CN206240115U - A kind of microemulsion extraction equipment - Google Patents
A kind of microemulsion extraction equipment Download PDFInfo
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- CN206240115U CN206240115U CN201621377090.7U CN201621377090U CN206240115U CN 206240115 U CN206240115 U CN 206240115U CN 201621377090 U CN201621377090 U CN 201621377090U CN 206240115 U CN206240115 U CN 206240115U
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- extractor
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Abstract
The utility model discloses a kind of microemulsion extraction equipment, including extractor, the bottom of the extractor sets discharge nozzle, the discharge nozzle is communicated with first point of flow container, second point of flow container by three-way pipe, first point of flow container sets drain pipe, and probe tube, recovery tube are set on the drain pipe, and the adjustable pipe of one end sealing is arranged in the drain pipe, the sealing end of the adjustable pipe sets first piston, and the openend of the adjustable pipe sets second piston；The first piston sets connecting rod away from one end of adjustable pipe, and the connecting rod is stretched out drain pipe, the first feed tube is set on the extractor, and return duct is set on the drain pipe.The beneficial effects of the utility model are：Extractor is entered by return duct if standard is not reaching to, adds fresh extractant to be extracted, until reaching extraction standard, it is only necessary to which an extractor can complete multitple extraction, not result in the waste of equipment.
Description
Technical field
The utility model relates generally to field of chemical equipment, specifically a kind of microemulsion extraction equipment.
Background technology
Microemulsion has many unique properties as separating medium, such as the spherical or bicontinuous structure of nanoscale, soon
Dynamical structure and property of solubilizing that speed polymerization again separate again, while micro emulsion particle is small, thus with larger mass transfer surface
Product, can improve mass-transfer efficiency, can be applied to hydrometallurgy, environmental protection, chemical industry, medicine and other fields, the single-stage extraction in extraction
The content of the extracting substance in extraction stoste is higher toward contact afterwards, and this is accomplished by carrying out multitple extraction, it is necessary to multiple is extracted
Tank is connected, and feed liquid and raffinate at different levels are all in contact with fresh extractant, and extraction yield is higher, but equipment is caused using more
Production cost is larger, and different extractant, extraction stoste coordinate reach extraction standard, it is necessary to extractor quantity not phase
Together, can be applicable under various extraction conditions to ensure equipment, the extractor of preparation can be relatively more, and the extractor positioned at end makes
Number of times is far smaller than the access times of front end extractor, is formed and wasted.
Utility model content
To solve deficiency of the prior art, the utility model provides a kind of microemulsion extraction equipment, is extracted by extractor
A point liquid operation is carried out after taking, is then sampled, the content of extracting substance in stoste is extracted after detection extraction, passed through if standard is reached
Recovery tube reclaims extraction stoste, and extractor is entered by return duct if standard is not reaching to, and adds fresh extractant to carry out
Extraction, until reaching extraction standard, it is only necessary to which an extractor can complete multitple extraction, not result in the waste of equipment.
The utility model to achieve the above object, is achieved through the following technical solutions：
A kind of microemulsion extraction equipment, including extractor, the bottom of the extractor set discharge nozzle, and the discharge nozzle leads to
Cross three-way pipe and be communicated with first point of flow container, second point of flow container, first point of flow container sets drain pipe, is set on the drain pipe
Probe tube, recovery tube, are arranged the adjustable pipe of one end sealing in the drain pipe, the sealing end of the adjustable pipe sets first and lives
Plug, the openend of the adjustable pipe sets second piston, and the adjustable pipe is located to be set between first piston, second piston and opens
Mouthful, the first chute being engaged with first piston, second piston is set in the drain pipe；The first piston is away from adjustable pipe
One end connecting rod is set, the connecting rod stretches out drain pipe, and sliding first piston, second piston can control liquid from sampling
Pipe or recovery tube outflow drain pipe, set the first feed tube on the extractor, return duct, described time are set on the drain pipe
Flow tube is connected with the first feed tube, and pump is set on the return duct.
