A kind of inorganic particle aqueous sample activation rate test device
Technical field
The utility model belongs to laboratory apparatus applied technical field, and in particular to a kind of inorganic particle aqueous sample activation rate
Test device.
Background technology
Pear shape separatory funnel is that current measurement surface is modified(Activation)The conventional tool of inorganic particle activation rate, its work is former
Reason is that surface is modified(Activation)Inorganic particle and water be sufficiently mixed concussion after stand, it is floating using modified lipophile powder
In the water surface(Or suspend in water), and it is unmodified(Activation)The principle of powder natural subsidence is distinguished modified with unmodified powder
Come, and discharged unmodified powder by pear shape separatory funnel bottom, dry, weighing to be modified(Activation)Ratio.By
It is directed to oiliness modified powder in the method and designs, therefore watersoluble modified powder is not applied to completely.In recent years, it is aqueous to change
Property technology be more and more applied in inorganic particle modified technique, but lack a kind of rationally effective modified gneiss side always
Method.
In water be in mainly suspension using watersoluble modified powder, do not tie bottom after standing, and unmodified powder in water from
So settle and tie the characteristic at bottom.After watersoluble modified powder is disperseed in the water it is uniform after, a period of time is stood, by container bottom
The modified powder outflow at bottom will not tied in certain inclination angle, and the unmodified powder at knot bottom is stayed in a reservoir, reach modified powder
The purpose of body and unmodified powder phase separation.Therefore, based on above mentioned problem, the utility model provides a kind of aqueous sample of inorganic particle
Product activation rate test device.
The content of the invention
In view of the shortcomings of the prior art, the utility model purpose is to provide a kind of inorganic particle aqueous sample activation rate to survey
Trial assembly is put, and test speed is fast, low cost, be obtain inorganic particle aqueous sample activation rate simple and effective method of testing it
One.
The utility model is provided technical problem to be solved and is realized using following technical scheme:
A kind of inorganic particle aqueous sample activation rate test device, including cuboid groove, and it is arranged on cuboid bottom land
The wedge in portion, and cuboid trench bottom is arranged on, the band plug circular hole of the thin end seamed edge of wedge.
The tilt angles of the wedge are 10 ° ~ 60 °.
The band plug Circularhole diameter is 0.5 ~ 3.5cm.
The volume of the cuboid groove is 200mL ~ 1000mL.
The material of the cuboid groove is glass, clear hard plastics, the one kind in crystalline ceramics.
The beneficial effects of the utility model:Compared with prior art, a kind of inorganic particle aqueous sample of the utility model is lived
Rate test device, for the activation rate test of inorganic particle aqueous sample, its design structure is simple, and test repeatability is good, with
The existing index of oiliness has certain comparativity, instrument long service life.
Brief description of the drawings
Fig. 1 is a kind of structural representation of inorganic particle aqueous sample activation rate test device of the present utility model;
Wherein, sequence number mark is as follows in figure:1- cuboids groove, 2- wedges, 3- band plug circular holes.
Fig. 2 is a kind of top view of inorganic particle aqueous sample activation rate test device of the present utility model.
Fig. 3 is a kind of inorganic particle aqueous sample activation rate method of testing schematic diagram of the present utility model.
Specific embodiment
Below in conjunction with the accompanying drawings and specific embodiment, the utility model is further elucidated.
Embodiment 1
A kind of inorganic particle aqueous sample activation rate test device as depicted in figs. 1 and 2, including cuboid groove 1, and
The wedge 2 of the bottom of cuboid groove 1 is arranged on, and is arranged on the bottom of cuboid groove 1, the band plug circular hole of the thin end seamed edge of wedge 2
3。
The material of cuboid groove 1 is glass, and volume is 200mL, a length of 8cm, a width of 5cm, a height of 5cm;Wedge 2 inclines
Oblique angle is 10 °, and most long right-angle side is 8cm as the length of cuboid groove 1;Band plug circular hole 3 is located at the bottom of cuboid groove 1, wedge shape
In the middle of the seamed edge at the thin end of block 2, a diameter of 0.5 cm.
