CN206252882U - A kind of taper extractor - Google Patents
A kind of taper extractor Download PDFInfo
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- CN206252882U CN206252882U CN201621281984.6U CN201621281984U CN206252882U CN 206252882 U CN206252882 U CN 206252882U CN 201621281984 U CN201621281984 U CN 201621281984U CN 206252882 U CN206252882 U CN 206252882U
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- tank body
- tube
- pipe
- recycling
- taper
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Abstract
The utility model discloses a kind of taper extractor, including tank body and rabbling mechanism, tank body top is provided with raw material feed tube and extractant feed tube, and the bottom of tank body is pyramidal structure, and tank base is provided with drain pipe;Drain pipe is connected with observation tube away from one end of tank body, and observation bottom of the tube is connected with the delivery pipe for conveying material, and drain pipe is provided with the first valve, and delivery pipe is provided with the second valve.With the effect for being conveniently layered, increasing operation rate.
Description
Technical field
The utility model is related to a kind of separator of two-phase immiscible liquid, more particularly to a kind of taper extractor.
Background technology
Extraction is that have different solubility in different solvents come the operation of separating mixture using component in system.Extensively
It is applied to the industry such as chemistry, pharmacy, metallurgy, food.In detailed process, liquid raw material is added in extractor, is added and liquid
In solvent it is immiscible and drug ingedient of to needing to extract has the extractant of higher solubility, extracted by stirring etc.
Journey, during original drug ingedient in liquid raw material extracted into extract, standing makes liquid raw material be layered with extract.It is quiet
To put need later and carry out a point liquid operation, the two-phase immiscible liquid after extraction is separated.If can two kinds it is immiscible
Liquid thoroughly separates the utilization rate for being then conducive to improving product.
At present during domestic production in enormous quantities extract, the extraction pot bottom for using is general in dome-type, after stirring stands
Extract is all that a point liquid is carried out in domed region.
Authorization Notice No. is CN202490604U, authorized announcement date is that the Chinese patent on October 17 in 2012 discloses one
Buffer reservoir point flow container, including tank body are planted, tank body top is respectively equipped with material inlet and reactor or condenser is joining true
Eat dishes without rice or wine, the pressure gauge with Guan Qiang UNICOMs be installed on the tank body between material inlet and vacuum port, the side wall of tank body be provided with
The liquid level gauge of tank body UNICOM, the bottom of tank body is provided with material outlet, and material outlet lower end is provided with vomit pipe, and vomit pipe is provided with
Baiting valve.
The deficiencies in the prior art part is that the container of dome-type causes point liquid level area between two-phase immiscible liquid
It is larger, it is difficult to two kinds of liquid are effectively separated, utilization rate is reduced.
Utility model content
The purpose of this utility model is to provide a kind of taper extractor, which solves and existing is difficult to be had two kinds of liquid
Separate problem is imitated, the effect for facilitating layering, increasing operation rate has been reached.
Above-mentioned technical purpose of the present utility model technical scheme is that:
A kind of taper extractor, including tank body and rabbling mechanism, tank body top are provided with raw material feed tube and extractant feed liquor
Pipe, the bottom of tank body is pyramidal structure, and tank base is provided with drain pipe;Drain pipe is connected with observation tube away from one end of tank body,
Observation bottom of the tube is connected with the delivery pipe for conveying material, and drain pipe is provided with the first valve, and delivery pipe is provided with the second valve
Door.
Using said structure, tank base is pyramidal structure, and with constantly carrying out for point liquid process, extract constantly subtracts
Few, the interface between two-phase immiscible liquid also constantly reduces, and effectively can separate two kinds of liquid in extractor, Ke Yiti
Utilization rate to drug ingedient high, drain pipe lower section is connected with observation tube, when the troubled liquor for observing two-phase mixtures is appeared in
When in observation tube, the second valve is closed in time, so as to the liquid of two-phase mixtures and remaining material solution are blocked in time
Before second valve of delivery pipe, prevent its via delivery pipe enter follow-up process container in, pollution extract and medicine into
Point.