The second piston away from first piston one end set the 3rd piston, the 3rd piston with diameter greater than second
The second chute being engaged with the 3rd piston is set in the diameter of piston, the adjustable pipe.
Second feed tube is set on the extractor.
Agitating device is set in the extractor, the agitating device includes rotating shaft, and the rotating shaft sets gradually from top to bottom
Puddler one, puddler two, puddler three, the two ends of the puddler one are upturned, and the two ends of the puddler two set montant,
The two ends of the puddler three are bent downwardly.
Also include oil cylinder, the piston rod of the oil cylinder is connected with connecting rod.
Contrast and prior art, the utility model beneficial effect is：
1st, the utility model carries out a point liquid operation after extractor is extracted, and then samples, extraction in detection extraction stoste
The content of material, if the extraction stoste if reaching standard after recovery tube reclaims extraction, passes through back if standard is not reaching to
Flow tube enters extractor, adds fresh extractant to be extracted, until reaching extraction standard, it is only necessary to an extractor
Multitple extraction is completed, the waste of equipment is not resulted in.
The 2nd, the second chute being engaged with the 3rd piston is set in the utility model adjustable pipe, when the 3rd piston slides into the
During the right-hand member of two chutes, first piston closes probe tube, recovery tube, slide to the left motion bar first piston be located at probe tube,
Probe tube is opened between recovery tube, opens recovery tube when the 3rd piston slides into the left end of the second chute, now second
Piston closes probe tube.
The 3rd, second feed tube be set on the utility model extractor, it is convenient to adding extractant in extractor.
4th, set in the utility model extractor and be stirred in agitating device extraction process, extractant is entered with extraction stoste
Row is fully contacted, and carries extraction efficiency.
5th, the piston rod and connecting rod of the utility model oil cylinder slip adjustable pipe easy to connect, control probe tube, recovery tube
Opening with close.
Brief description of the drawings
Accompanying drawing 1 is structural representation of the present utility model；
Accompanying drawing 2 is the structural representation that first piston is located at the first chute left end；
Accompanying drawing 3 is the structural representation that first piston is located at the first chute right-hand member；
Accompanying drawing 4 is the structural representation of extractor.
Label shown in accompanying drawing：1st, extractor；11st, discharge nozzle；12nd, three-way pipe；13rd, the first feed tube；14th, the second feed liquor
Pipe；15th, control valve；2nd, first point of flow container；3rd, second point of flow container；4th, drain pipe；41st, oil cylinder；5th, probe tube；6th, recovery tube；
7th, adjustable pipe；71st, first piston；72nd, second piston；73rd, it is open；74th, connecting rod；75th, the 3rd piston；8th, return duct；81、
Pump；9th, agitating device；91st, rotating shaft；92nd, puddler one；93rd, puddler two；94th, puddler three.
Specific embodiment
With reference to the drawings and specific embodiments, the utility model is described in further detail.It should be understood that these embodiments are only used for
Illustrate the utility model rather than limit scope of the present utility model.In addition, it is to be understood that reading the utility model instruction
Content after, those skilled in the art can make various changes or modifications to the utility model, and these equivalent form of values equally fall
In scope defined herein.
