CN206292220U - A kind of sample cell for gas absorption instrument - Google Patents

A kind of sample cell for gas absorption instrument Download PDF

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Publication number
CN206292220U
CN206292220U CN201621342173.2U CN201621342173U CN206292220U CN 206292220 U CN206292220 U CN 206292220U CN 201621342173 U CN201621342173 U CN 201621342173U CN 206292220 U CN206292220 U CN 206292220U
Authority
CN
China
Prior art keywords
tube
sample cell
interior caliber
gas absorption
caliber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn - After Issue
Application number
CN201621342173.2U
Other languages
Chinese (zh)
Inventor
李正操
李明阳
姜辛灏
康世栋
赵书芬
李红
曹建主
房超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tsinghua University
Original Assignee
Tsinghua University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tsinghua University filed Critical Tsinghua University
Priority to CN201621342173.2U priority Critical patent/CN206292220U/en
Application granted granted Critical
Publication of CN206292220U publication Critical patent/CN206292220U/en
Withdrawn - After Issue legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model belongs to measuring for materials field, more particularly to a kind of sample cell for gas absorption instrument.The sample cell includes a U-tube and a connecting tube, and the U-tube is divided into setting-out side, bottom and connecting side, and the connecting tube is connected by nut with U-tube setting-out side, and sealing gasket and sleeve pipe have been compressed between the connecting tube and nut and U-tube.The interior caliber of U-tube setting-out side is more than bottom and the interior caliber of connecting side.Sample cell air-tightness of the present utility model is good, and can place large-sized sample.

