CN206281829U - A kind of experimental optical catalytic reactor - Google Patents

A kind of experimental optical catalytic reactor Download PDF

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Publication number
CN206281829U
CN206281829U CN201621375849.8U CN201621375849U CN206281829U CN 206281829 U CN206281829 U CN 206281829U CN 201621375849 U CN201621375849 U CN 201621375849U CN 206281829 U CN206281829 U CN 206281829U
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CN
China
Prior art keywords
cover plate
catalytic reactor
tube
camera bellows
experimental optical
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621375849.8U
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Chinese (zh)
Inventor
王克强
赵文霞
杨朝旭
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Hebei University of Science and Technology
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Hebei University of Science and Technology
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Priority to CN201621375849.8U priority Critical patent/CN206281829U/en
Application granted granted Critical
Publication of CN206281829U publication Critical patent/CN206281829U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model is related to a kind of experimental optical catalytic reactor, and it includes camera bellows, the cover plate that is arranged on camera bellows two ends, the reaction tubes being fixedly connected with the cover plate successively from the inside to the outside, outer reaction tube and the light supply apparatus being connected is rotated with the cover plate;The reaction tubes and outer reaction tube are coaxially disposed with camera bellows;The light supply apparatus includes being arranged on the cover plate and the fluorescent tube of the change and change described in connection two being connected is rotated with cover plate, and the fluorescent tube be arranged in parallel with outer reaction tube.The utility model can meet photochemical catalyst under different temperatures, damp condition carry out that gas phase is static and dynamic experiment, liquid phase are static and dynamic experiment the need for.