The as shown in Figure 3 inorganic particle aqueous sample activation rate test device, method of testing is:
A kind of method of testing of inorganic particle aqueous sample activation rate, comprises the following steps:
(1)Sample pretreatment:By 10.00g(m1)Calcium carbonate aqueous sample and 80mL water fully rock concussion mixing;
(2)The device of sample:Two cuboid grooves 1 are placed one on the other according to staged, and will fully rock concussion
The powder aqueous mixtures of mixing are poured into inside upper cuboid groove 1;
(3)Test:After standing 1 h, open in upper cuboid groove 1, will suspend and sedimentation but still loose powder water
Inside the cuboid groove 1 that mixture is entered under, the deposit in the upper bottom of cuboid groove 1 is weighed after being dried at 105 DEG C
To 0.85g(m2)Unactivated sample;After the inner sample of cuboid groove 1 under stands 24 h, open cuboid groove 1 will suspend with
And settle but still loose powder aqueous mixtures discharge, the deposit in the bottom of lower rectangular slot 1 is weighed in drying at 105 DEG C
To 0.04g(m3)Unactivated sample, calculates as follows, you can obtain the activation rate η of the inorganic particle:
Then the sample activation rate is [10- (0.85+0.04)]/10*100%, i.e., 91.1%.
Embodiment 2
A kind of inorganic particle aqueous sample activation rate test device as shown in Figure 1, including cuboid groove 1, and set
In the wedge 2 of the bottom of cuboid groove 1, and the bottom of cuboid groove 1 is arranged on, the band plug circular hole 3 of the thin end seamed edge of wedge 2.
The material of cuboid groove 1 is clear hard plastics, and volume is 1000mL, a length of 20cm, a width of 10cm, a height of 5cm;
The inclination angle of wedge 2 is 60 °, and most long right-angle side is 20 cm as the length of cuboid groove 1;Band plug circular hole 3 is located at cuboid
The bottom of groove 1, in the middle of the seamed edge at the thin end of wedge 2, a diameter of 3.5 cm.Its application method is same as Example 1.
The as shown in Figure 3 inorganic particle aqueous sample activation rate test device, method of testing is:
A kind of method of testing of inorganic particle aqueous sample activation rate, comprises the following steps:
(1)Sample pretreatment:By 10.00g(m1)Calcium carbonate aqueous sample and 80mL water fully rock concussion mixing;
(2)The device of sample:Two cuboid grooves 1 are placed one on the other according to staged, and will fully rock concussion
The powder aqueous mixtures of mixing are poured into inside upper cuboid groove 1;
(3)Test:After standing 2h, open in upper cuboid groove 1, will suspend and settle but still loose powder water is mixed
Inside the cuboid groove 1 that compound is entered under, the deposit in the upper bottom of cuboid groove 1 is weighed after being dried at 105 DEG C and is obtained
0.70g(m2)Unactivated sample;After the inner sample of cuboid groove 1 under stands 48 h, open cuboid groove 1 will suspend and
Sedimentation but still loose powder aqueous mixtures discharge, the deposit in the bottom of lower rectangular slot 1 are weighed in drying at 105 DEG C and are obtained
0.01g(m3)Unactivated sample, calculates as follows, you can obtain the activation rate η of the inorganic particle:
Then the sample activation rate is [10- (0.70+0.01)]/10*100%, i.e., 92.9%.
Embodiment 3
A kind of inorganic particle aqueous sample activation rate test device as shown in Figure 1, including cuboid groove 1, and set
In the wedge 2 of the bottom of cuboid groove 1, and the bottom of cuboid groove 1 is arranged on, the band plug circular hole 3 of the thin end seamed edge of wedge 2.
The material of cuboid groove 1 is glass, and volume is 500mL, a length of 10cm, a width of 5cm, a height of 10cm;Wedge 2
Inclination angle is 15 °, and most long right-angle side is 10 cm as the length of cuboid groove 1;Band plug circular hole 3 is located at the bottom of cuboid groove 1,
In the middle of the seamed edge at the thin end of wedge 2, a diameter of 1cm.Its application method is same as Example 1.
The above is only preferred embodiment of the present utility model, it is noted that for the common skill of the art
For art personnel, on the premise of the utility model principle is not departed from, some improvement can also be made, these improvement also should be regarded as
Protection domain of the present utility model.