Description

A kind of sample cell for gas absorption instrument
Technical field
The utility model belongs to measuring for materials field, more particularly to a kind of sample cell for gas absorption instrument.
Background technology
Current people place sample more than carry out when gas absorption is tested using caliber U-tube equal everywhere, due to Caliber with adsorption instrument Interface Matching, therefore need to cannot place larger sample.And in order to adsorption instrument Interface Matching, only increase U-shaped The caliber in a part of region in pipe setting-out side simultaneously sets injection port at the position, then the heating of adsorption experiment is in due to the position , there is poor air-tightness in area.
Utility model content
The purpose of this utility model is to provide a kind of sample cell for gas absorption instrument, i.e., one kind is carrying out gas absorption Ensure that sample is contacted with experimental gas and ensures the device for placing sample of air-tightness during experiment, concrete technical scheme is as follows:
A kind of sample cell for gas absorption instrument, including a U-tube and a connecting tube, the U-tube is divided into be put Sample side, bottom and connecting side, the connecting tube are connected by nut with U-tube setting-out side, the connecting tube and nut and U-tube Between compressed sealing gasket and sleeve pipe.
Wherein, the interior caliber of U-tube setting-out side is more than bottom and the interior caliber of connecting side.
Connecting tube is divided into two sections by outer tube diameter, and thick outer tube diameter section and thin outer tube diameter section are followed successively by from lower to upper;Connecting tube is pressed Interior caliber is divided into three sections, and caliber section in thick, interior caliber converging transition and thin interior caliber section are followed successively by from lower to upper.Connecting tube it is thick in The interior caliber of caliber section is identical with the outer tube diameter of sleeve pipe, more than the outer tube diameter of U-tube setting-out side;In thick interior caliber section and interior caliber The intersection of converging transition, interior caliber is identical with the interior caliber of U-tube setting-out side by the outer tube diameter identical mutation with sleeve pipe;Up It is interior caliber converging transition, interior caliber is tapered to the outer tube diameter less than U-tube connecting side and no longer changes;It is up thin interior caliber Section.The outer tube diameter of the thin outer tube diameter section of connecting tube is identical with the outer tube diameter of U-tube connecting side, so as to guarantee to insert adsorption instrument Interface.
Connecting tube has screw thread on the outside of the one end being connected with U-tube, is constituted between nut and is threadedly coupled.
The material of connecting tube, sleeve pipe and nut is metal, and the material of U-tube is quartz glass, and gasket material is selected Rubber.
The application of sample cell as described above:Sample is loaded into U-tube by setting-out side, using nut by connecting tube and U Shape pipe links together, tightening nuts so that sleeve pipe compress sealing gasket, so as to ensure air-tightness;Connecting tube upper end, U-tube are connected Connect side upper end to be connected with gas absorption instrument respectively, you can carry out related experiment.
In the utility model, air-tightness ensure that by sleeve pipe and sealing gasket;Simultaneously because connecting tube is located at the upper of U-tube End, connection member can individually carry out cooling treatment away from heating zone during heating, reduce the temperature of junction, preferably protect Air-tightness is demonstrate,proved.
The utility model U-tube both sides caliber is different, and setting-out side uses big caliber, so as to meet placement compared with large sample Demand;Bottom and connecting side use small caliber, match corresponding gas absorption instrument, and reduce the volume of non-sample section.
The beneficial effects of the utility model are:Sample cell air-tightness is good, and can place large-sized sample.
Brief description of the drawings
Fig. 1 is sample cell described in the utility model longitudinal sectional drawing when in use;
Fig. 2 is the partial enlarged drawing of sample cell described in the utility model;
Wherein, 1- connecting tubes, 2- sealing gaskets, 3- sleeve pipes, 4- nuts, 5-U shape pipes.
Specific embodiment
The utility model is described further with specific embodiment below in conjunction with the accompanying drawings, but does not therefore limit this The protection domain of utility model.
Embodiment 1
A kind of sample cell for gas absorption instrument as depicted in figs. 1 and 2, including a U-tube 5 and a connecting tube 1,5 points of the U-tube is setting-out side, bottom and connecting side, and the connecting tube 1 is connected by nut 4 with the setting-out side of U-tube 5, institute State and sealing gasket 2 and sleeve pipe 3 have been compressed between connecting tube 1 and nut 4 and U-tube 5.
Wherein, the interior caliber of the setting-out side of U-tube 5 is more than bottom and the interior caliber of connecting side.
Connecting tube 1 is divided into two sections by outer tube diameter, and thick outer tube diameter section and thin outer tube diameter section are followed successively by from lower to upper;Connecting tube 1 It is divided into three sections by interior caliber, caliber section in thick, interior caliber converging transition and thin interior caliber section is followed successively by from lower to upper.Connecting tube 1 The interior caliber of caliber section is identical with the outer tube diameter of sleeve pipe 3 in thick, more than the outer tube diameter of the setting-out side of U-tube 5;In thick caliber section with The intersection of interior caliber converging transition, interior caliber is by interior caliber that the outer tube diameter identical mutation with sleeve pipe 3 is with the setting-out side of U-tube 5 It is identical;It is up interior caliber converging transition, interior caliber is tapered to the outer tube diameter less than the connecting side of U-tube 5 and no longer changes;It is up Caliber section in thin.The outer tube diameter of the thin outer tube diameter section of connecting tube 1 is identical with the outer tube diameter of the connecting side of U-tube 5, so as to guarantee Insert the interface of adsorption instrument.
Connecting tube 1 has screw thread on the outside of the one end being connected with U-tube 5, is constituted between nut 4 and is threadedly coupled.
The material of connecting tube 1, sleeve pipe 3 and nut 4 is metal, and the material of U-tube 5 is quartz glass, the material of sealing gasket 2 From rubber.
Sample is loaded into U-tube 5 by setting-out side, connecting tube 1 is linked together with U-tube 5 using nut 4, tightened Nut 4 so that sleeve pipe 3 compress sealing gasket 2, so as to ensure air-tightness;By the upper end of connecting tube 1, the connecting side upper end of U-tube 5 respectively with Gas absorption instrument is connected, you can carry out related experiment.