Description

A kind of experimental optical catalytic reactor
Technical field
The utility model is related to light-catalyzed reaction technical field of experiment equipment, and in particular to a kind of experimental optical catalysis is anti- Answer device.
Background technology
In recent years, photocatalysis technology is continued to develop, because it has the advantages that nontoxic, non-secondary pollution, therefore, photocatalysis is controlled Dirt is increasingly taken seriously, and has broad application prospects.Photo catalysis reactor is an indispensable part in process of scientific research. In process of scientific research, often to photochemical catalyst in dynamic or static state to gas, liquid in the catalytic performance of pollutant study, In order to be fully understood by catalyst performance, in addition it is also necessary to change the catalytic conditions such as light intensity, humidity, temperature, and simple reactor can not Meet the performance test under varying environment, certain difficulty is caused to scientific research.
Utility model content
The purpose of this utility model is to provide photochemical catalyst under one kind can complete different temperatures, damp condition and carries out gas phase Static and dynamic experiment the experimental optical catalytic reactor of static and dynamic experiment, liquid phase.
The utility model is adopted the following technical scheme that:
A kind of experimental optical catalytic reactor, it includes camera bellows, the cover plate that is arranged on camera bellows two ends, from the inside to the outside successively with Reaction tubes that the cover plate is fixedly connected, outer reaction tube and the light supply apparatus being connected is rotated with the cover plate;It is described interior anti- The outer reaction tubes of Ying Guanhe are coaxially disposed with camera bellows;The light supply apparatus includes being arranged on the cover plate and being rotated with cover plate connecting The change for connecing and the fluorescent tube of change described in connection two, the fluorescent tube be arranged in parallel with outer reaction tube.
Further, the inside bottom of the outer reaction tube is provided with pedestal, heater is provided with the pedestal, is added Wet device and aerator.
Further, Temperature Humidity Sensor is provided with the outer reaction tube, control is provided with the lateral wall of the camera bellows Device processed, the controller is connected with Temperature Humidity Sensor, heater, humidification device and aerator.
Further, the ventilation unit connected with camera bellows inside is provided with the cover plate.
Further, the sample port connected with outer reaction tube inside is provided with the cover plate, is set on the sample port There is closure to fill in.
Further, the change is rotated with cover plate by bearing and is connected.
Further, lamp socket is provided with the change, the fluorescent tube is fixedly connected by lamp socket with change.
Further, the fluorescent tube is uniformly arranged in change.
Further, it is provided with case lid on the upper end side wall of the camera bellows.
Further, the fluorescent tube is ultraviolet lamp tube, visible fluorescent tube or simulated solar light lamp tube.
The beneficial effects of the utility model are:It is static quiet with dynamic experiment, liquid phase that the utility model can investigate gas phase The performance of photochemical catalyst in state and dynamic experiment, can by Temperature Humidity Sensor monitor react when temperature and humidity and pass through Temperature and humidity when heater and humidification device regulation reaction, difference is met by adjusting lamp strip position, replacing fluorescent tube The requirement of illumination composition and lighting angle.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Wherein, 1 camera bellows, 2 cover plates, 3 reaction tubes, 4 outer reaction tubes, 5 changes, 6 fluorescent tubes, 7 pedestals, 8 heaters, 9 add Wet device, 10 aerators, 11 ventilation units, 12 sample ports, 13 closure plugs, 14 lamp sockets, 15 case lids, 16 Temperature Humidity Sensors, 17 controllers, 18 handles.
Specific embodiment
With reference to shown in Fig. 1, a kind of experimental optical catalytic reactor, it includes camera bellows 1, is arranged on the cover plate at the two ends of camera bellows 1 2nd, the reaction tubes 3 that are fixedly connected with the cover plate 2 successively from the inside to the outside, outer reaction tube 4 and being rotated with the cover plate 2 is connected Light supply apparatus;The reaction tubes 3 and outer reaction tube 4 are coaxially disposed with camera bellows 1;The light supply apparatus includes being arranged on institute The fluorescent tube 6 stated on cover plate 2 and rotate the change 5 being connected with cover plate 2 and connect change 5 described in two, the fluorescent tube 6 and outer reaction Pipe 4 be arranged in parallel.Camera bellows 1 is made up of light-proof material, and inwall smears reflectorized material, and outer reaction tube 4 and reaction tubes 3 are quartz Pipe, reaction tubes 3 have different model, detachable and can be in two ends connection external pipe.
The inside bottom of the outer reaction tube 4 is provided with pedestal 7, and heater 8, humidification dress are provided with the pedestal 7 Put 9 and aerator 10.The heater 8 is preferably heating plate.The preferred ultrasonic humidifier of humidification device 9.Aerator 10 preferred cycle blower fans.
Temperature Humidity Sensor 16 is provided with the outer reaction tube 4, controller is provided with the lateral wall of the camera bellows 1 17, the controller 17 is connected with Temperature Humidity Sensor 16, heater 8, humidification device 9 and aerator 10.The control Device 17 can be with PLC or single-chip microcomputer, its signal that can receive Temperature Humidity Sensor 16, control heater 8, humidification device 9 and exposure The work of device of air 10, completes the control of the temperature and humidity environment in external reaction pipe.
The ventilation unit 11 connected with the inside of camera bellows 1 is provided with the cover plate 2.Ventilation unit 11 includes some air drafts Fan.The heat that ventilating fan can produce fluorescent tube in camera bellows discharges camera bellows, it is ensured that the temperature of outer reaction tube is unaffected.
The sample port 12 connected with the inside of outer reaction tube 4 is provided with the cover plate 2, envelope is provided with the sample port 12 Block 13.
The change 5 is rotated with cover plate 2 by bearing and is connected.Bearing can be rolling bearing or turntable bearing.It is described Lamp socket 14 is provided with change 5, the fluorescent tube 6 is fixedly connected by lamp socket 14 with change 5.
The fluorescent tube 6 is uniformly arranged in change 5.The fluorescent tube is several, and preferably 6, fluorescent tube is uniformly distributed outside Reaction tube periphery, lamp tube ends are separately mounted in change, and ventilating fan is arranged on the cover plate on the inside of change, are set with fluorescent tube interval Put.
Case lid 15 is provided with the upper end side wall of the camera bellows 1.The fluorescent tube 6 is ultraviolet lamp tube, visible fluorescent tube or simulation Sun-light lamp-tube.The conveniently replaced suitable light source of case lid 15 is opened, change outer end is provided with handle 18, is rotated using handle 18 Change 5 meets the requirement to illumination composition and lighting angle in testing to adjust light source position.
When static light Catalysis experiments are done, reaction tubes are removed, catalyst is put into outer reaction tube, controller passes through Temperature Humidity Sensor signal controls humidification device and heater and makes up to adjusting humiture to require numerical value.During catalyzed gas Directly gaseous sample can be injected or liquid sample is expelled on heater with syringe and be allowed to rapid volatilization, catalytic fluid When the closure plug of sample port can be removed, then sample is poured into outer reaction tube, disturbed by aerator, make catalyst and sample Product mix.Finally open light source and start experiment.Sample port closure plug can be pierced through in experiment with syringe to be taken from outer reaction tube Sample.
When dynamic optical Catalysis experiments are done, the reaction tubes of different model are selected according to requirement of experiment, urged to filling in pipe Agent, two mouthfuls of the left and right of reaction tubes is connected with exterior line.When testing, by pending sample from one end of reaction tubes Into by the catalysis of photochemical catalyst in reaction tubes again from other end discharge.Sample before and after catalysis can be existed with syringe Exterior line is gathered.
Above example is only used to illustrate the technical solution of the utility model, rather than its limitations;Although with reference to foregoing reality Example is applied to be described in detail the utility model, it will be understood by those within the art that:It still can be to preceding State the technical scheme described in embodiment to modify, or equivalent is carried out to which part technical characteristic;And these are repaiied Change or replace, do not make the spirit and scope of essence disengaging the utility model embodiment technical scheme of appropriate technical solution.