A kind of microemulsion extraction equipment, including extractor 1, the bottom of the extractor 1 set discharge nozzle 11, the discharging
Pipe 11 is communicated with first point of flow container, 2, second point of flow container 3 by three-way pipe 12, former with extraction using microemulsion as extractant first
Liquid peace certain proportion mixing, liquid stratification after extraction obtains extraction phase and raffinate phase, extraction phase is flowed into the second diversion cans,
Raffinate phase enters the first diversion cans.First point of flow container 2 sets drain pipe 4, probe tube 5 is set on the drain pipe 4, is reclaimed
The adjustable pipe 7 of one end sealing is arranged in pipe 6, the drain pipe 4, the sealing end of the adjustable pipe 7 sets first piston 71, described
The openend of adjustable pipe 7 sets second piston 72, and sealing ring is preferably arranged outside first piston 71, second piston 72, increases sealing
Property.The adjustable pipe 7 is located to be set in opening 73, the drain pipe 4 between first piston 71, second piston 72 and sets and first
The first chute that piston 71, second piston 72 are engaged；The first piston 71 sets connecting rod away from one end of adjustable pipe 7
74, the connecting rod 74 stretches out drain pipe 4, and when second piston 72 slides into the right-hand member of the first chute, first piston 71 will take
Sample pipe 5, recovery tube 6 are closed, and motion bar first piston 71 is slided to the left and is located at probe tube 5 dozens between probe tube 5, recovery tube 6
Open, open recovery tube 6 when second piston 72 slides into the left end of the first chute, now second piston 72 closes probe tube 5
Close, sliding first piston 71, second piston 72 can control liquid from probe tube 5 or the outflow drain pipe 4 of recovery tube 6.The extraction
Take and set on tank 1 first feed tube 13, return duct 8 is set on the drain pipe 4, the return duct 8 connects with the first feed tube 13
It is logical, pump 81 is set on the return duct 8, return duct 8 can be oppositely arranged with recovery tube 5, open probe tube 5 and be sampled, and examine
The content of extraction stoste (raffinate phase) the interior extracting substance surveyed after extraction, if reaching standard, after opening the recovery extraction of recovery tube 6
Extraction stoste, pump 81 is opened if too high levels are not reaching to standard, by return duct 8 by raffinate phase be pumped into extractor 1, plus
Enter fresh extractant to be extracted, until reaching extraction standard, it is only necessary to which an extractor 1 can complete multitple extraction, no
The waste of equipment can be caused.
Preferably, the second piston 72 sets the 3rd piston 75 away from one end of first piston 71, increases to drain pipe 4
Sealing；Set and the 3rd piston in the diameter with diameter greater than second piston 72 of the 3rd piston 75, the adjustable pipe 7
75 the second chutes being engaged, when the 3rd piston 75 slides into the right-hand member of the second chute, first piston 71 by probe tube 5, return
Closed tube 6 is closed, and motion bar first piston 71 is slided to the left positioned at probe tube 5 is opened between probe tube 5, recovery tube 6, when the 3rd
Recovery tube 6 is opened when piston 75 slides into the left end of the second chute, now second piston 72 closes probe tube 5, the 3rd lives
Probe tube 5, the Close All of recovery tube 6 when plug 75 is moved to right-hand member, recovery tube 6 is opened when the 3rd piston 75 is moved to left end, is taken
Sample pipe 5 is closed；Centre position is moved to, recovery tube 6 is closed, and probe tube 5 is opened, is conducive to control first piston 71, second to live
The stroke of plug 72.
Preferably, the second feed tube 14 is set on the extractor 1, it is convenient to adding extractant in extractor 1.
Preferably, set agitating device 9 in the extractor 1, the agitating device 9 includes rotating shaft 91, the rotating shaft 91 by
On set gradually puddler 1, puddler 2 93, puddler 3 94 downwards, the two ends of the puddler 1 are upturned, institute
State the two ends of puddler 2 93 and montant is set, the two ends of the puddler 3 94 are bent downwardly, improve mixing effect, make extractant with extraction
Take stoste to be fully contacted, carry extraction efficiency.
Preferably, also including oil cylinder 41, the piston rod of the oil cylinder 41 is connected with connecting rod 74, convenient to slide adjustable pipe 7,
Control probe tube 5, the opening of recovery tube 6 and closing.