Claims (9)

1. a kind of sample cell for gas absorption instrument, it is characterised in that including a U-tube (5) and a connecting tube (1), The U-tube (5) is divided into setting-out side, bottom and connecting side, and the connecting tube (1) is by nut (4) and U-tube (5) setting-out side Connection, has compressed sealing gasket (2) and sleeve pipe (3) between the connecting tube (1) and nut (4) and U-tube (5).
2. a kind of sample cell for gas absorption instrument according to claim 1, it is characterised in that U-tube setting-out side Interior caliber is more than bottom and the interior caliber of connecting side.
3. a kind of sample cell for gas absorption instrument according to claim 1, it is characterised in that the connecting tube is by outer Caliber is divided into two sections, and thick outer tube diameter section and thin outer tube diameter section are followed successively by from lower to upper;Connecting tube is divided into three sections by interior caliber, under Up it is followed successively by caliber section in thick, interior caliber converging transition and thin interior caliber section.
4. a kind of sample cell for gas absorption instrument according to claim 3, it is characterised in that the connecting tube it is thick The interior caliber of interior caliber section is identical with the outer tube diameter of sleeve pipe, more than the outer tube diameter of U-tube setting-out side;In thick interior caliber section and inner tube The intersection of footpath converging transition, interior caliber is identical with the interior caliber of U-tube setting-out side by the outer tube diameter identical mutation with sleeve pipe;It is past Upper is interior caliber converging transition, and interior caliber is tapered to the outer tube diameter less than U-tube connecting side and no longer changes, and is up thin interior caliber Section.
5. a kind of sample cell for gas absorption instrument according to claim 3, it is characterised in that the connecting tube it is thin The outer tube diameter of outer tube diameter section is identical with the outer tube diameter of U-tube connecting side.
6. a kind of sample cell for gas absorption instrument according to claim 1, it is characterised in that the connecting tube and U There is screw thread on the outside of one end of shape pipe connection, constituted between nut and be threadedly coupled.
7. a kind of sample cell for gas absorption instrument according to claim 1, it is characterised in that the connecting tube, set The material of pipe and nut is metal.
8. a kind of sample cell for gas absorption instrument according to claim 1, it is characterised in that the material of the U-tube Matter is quartz glass.
9. a kind of sample cell for gas absorption instrument according to claim 1, it is characterised in that the gasket material From rubber.
CN201621342173.2U 2016-12-08 2016-12-08 A kind of sample cell for gas absorption instrument Withdrawn - After Issue CN206292220U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621342173.2U CN206292220U (en) 2016-12-08 2016-12-08 A kind of sample cell for gas absorption instrument

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621342173.2U CN206292220U (en) 2016-12-08 2016-12-08 A kind of sample cell for gas absorption instrument

Publications (1)

Publication Number Publication Date
CN206292220U true CN206292220U (en) 2017-06-30

Family

ID=59097630

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621342173.2U Withdrawn - After Issue CN206292220U (en) 2016-12-08 2016-12-08 A kind of sample cell for gas absorption instrument

Country Status (1)

Country Link
CN (1) CN206292220U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106526089A (en) * 2016-12-08 2017-03-22 清华大学 Sample tube for gas adsorption instrument
CN110471011A (en) * 2019-09-06 2019-11-19 江苏师范大学 A kind of resonance sample sets tubulature of novel nuclear magnetic and its assemble method

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106526089A (en) * 2016-12-08 2017-03-22 清华大学 Sample tube for gas adsorption instrument
CN106526089B (en) * 2016-12-08 2019-02-22 清华大学 A kind of sample cell for gas absorption instrument
CN110471011A (en) * 2019-09-06 2019-11-19 江苏师范大学 A kind of resonance sample sets tubulature of novel nuclear magnetic and its assemble method

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GR01 Patent grant
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AV01 Patent right actively abandoned

Granted publication date: 20170630

Effective date of abandoning: 20190222

AV01 Patent right actively abandoned