More preferably:Qing Xie Jiao Du≤45 ° between the taper inclined plane and horizontal plane of tank base.
Using said structure, with the increase at angle of inclination, a point liquid effect is further improved, increased operation rate.
More preferably:Recycling can is also associated with tank body, recycling can is connected to observation tube bottom by the first recovery tube
Portion, recycling can is provided with discharging tube.
Using said structure, recycling can is used to reclaiming and temporarily storing the two-phase mixtures liquid in observation tube, it is also possible to use
Remaining material solution is operated in storage point liquid, it is possible to discharged from discharging tube.
More preferably:Reclaim pot bottom to be connected with extractant feed tube by the second recovery tube, on the second recovery tube
Water pump is connected with, the second recovery tube between water pump and extractant feed tube is provided with the 3rd valve.
Using said structure, be stored in and also include certain raw material in the liquid in recycling can, can with water pump by its
It is recycled in tank body by the second recovery tube, carries out reextraction, is increased operation rate.3rd valve is prevented during being used to feed
Extractant directly enters recycling can from the second recovery tube.
More preferably:Recycling can top is connected by return duct with tank body top.
Using said structure, the part distillate produced in stirring extraction process can be via in backflow manifold to recycling can.
More preferably:Observation tube includes the metal frame being connected with drain pipe and conveying pipe flange respectively and located at gold
Transparent pipe in category frame, transparent pipe wraps around the column for being provided with some connection metal frame two ends.
Using said structure, metal frame is provided a supporting role for transparent pipe, is prevented its stress too big and is destroyed, transparent
Pipe is between the metal frame and transparent pipe wraps around the column of setting and is conducive to from periphery protection transparent pipe.
More preferably:Rabbling mechanism includes being located at the motor at the top of tank body and is driven in tank body and by motor
Agitating paddle, agitating paddle includes the agitating shaft double helix ribbon opposite with two hands of spiral on agitating shaft.
Using said structure, the hand of spiral of double helix ribbon is and another conversely, a ribbon drives upward fluid
Bar ribbon drives fluid to move downward so that the liquid under stirring produces the flowing of different directions respectively in the upper and lower, this
Planting structure can improve mixed effect, be particularly suited for being susceptible to the mixing of the two-phase immiscible liquid of lower leaf.
More preferably:Tank body outside is provided with liquid level gauge.
Using said structure, the liquid height in tank body is able to observe that by liquid level gauge, can be by the beginning of liquid height
What step judged point liquid carries out degree, the liquid height shown in liquid level gauge reduce to extract liquid will be divided to finish when, then
Observation observation tube such that it is able to the more accurately end of control point liquid process, keeps the cleaning of extract not contaminated.
In sum, the utility model has the advantages that:1st, the taper of tank base sets You Qishi≤45 °
Angle of inclination sets and effectively can be separated two-phase immiscible liquid, increases operation rate;2nd, the observation of drain pipe lower section connection
Pipe, in time observation two-phase mixtures troubled liquor occur, be easy to close the second valve in time, by the liquid of two-phase mixtures with
And before remaining material solution is blocked in the second valve of delivery pipe in time, prevent it from entering follow-up operation via delivery pipe
In container, extract and drug ingedient are polluted;3rd, it is remaining after liquid and the extraction that recycling can is used to store in observation tube
Material solution, to carry out reextraction, improves its utilization rate.
Brief description of the drawings
Fig. 1 is the overall structure diagram of embodiment;
Fig. 2 be embodiment Fig. 1 in A portions partial enlarged drawing.