Claims (10)

1. a kind of experimental optical catalytic reactor, it is characterised in that it includes camera bellows(1), be arranged on camera bellows(1)The cover plate at two ends (2), from the inside to the outside successively with the cover plate(2)The reaction tubes being fixedly connected(3), outer reaction tube(4)And with the cover plate (2)Rotate the light supply apparatus of connection;The reaction tubes(3)With outer reaction tube(4)And camera bellows(1)It is coaxially disposed;The light Source device includes being arranged on the cover plate(2)Upper and and cover plate(2)Rotate the change of connection(5)And change described in connection two (5)Fluorescent tube(6), the fluorescent tube(6)With outer reaction tube(4)It is arranged in parallel.
2. a kind of experimental optical catalytic reactor according to claim 1, it is characterised in that the outer reaction tube(4)'s Inside bottom is provided with pedestal(7), the pedestal(7)On be provided with heater(8), humidification device(9)And aerator (10).
3. a kind of experimental optical catalytic reactor according to claim 2, it is characterised in that the outer reaction tube(4)It is interior It is provided with Temperature Humidity Sensor(16), the camera bellows(1)Lateral wall on be provided with controller(17), the controller(17)With Temperature Humidity Sensor(16), heater(8), humidification device(9)And aerator(10)Connection.
4. a kind of experimental optical catalytic reactor according to claim 3, it is characterised in that the cover plate(2)Upper setting Have and camera bellows(1)The ventilation unit of inside connection(11).
5. a kind of experimental optical catalytic reactor according to claim 4, it is characterised in that the cover plate(2)Upper setting Have and outer reaction tube(4)The sample port of inside connection(12), the sample port(12)On be provided with closure plug(13).
6. a kind of experimental optical catalytic reactor according to claim 1, it is characterised in that the change(5)By axle Hold and cover plate(2)Rotate connection.
7. a kind of experimental optical catalytic reactor according to claim 1, it is characterised in that the change(5)Upper setting There is lamp socket(14), the fluorescent tube(6)By lamp socket(14)With change(5)It is fixedly connected.
8. a kind of experimental optical catalytic reactor according to claim 7, it is characterised in that the fluorescent tube(6)Uniform peace Mounted in change(5)On.
9. a kind of experimental optical catalytic reactor according to claim 1, it is characterised in that the camera bellows(1)Upper end Case lid is provided with the wall of side(15).
10. a kind of experimental optical catalytic reactor according to any one of claim 1 ~ 9, it is characterised in that the fluorescent tube (6)It is ultraviolet lamp tube, visible fluorescent tube or simulated solar light lamp tube.
CN201621375849.8U 2016-12-15 2016-12-15 A kind of experimental optical catalytic reactor Expired - Fee Related CN206281829U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621375849.8U CN206281829U (en) 2016-12-15 2016-12-15 A kind of experimental optical catalytic reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621375849.8U CN206281829U (en) 2016-12-15 2016-12-15 A kind of experimental optical catalytic reactor

Publications (1)

Publication Number Publication Date
CN206281829U true CN206281829U (en) 2017-06-27

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CN201621375849.8U Expired - Fee Related CN206281829U (en) 2016-12-15 2016-12-15 A kind of experimental optical catalytic reactor

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109316959A (en) * 2018-11-14 2019-02-12 上海电力学院 A kind of removing gas mercury photocatalytic reaction device
CN109444322A (en) * 2018-08-31 2019-03-08 浙江工业大学 The device of photocatalytic degradation pernicious gas efficiency under a kind of Observable difference light source

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109444322A (en) * 2018-08-31 2019-03-08 浙江工业大学 The device of photocatalytic degradation pernicious gas efficiency under a kind of Observable difference light source
CN109316959A (en) * 2018-11-14 2019-02-12 上海电力学院 A kind of removing gas mercury photocatalytic reaction device

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170627

Termination date: 20181215