CN206248491U - A kind of silk gum content tester - Google Patents

A kind of silk gum content tester Download PDF

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Publication number
CN206248491U
CN206248491U CN201621317673.0U CN201621317673U CN206248491U CN 206248491 U CN206248491 U CN 206248491U CN 201621317673 U CN201621317673 U CN 201621317673U CN 206248491 U CN206248491 U CN 206248491U
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CN
China
Prior art keywords
room
degumming
liquefied
water
recover
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621317673.0U
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Chinese (zh)
Inventor
王慧玲
周彬
刘华
戴毅
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Yancheng Institute of Industry Technology
Yancheng Vocational Institute of Industry Technology
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Yancheng Vocational Institute of Industry Technology
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Priority to CN201621317673.0U priority Critical patent/CN206248491U/en
Application granted granted Critical
Publication of CN206248491U publication Critical patent/CN206248491U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model provides a kind of silk gum content tester, it is characterized in that including in stacked up and down recover and degumming device;Recover includes water receiver and electric heater, electric heater is fixedly mounted with the bottom of water receiver, the top of water receiver is connected with the degumming room of degumming device bottom, degumming room bottom is fixedly mounted with ultrasonic oscillator, there are pipeline and siphoning installation in degumming room both sides respectively, pipeline and siphoning installation lower end communicate with recover, and pipeline upper end communicates with degumming room, and the lower port of siphoning installation fills a glue filter.A sample orifice plate is fixedly mounted with degumming room, sample orifice plate has a certain distance away from degumming room bottom, degumming room is provided with a sample and places mouth, liquefied room is connected above degumming room, liquefied room is respectively provided on two sides with liquefaction water inlet and liquefaction water out, there is multistage bend pipe in liquefied room, multistage bend pipe lower end communicates with degumming room upper end, multistage bend pipe upper end connects a passage, and passage upper end connects water filling room, and water filling room sealing is on liquefied room top.