In figure, 1, tank body;11st, raw material feed tube;12nd, extractant feed tube;13rd, liquid level gauge;2nd, rabbling mechanism;21st, electricity
Machine;22nd, agitating paddle;221st, agitating shaft;222nd, double helix ribbon;3rd, drain pipe;31st, the first valve;4th, observation tube;41st, metal
Frame;42nd, transparent pipe;43rd, column;5th, delivery pipe;51st, the second valve;6th, recycling can;61st, the first recovery tube;62nd, discharging tube;
63rd, the second recovery tube;631st, the 3rd valve;64th, return duct;7th, water pump.
Specific embodiment
The utility model is described in further detail below in conjunction with accompanying drawing.
This specific embodiment is only that, to explanation of the present utility model, it is not to limitation of the present utility model, ability
Field technique personnel can make the modification without creative contribution to the present embodiment as needed after this specification is read, but
As long as all being protected by Patent Law in protection domain of the present utility model.
A kind of taper extractor, as depicted in figs. 1 and 2, including tank body 1 and rabbling mechanism 2, the top of tank body 1 is provided with raw material
Feed tube 11 and extractant feed tube 12, the outside of tank body 1 are provided with liquid level gauge 13.The bottom of tank body 1 is pyramidal structure, and tank body 1
Qing Xie Jiao Du≤45 ° between the taper inclined plane and horizontal plane of bottom.The bottom of tank body 1 is provided with drain pipe 3;Drain pipe 3 away from
One end of tank body 1 is connected with observation tube 4, and the bottom of observation tube 4 is connected with the delivery pipe 5 for conveying material, and drain pipe 3 is provided with
First valve 31, delivery pipe 5 is provided with the second valve 51.
Observation tube 4 includes the metal frame 41 being connected with drain pipe 3 and the flange of delivery pipe 5 respectively and in metal frame 41
Transparent pipe 42, transparent pipe 42 wraps around the columns 43 for being provided with some connection metal frame 41 two ends.
Rabbling mechanism 2 includes the stirring driven located at the motor 21 at the top of tank body 1 and in tank body 1 and by motor 21
Oar 22, agitating paddle 22 includes the double helix ribbon 222 opposite with two hands of spiral on agitating shaft 221 of agitating shaft 221.
Recycling can 6 is also associated with tank body 1, recycling can 6 is connected to the bottom of observation tube 4 by the first recovery tube 61, reclaimed
Tank 6 is provided with discharging tube 62.The bottom of recycling can 6 is connected by the second recovery tube 63 with extractant feed tube 12, the second recovery tube
Water pump 7 is connected with 63, the second recovery tube 63 between water pump 7 and extractant feed tube 12 is provided with the 3rd valve 631.Reclaim
The top of tank 6 is connected by return duct 64 with the top of tank body 1.
Use process:Liquid raw material and extractant are passed through tank body 1 from raw material feed tube 11 and extractant feed tube 12 respectively
It is interior, open motor 21 and drive agitating paddle 22 to be stirred extraction, stratification after the completion of extraction.The first valve 31 is opened by lower floor
Extract is released.The bottom of tank body 1 is pyramidal structure, and with constantly carrying out for point liquid process, extract is constantly reduced, two-phase not phase
Interface between solution body also constantly reduces, and effectively can separate two kinds of liquid in tank body 1, can improve to drug ingedient
Utilization rate, the lower section of drain pipe 3 is connected with observation tube 4, in the troubled liquor for observing two-phase mixtures appears in observation tube 4
When, the second valve 51 is closed in time, so as to the liquid of two-phase mixtures and remaining material solution are blocked in into delivery pipe 5 in time
The second valve 51 before, prevent its via delivery pipe 5 enter follow-up process container in, pollute extract and drug ingedient.
Troubled liquor in observation tube 4 can enter storage in recycling can 6 via the first recovery tube 61.Storage is opened to after a certain amount of
The valve 631 of water pump 7 and the 3rd, makes recovered liquid be recycled in tank body 1 via the second recovery tube 63, add extractant carry out it is secondary
Extraction, increases operation rate.Carry out the liquid raw material after fully extraction and be discharged into recycling can 6 and from the row of discharging tube 62 of recycling can 6
Go out.
