected.Heating plate 3 is generally the heat-conducting plate of metal, and supporting plate 4 can be plastic plate.
Transparent bell jar 2 is suprasil bell jar in the present embodiment, and transparent bell jar 2 is the open hollow cavity structure in lower end,
Specifically, can be the cylindrical hollow cavity shown in Fig. 1, it is of course also possible to be rectangular structure etc..Transparent bell jar 2 is buckled
Cover on base 1, and transparent bell jar 2 covers the heating plate 3 on base 1.The transparent clock that base 1 and transparent bell jar 2 are surrounded
The space of closing is formd in the inner chamber of cover 2.The position being in contact with base 1 in the lower end opening of transparent bell jar 2 is provided with close
Seal 5, can well be sealed by sealing ring 5 to the inner chamber of transparent bell jar 2.
Through-thickness is provided with and is connect with the pressure tap 6 of the intracavity inter-connection of transparent bell jar 2, inflation inlet 7 and vacuum on base 1
Mouth 8.By the pressure of the measurable inner chamber of transparent bell jar 2 of pressure tap 6, can be to being passed through in the inner chamber of transparent bell jar 2 by inflation inlet 7
Required gas（For example it is passed through nitrogen）, the inner chamber of transparent bell jar 2 can be vacuumized by vacuum interface 8.It is of course also possible to
While being passed through required gas to the inner chamber of transparent bell jar 2, while being vacuumized to the inner chamber of transparent bell jar 2, transparent bell jar 2 is finally caused
The atmosphere of inner chamber meets atmospheric condition required when sample heating or light irradiation.Inflation inlet 7 can also act as the effect of gas vent,
I.e.：By inflation inlet 7 also the gas of the inner chamber of transparent bell jar 2 can discharge.
Because transparent bell jar 2 is the cavity of all-transparent, therefore, the external light source outside transparent bell jar 2 can be by saturating
Bright bell jar 2 carries out light irradiation to the sample to be heated in heating plate 3.
Through-thickness is worn and is connected to three binding posts 10 on base 1, and the upper end of each binding post 10 extend into
In the inner chamber of bright bell jar 2（Not shown in figure）, each lower end of binding post 10 is reached the lower section of base 1, is connect by three
Terminal 10, may be such that the wire inside transparent bell jar 2 is realized being connected with the wire outside transparent bell jar 2.
One of binding post, for realizing the control power electric connection outside heating plate 3 and transparent bell jar 2, by control
Whether is the work of the controllable heating plate 3 of power supply processed.
Temperature probe can be set between heating plate 3 and supporting plate 4, and make temperature probe pass through wire and wear to be connected on bottom
A binding post on seat 1 is electrically connected with the thermometer outside transparent bell jar 2, so as to realize to the internal temperature of transparent bell jar 2
Measurement.
If it is intended to being contrasted to the result after sample light predose, can be used in test sample characteristic（Such as I-V is special
Property）Probe is by wire and wears another binding post being connected on base 1 and connects with the tester outside transparent bell jar 2.
Claims (5)
1. it is a kind of can light irradiation, the heater of controlled atmosphere, it is characterized in that, including base and be arranged on the base plus
Hot plate and transparent bell jar, the transparent bell jar are the open hollow cavity structure in lower end, and the transparent bell jar buckle closure is at the bottom
On seat so that the inner chamber of the transparent bell jar is closing space；The heating plate is located in the inner chamber of the transparent bell jar, described
It is used to place sample to be heated in heating plate；Through-thickness is provided with and the transparent bell jar intracavity inter-connection on the base
Inflation inlet and vacuum interface；Can be to required atmosphere be passed through in the inner chamber of the transparent bell jar, by institute by the inflation inlet
Stating vacuum interface can vacuumize to the inner chamber of the transparent bell jar；External light source can be by transparent bell jar in heating plate
Sample to be heated carries out light irradiation.
2. it is according to claim 1 can light irradiation, the heater of controlled atmosphere, it is characterized in that, in the transparent bell jar
The open position being in contact with the base in lower end be provided with sealing ring.
3. it is according to claim 1 can light irradiation, the heater of controlled atmosphere, it is characterized in that, the edge on the base
Thickness direction is provided with the pressure tap with the transparent bell jar intracavity inter-connection, can be in the transparent bell jar by the pressure tap
The pressure in chamber is measured.
4. it is according to claim 1 can light irradiation, the heater of controlled atmosphere, it is characterized in that, the heating plate passes through
Control power electric connection outside the binding post that wire and wearing is connected on the base and the transparent bell jar.
5. it is according to claim 1 can light irradiation, the heater of controlled atmosphere, it is characterized in that, set on the base
The supporting plate for being supported to the heating plate is equipped with, support column is provided between the supporting plate and the heating plate；
It is provided with temperature probe between the heating plate and the supporting plate, the temperature probe is connected on described by wire and wearing
Binding post on base is electrically connected with the thermometer outside the transparent bell jar.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621358547.XU CN206300830U (en) | 2016-12-12 | 2016-12-12 | Can light irradiation, the heater of controlled atmosphere |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621358547.XU CN206300830U (en) | 2016-12-12 | 2016-12-12 | Can light irradiation, the heater of controlled atmosphere |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206300830U true CN206300830U (en) | 2017-07-04 |
Family
ID=59213562
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621358547.XU Expired - Fee Related CN206300830U (en) | 2016-12-12 | 2016-12-12 | Can light irradiation, the heater of controlled atmosphere |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206300830U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111208163A (en) * | 2018-11-21 | 2020-05-29 | 中国科学院化学研究所 | Inflatable/air-pumping type XPS (extruded polystyrene) freezing-quasi-in-situ sample transfer device |
-
2016
- 2016-12-12 CN CN201621358547.XU patent/CN206300830U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111208163A (en) * | 2018-11-21 | 2020-05-29 | 中国科学院化学研究所 | Inflatable/air-pumping type XPS (extruded polystyrene) freezing-quasi-in-situ sample transfer device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170704 Termination date: 20191212 |