Embodiment：
Agitating device 9, the agitating device 9 are set in a kind of microemulsion extraction equipment, including extractor 1, the extractor 1
Including rotating shaft 91, the rotating shaft 91 sets gradually puddler 1, puddler 2 93, puddler 3 94 from top to bottom, described to stir
Mix the two ends of bar 1 to be upturned, the two ends of the puddler 2 93 set montant, and the two ends of the puddler 3 94 are bent downwardly.Institute
The bottom for stating extractor 1 sets discharge nozzle 11, and the discharge nozzle 11 is communicated with first point of 2, second point of flow container by three-way pipe 12
Flow container 3, first mixes microemulsion as extractant with extraction stoste peace certain proportion, and liquid stratification after extraction is extracted
Phase and raffinate phase are taken, extraction phase is flowed into the second diversion cans, raffinate phase enters the first diversion cans.First point of flow container 2 is set
Drain pipe 4, sets the adjustable pipe 7 that one end sealing is arranged in probe tube 5, recovery tube 6, the drain pipe 4 on the drain pipe 4,
The sealing end of the adjustable pipe 7 sets first piston 71, and the openend of the adjustable pipe 7 sets second piston 72, preferably first
Sealing ring is arranged outside piston 71, second piston 72, increases sealing.The adjustable pipe 7 is located at first piston 71, second piston 72
Between opening 73 is set, the first chute being engaged with first piston 71, second piston 72 is set in the drain pipe 4；It is described
Second piston 72 away from first piston 71 one end set the 3rd piston 75, the 3rd piston 75 with diameter greater than second piston
The second chute being engaged with the 3rd piston 75 is set in 72 diameter, the adjustable pipe 7.The first piston 71 is away from activity
One end of pipe 7 sets connecting rod 74, and the connecting rod 74 stretches out drain pipe 4, also including oil cylinder 41, the piston rod of the oil cylinder 41
It is connected with connecting rod 74；When second piston 72 slides into the right-hand member of the first chute, first piston 71 is by probe tube 5, recovery tube 6
Close, motion bar first piston 71 is slided to the left positioned at probe tube 5 is opened between probe tube 5, recovery tube 6, work as second piston
72 slide into the first chute left end when recovery tube 6 is opened, now second piston 72 closes probe tube 5, slide first live
Plug 71, second piston 72 can control liquid from probe tube 5 or the outflow drain pipe 4 of recovery tube 6.Is set on the extractor 1
One feed tube 13, the second feed tube 14, set return duct 8 on the drain pipe 4, the return duct 8 connects with the first feed tube 13
It is logical, pump 81 is set on the return duct 8, open probe tube 5 and be sampled, extraction in the extraction stoste (raffinate phase) after detection extraction
The content of material is taken, if reaching standard, the extraction stoste after recovery tube 6 reclaims extraction is opened, if too high levels are not reaching to
Standard then enters extractor 1 by return duct 8, adds fresh extractant to be extracted, until reaching extraction standard, it is only necessary to
One extractor 1 can complete multitple extraction, not result in the waste of equipment.First feed tube 13, the second feed tube 14, first
Divide on 2, second point of feed tube of flow container 3 of flow container, recovery tube 6 and be respectively provided with control valve 15.The beneficial effect of the present embodiment is：
When the 3rd piston 75 slides into the right-hand member of the second chute, first piston 71 closes probe tube 5, recovery tube 6, slides live to the left
Lever first piston 71 is located at and opens probe tube 5 between probe tube 5, recovery tube 6, when the 3rd piston 75 slides into the second chute
Left end when recovery tube 6 is opened, now second piston 72 closes probe tube 5, is sampled when the 3rd piston 75 is moved to right-hand member
Pipe 5, the Close All of recovery tube 6, recovery tube 6 is opened when the 3rd piston 75 is moved to left end, and probe tube 5 is closed；It is moved to centre
Position, recovery tube 6 is closed, and probe tube 5 is opened, and is conducive to control first piston 71, the stroke of second piston 72, agitating device 9
Mixing effect is improved, extractant is fully contacted with extraction stoste, carried extraction efficiency.