Description

A kind of silk gum content tester
Technical field
The utility model is related to a kind of textile testing instrument, more particularly to a kind of silk gum content tester.
Background technology
The main component of silk is silk gum and fibroin, and silk gum is wrapped in the appearance of fibroin, has certain protection to make to fibroin With, but the property of silk gum is harder, if the content of silk gum excessively, can influence adding for gloss, feel and the silk fiber of fibroin Work technique;The presence of the impurity such as grease, wax also can bring certain difficulty to post-processing;Therefore, before processing, it is necessary to remove The debris such as most of silk gum, grease, wax are removed, makes that silk fiber is soft, loose, cleaning, increase product aesthetic property, improve quality, This operation is exactly the degumming of silk fiber.Degumming is one of important link in silk processing technology, the quality of degumming, to silk Quality and the row yielding of raw material all have significant effect, appropriate gel content (about 20%) left and right can strengthen embracing for silk Close, fibroin is shielded to a certain extent, be conducive to the processing and sorting of later process, silk piece is difficult disorder, and strand resists Pressure is wear-resisting;As gel content is very few, then obvolvent is influenceed, fabric easily fluffs;Conversely, as gel content is too high, then strand is rough hard, influence Silk gloss feel, the reed easy to wear in looming process;Meanwhile, consumption of raw materials is increased during weaving, increase cost.Therefore silk Gel content paid attention to by trade, be classified as selection check project.
The method of testing of current silk gum content is essentially according to professional standard FZ/T 40004-2009《Silk gum content is tried Proved recipe method》With commodity inspection standard SN/T2843-2011《The assay method of raw silk gum content》Carry out, cardinal principle is to be placed in sample After being dried to constant weight in baking oven, it is put into the stainless-steel pan for fill sodium carbonate liquor to heat and boils, and is gently mixed with glass bar, Taken out after 30min, fully washed with clear water at least three times.After total repetition above step three times, the sample of degumming is dried Dry to constant weight again, that is, obtain dry weight after degumming, by calculating silk boiling-off before and after dry weight it is poor, draw silk percentage containing glue.But There is following defect in this method:1st, when concentration of lye is too high, temperature is too high, and action time, long easily generation to fibroin was hindered Evil, causes test result inaccurate.2nd, for the determination methods of degumming degree, also it is not related in standard method.For silkworm The judgement of degumming of silk degree, the method for being provided on many documents at this stage is all that boiled silk is carried out by picric acid famille rose Dyeing, observes the color of boiled silk.The silk gum of silk, fibroin to carmine different with picric adsorption capacity, after coloring The degumming degree of silk is judged according to the apparent colour of silk.Silk is excessively sensitive and unstable with the effect of colouring agent, so Operation requirement for dyeing is higher, and test accuracy is not high, as a result can only be for qualitative analysis.3rd, in whole scouring processes, Need inspector to be continuously agitated by hand, not only take time and effort, reduce checkability, stir it is insufficient also result in it is de- Glue is uneven, influences the accuracy of assay, and in addition, stirring boiling water also causes potential to the personal safety of inspector Threat.
The content of the invention
It is an object of the invention to provide a kind of silk gum content tester, it can overcome the deficiencies in the prior art it Place.
A kind of silk gum content tester, it is characterized in that including in stacked up and down recover and degumming device;Recover Comprising water receiver and electric heater, electric heater is fixedly mounted with the bottom of water receiver, the top of water receiver is de- with degumming device bottom Glue room connects, and degumming room bottom is fixedly mounted with ultrasonic oscillator, and there are pipeline and siphoning installation, pipeline and siphon in degumming room both sides respectively Device lower end communicates with recover, and pipeline upper end communicates with degumming room, and the lower port of siphoning installation fills a glue filter.Degumming A sample orifice plate is fixedly mounted with room, sample orifice plate has a certain distance away from degumming room bottom, and degumming room is provided with a sample and places mouth, Liquefied room is connected above degumming room, liquefied room is respectively provided on two sides with liquefaction water inlet and liquefaction water out, there is multistage in liquefied room Bend pipe, multistage bend pipe lower end communicates with degumming room upper end, and multistage bend pipe upper end connects a passage, the connection water filling of passage upper end Room, water filling room sealing is on liquefied room top.
Easy to operate, quick the beneficial effects of the present invention are its simple structure, test result is accurate, reliable.Meanwhile, The surveyed adaptation of product is strong, general fiber such as mulberry silk, ricinus silk, mulberry fibre, high mallow fiber and other material containing glue class Gum content can be tested.It can also save energy simultaneously, not result in environmental pollution.
Brief description of the drawings
Accompanying drawing 1 is the structural representation of the present invention;Wherein 1 is water receiver, and 2 is electric heater, and 3 is ultrasonic oscillator, 4 It is glue filter, 5 is siphoning installation, and 6 is sample orifice plate, and 7 is pipeline, and 8 is that sample places mouth, and 9 is liquefied room, and 10 is multistage curved Pipe, 11 is liquefaction water inlet, and 12 is liquefaction water out, and 13 is passage, and 14 is degumming room, and 15 is water filling room.
Specific embodiment
A kind of silk gum content tester, it is characterized in that including in stacked up and down recover A and degumming device B;Reclaim Device A includes water receiver 1 and electric heater 2, and electric heater 2, top and the degumming device B of water receiver 1 are fixedly mounted with the bottom of water receiver 1 The degumming room 14 of bottom connects, and the bottom of degumming room 14 is fixedly mounted with ultrasonic oscillator 3, and there are pipeline 7 and rainbow in the both sides of degumming room 14 respectively Device 5 is inhaled, pipeline 7 and the lower end of siphoning installation 5 communicate with recover A, and the upper end of pipeline 7 communicates with degumming room 14, siphoning installation 5 Lower port fill a glue filter 4.A sample orifice plate 6 is fixedly mounted with degumming room 14, aperture is uniform-distribution with sample orifice plate 6, Sample orifice plate 6 has a certain distance away from the bottom of degumming room 14, and in scouring processes, sample orifice plate 6 can prevent short silk fiber from mixing Flow to the bottom of degumming room 14.Degumming room 14 is provided with a sample and places mouth 8, and degumming room 14 connects liquefied room 9, liquefied room 9 above Be respectively provided on two sides with liquefaction water inlet 11 and liquefaction water out 12, there is multistage bend pipe 10 in liquefied room 9, the lower end of multistage bend pipe 10 with The upper end of degumming room 14 communicates, and the upper end of multistage bend pipe 10 connects a passage 13, the upper end of passage 13 connection water filling room 15, water filling room 15 sealings are on the top of liquefied room 9.
During test, the silk for weighing certain mass is dried and weighed, and is designated as G0, silk is placed into mouth 8 from sample and is uniformly put Onto the sample orifice plate 6 in degumming room 14, close sample and place mouth 8;Appropriate deionized water is injected in recover A, will be returned Device A and degumming device B is received to connect.The liquefaction connection running water pipe of water inlet 11, the liquefaction connection sewer pipe of water out 12.
Electric heater 2 is opened, temperature is set at 200 DEG C or so, the water in recover A is brought rapidly up vaporization, by pipeline 7 Multistage bend pipe 10 is upwardly into, in the liquefied room 9 under the cooling effect of condensed water, steam liquefaction is back in degumming room 14, by Passage 13 is connected in the upper end of multistage bend pipe 10, its internal filling porous material prevents steam to be lost in.Open ultrasonic oscillator 3, ultrasonic frequency is controlled in 20-40kHZ, and power is 1kW, because " cavitation " of ultrasonic wave is acted on, make hot water and silk it is quick, Fully wetting, infiltration, silk gum is constantly separated with fibroin.With the accumulation of recirculation water, when recirculation water liquid level reaches siphon At the upper end bend pipe lower camber side of device 5, due to siphonage, recirculation water is together with the silk gum taken off just from siphoning installation 5 and degumming The position of the connection of room 14 flows into recover A through siphoning installation 5, due to the filtration of the lower end glue filter 4 of siphoning installation 5, silkworm The short fibre backed off on silk will not be entered into recover A.Water in recover A continuously vaporizes rising, cooling for reflux, takes off Glue, and silk gum is repeated several times in recover A, so all the time, silk gum will be taken off, and silk gum is all collected with degumming liquid To in recover A.
Such as in scouring processes, due to there is moisture loss to cause liquid level in degumming room 14 curved less than the upper end of siphoning installation 5 At pipe lower camber side, then deionized water directly can be added from water filling room 15, to ensure that scouring processes are smoothly completed.
After degumming terminates, electric heater 2 and ultrasonic oscillator 3 and cooling water are closed, by recover A and degumming device B points From, silk sample is taken out from sample orifice plate 6 and glue filter 4, drying is weighed and is designated as G1, then silk gum content be represented by:
Silk gum content=(G0-G1)/G0×100%
Above-mentioned involved circuit is known or general.