Claims (8)
1. a kind of taper extractor, including tank body (1) and rabbling mechanism (2), it is characterized in that:Tank body (1) top is provided with original
Material feed tube (11) and extractant feed tube (12), the bottom of the tank body (1) is pyramidal structure, and tank body (1) bottom is provided with out
Liquid pipe (3);The drain pipe (3) is connected with observation tube (4) away from one end of tank body (1), and observation tube (4) bottom is connected with
Delivery pipe (5) for conveying material, the drain pipe (3) is provided with the first valve (31), and the delivery pipe (5) is provided with
Two valves (51).
2. a kind of taper extractor according to claim 1, it is characterized in that:The taper inclined plane of tank body (1) bottom
Qing Xie Jiao Du≤45 ° between horizontal plane.
3. a kind of taper extractor according to claim 1, it is characterized in that:Recycling can is also associated with the tank body (1)
(6), the recycling can (6) is connected to observation tube (4) bottom, recycling can (6) row of being provided with by the first recovery tube (61)
Liquid pipe (62).
4. a kind of taper extractor according to claim 3, it is characterized in that:Recycling can (6) bottom passes through second time
Closed tube (63) is connected with extractant feed tube (12), and water pump (7), the water pump (7) are connected with second recovery tube (63)
The 3rd valve (631) is provided with the second recovery tube (63) between extractant feed tube (12).
5. a kind of taper extractor according to claim 4, it is characterized in that:Recycling can (6) top passes through return duct
(64) it is connected with tank body (1) top.
6. a kind of taper extractor according to claim 1 or 4, it is characterized in that:The observation tube (4) including respectively with go out
Liquid pipe (3) and the metal frame (41) and the transparent pipe (42) in metal frame (41) of the connection of delivery pipe (5) flange, it is described
Bright pipe (42) wraps around the column (43) for being provided with some connection metal frame (41) two ends.
7. a kind of taper extractor according to claim 6, it is characterized in that:The rabbling mechanism (2) is including located at tank body
(1) motor (21) at the top of and the agitating paddle (22) driven in tank body (1) and by motor (21), the agitating paddle (22)
The opposite double helix ribbon (222) of two hands of spiral including agitating shaft (221) and on agitating shaft (221).
8. a kind of taper extractor according to claim 7, it is characterized in that:Tank body (1) outside is provided with liquid level gauge
(13)。
Priority Applications (1)
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CN201621281984.6U CN206252882U (en) | 2016-11-28 | 2016-11-28 | A kind of taper extractor |
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CN201621281984.6U CN206252882U (en) | 2016-11-28 | 2016-11-28 | A kind of taper extractor |
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CN206252882U true CN206252882U (en) | 2017-06-16 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107789862A (en) * | 2017-10-28 | 2018-03-13 | 株洲冶炼集团股份有限公司 | A kind of back extraction tank with heater |
CN108114506A (en) * | 2017-12-13 | 2018-06-05 | 安徽金龙山葛业有限公司 | A kind of pueraria lobata dissolution extraction device |
-
2016
- 2016-11-28 CN CN201621281984.6U patent/CN206252882U/en active Active
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107789862A (en) * | 2017-10-28 | 2018-03-13 | 株洲冶炼集团股份有限公司 | A kind of back extraction tank with heater |
CN108114506A (en) * | 2017-12-13 | 2018-06-05 | 安徽金龙山葛业有限公司 | A kind of pueraria lobata dissolution extraction device |
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CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 311199 Nanyuan street, Yuhang District, Zhejiang, Jiangsu Province, Su Village (security bridge) Patentee after: Hangzhou Yipin Jiuzhitang Pharmaceutical Co. Ltd. Address before: 311199 Nanyuan street, Yuhang District, Zhejiang, Jiangsu Province, Su Village (security bridge) Patentee before: Hangzhou Huadong medicine group Jiuzhitang Pharmaceutical Co. Ltd. |