Claims (5)
1. a kind of microemulsion extraction equipment, including extractor (1), it is characterised in that：The bottom of the extractor (1) sets discharging
Pipe (11), the discharge nozzle (11) is communicated with first point of flow container (2), second point of flow container (3), described first by three-way pipe (12)
Divide flow container (2) that drain pipe (4) is set, set in probe tube (5), recovery tube (6), the drain pipe (4) on the drain pipe (4)
The adjustable pipe (7) of an end closure is arranged, the sealing end of the adjustable pipe (7) sets first piston (71), the adjustable pipe (7)
Openend sets second piston (72), and the adjustable pipe (7) sets opening between first piston (71), second piston (72)
(73) the first chute being engaged with first piston (71), second piston (72), is set in the drain pipe (4)；Described first
Piston (71) sets connecting rod (74) away from one end of adjustable pipe (7), and the connecting rod (74) stretches out drain pipe (4), slides the
One piston (71), second piston (72) can control liquid to flow out drain pipe (4), the extraction from probe tube (5) or recovery tube (6)
Take and the first feed tube (13) is set on tank (1), return duct (8), the return duct (8) and first are set on the drain pipe (4)
Feed tube (13) is connected, and pump (81) is set on the return duct (8).
2. a kind of microemulsion extraction equipment according to claim 1, it is characterised in that：The second piston (72) is away from
One end of one piston (71) sets the 3rd piston (75), the 3rd piston (75) it is straight with diameter greater than second piston (72)
The second chute being engaged with the 3rd piston (75) is set in footpath, the adjustable pipe (7).
3. a kind of microemulsion extraction equipment according to claim 1, it is characterised in that：Is set on the extractor (1)
Two feed tubes (14).
4. a kind of microemulsion extraction equipment according to claim 1, it is characterised in that：Stirring is set in the extractor (1)
Device (9), the agitating device (9) includes rotating shaft (91), the rotating shaft (91) set gradually from top to bottom puddler one (92),
Puddler two (93), puddler three (94), the two ends of the puddler one (92) are upturned, and the two ends of the puddler two (93) set
Montant is put, the two ends of the puddler three (94) are bent downwardly.
5. a kind of microemulsion extraction equipment according to claim 1, it is characterised in that：Also include oil cylinder (41), the oil
The piston rod of cylinder (41) is connected with connecting rod (74).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621377090.7U CN206240115U (en) | 2016-12-14 | 2016-12-14 | A kind of microemulsion extraction equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621377090.7U CN206240115U (en) | 2016-12-14 | 2016-12-14 | A kind of microemulsion extraction equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206240115U true CN206240115U (en) | 2017-06-13 |
Family
ID=59007864
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621377090.7U Expired - Fee Related CN206240115U (en) | 2016-12-14 | 2016-12-14 | A kind of microemulsion extraction equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206240115U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109529408A (en) * | 2019-01-18 | 2019-03-29 | 北京兴通泰克科技发展有限公司 | A kind of superhigh temperature ultralow permeable reservoir microemulsion plugging removal technology |
| CN114029203A (en) * | 2021-11-19 | 2022-02-11 | 潍坊联威机械有限公司 | Pipe fitting undercoating negative pressure production facility |
| CN115054946A (en) * | 2022-07-21 | 2022-09-16 | 安徽恒景堂生物医药科技有限公司 | Extraction device for antibacterial liquid production |
-
2016
- 2016-12-14 CN CN201621377090.7U patent/CN206240115U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109529408A (en) * | 2019-01-18 | 2019-03-29 | 北京兴通泰克科技发展有限公司 | A kind of superhigh temperature ultralow permeable reservoir microemulsion plugging removal technology |
| CN114029203A (en) * | 2021-11-19 | 2022-02-11 | 潍坊联威机械有限公司 | Pipe fitting undercoating negative pressure production facility |
| CN115054946A (en) * | 2022-07-21 | 2022-09-16 | 安徽恒景堂生物医药科技有限公司 | Extraction device for antibacterial liquid production |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170613 Termination date: 20171214 |