Claims (1)

1. a kind of silk gum content tester, it is characterized in that including in stacked up and down recover and degumming device;Recover bag Containing water receiver and electric heater, electric heater, the top of water receiver and the degumming of degumming device bottom are fixedly mounted with the bottom of water receiver Room connects, and degumming room bottom is fixedly mounted with ultrasonic oscillator, and there are pipeline and siphoning installation in degumming room both sides respectively, and pipeline and siphon are filled Put lower end to be communicated with recover, pipeline upper end communicates with degumming room, the lower port of siphoning installation fills a glue filter;Degumming room In be fixedly mounted with a sample orifice plate, sample orifice plate has a certain distance away from degumming room bottom, and degumming room is provided with a sample and places mouth, takes off Liquefied room is connected above glue room, liquefied room is respectively provided on two sides with liquefaction water inlet and liquefaction water out, there is multistage curved in liquefied room Pipe, multistage bend pipe lower end communicates with degumming room upper end, and multistage bend pipe upper end connects a passage, the connection water filling of passage upper end Room, water filling room sealing is on liquefied room top.
CN201621317673.0U 2016-12-03 2016-12-03 A kind of silk gum content tester Expired - Fee Related CN206248491U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621317673.0U CN206248491U (en) 2016-12-03 2016-12-03 A kind of silk gum content tester

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Application Number Priority Date Filing Date Title
CN201621317673.0U CN206248491U (en) 2016-12-03 2016-12-03 A kind of silk gum content tester

Publications (1)

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CN206248491U true CN206248491U (en) 2017-06-13

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106442211A (en) * 2016-12-03 2017-02-22 盐城工业职业技术学院 Silk sericin test instrument
CN108169060A (en) * 2018-02-20 2018-06-15 盐城工业职业技术学院 Natural color-cotton fiber non-fiber component content high speed tester device
CN109030276A (en) * 2018-09-16 2018-12-18 盐城工业职业技术学院 A kind of instrument based on the drum process test gum content of fiber containing glue

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106442211A (en) * 2016-12-03 2017-02-22 盐城工业职业技术学院 Silk sericin test instrument
CN108169060A (en) * 2018-02-20 2018-06-15 盐城工业职业技术学院 Natural color-cotton fiber non-fiber component content high speed tester device
CN109030276A (en) * 2018-09-16 2018-12-18 盐城工业职业技术学院 A kind of instrument based on the drum process test gum content of fiber containing glue

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170613

Termination date: 20171203

CF01 Termination of patent right due to non-payment of annual fee