CN206228983U - Online magnetic force auxiliary stirring liquid liquid extraction plant - Google Patents
Online magnetic force auxiliary stirring liquid liquid extraction plant Download PDFInfo
- Publication number
- CN206228983U CN206228983U CN201621333475.3U CN201621333475U CN206228983U CN 206228983 U CN206228983 U CN 206228983U CN 201621333475 U CN201621333475 U CN 201621333475U CN 206228983 U CN206228983 U CN 206228983U
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- CN
- China
- Prior art keywords
- extractor
- sealed
- liquid
- magnetic force
- magnet rotor
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The utility model discloses a kind of online magnetic force auxiliary stirring liquid liquid extraction plant, belong to extraction equipment field, for extracting, it includes sealed extractor, the outside of the sealed extractor is provided with the magnetic stirring apparatus of reverse symmetry setting, feed tube, blast pipe are provided with the top of wherein described sealed extractor, discharging tube is provided with the bottom of sealed extractor, and the inside of described sealed extractor is provided with vane type magnet rotor corresponding with magnetic stirring apparatus, vane type magnet rotor is provided with magnetic stir bar.In view of above-mentioned technical proposal, the utility model can adapt in on-line measuring device, the auto extractive and enrichment process of measured matter during on-line monitoring and automatic detection are realized, extraction time is short, good mixing effect, extraction efficiency are high, reduces labour intensity and the injury to experimenter.
Description
Technical field
The utility model belongs to extraction equipment field, specifically, more particularly to a kind of online magnetic force auxiliary stirring liquid
Liquid extraction equipment.
Background technology
Liquid-liquid extraction is the difference using thing to be extracted solubility in the compatible liquid phase of two kinds of complementations, by extract from
A kind of liquid-phase extraction is concentrated to another liquid phase, so as to reach the Sample Pretreatment Technique that material is separated and is enriched with.Above-mentioned extraction
Mode is widely applied to the fields such as chemical industry, environment, food, pharmacy.
But the side such as extraction or the hand extraction of separatory funnel is still shaken in the operation of the liquid-liquid extraction for generally using at present
Formula, has that extraction time is long, mixed effect is poor, extraction efficiency is low and hand labor intensity is big, wound is easily brought to experimenter
The problems such as evil.
The content of the invention
The purpose of this utility model is to provide a kind of online magnetic force auxiliary stirring liquid liquid extraction plant, and it is adapted to
Line detector, realizes the auto extractive and enrichment process of measured matter during on-line monitoring and automatic detection, extraction time
Short, good mixing effect, extraction efficiency are high, reduce labour intensity and the injury to experimenter.
To reach above-mentioned purpose, the utility model is achieved through the following technical solutions：
Online magnetic force auxiliary stirring liquid liquid extraction plant described in the utility model, including sealed extractor, institute
The outside for stating sealed extractor is provided with the magnetic stirring apparatus of reverse symmetry setting, wherein being set at the top of the sealed extractor
There are feed tube, blast pipe, discharging tube is provided with the bottom of sealed extractor, and the inside of described sealed extractor is provided with
Vane type magnet rotor corresponding with magnetic stirring apparatus, vane type magnet rotor is provided with magnetic stir bar.
Further speaking, the tail end of the feed tube described in the utility model is provided with rotation liquid distribution sprayer, the liquid spray of rotation cloth
Head is located at the top of sealed extractor.
Further speaking, speed regulator, the rotating speed are additionally provided with the sealed extractor described in the utility model
Adjuster is connected with magnetic stirring apparatus.
Further speaking, thermoregulator is also equipped with the sealed extractor described in the utility model, temperature is adjusted
Section device is connected with temperature regulating device, and temperature regulating device is located in sealed extractor.
Further speaking, the vane type magnet rotor described in the utility model is installed on the leaf of both sides in sealed extractor
On piece bolt.
Further speaking, the sealed extractor described in the utility model is made up of polytetrafluoroethylmaterial material.
Further speaking, the rotating speed of the vane type magnet rotor described in the utility model is less than or equal to 160r/min.
Compared with prior art, the beneficial effects of the utility model are：
1st, the utility model can be connected with the external computer controls part of on-line detecting system, thoroughly instead of artificial
Mechanical manipulation, while also reducing the labour intensity of experimenter, avoiding the directly contact of people and toxic reagent.
2nd, the Automation Design used in the utility model not only avoids manually-operated individual sex differernce, and causes
Extraction conditions easily optimization and control, can online complete the processes such as auto injection, extraction, separation, cleaning, its simple structure, operation
Convenient, rate of extraction is fast, favorable reproducibility.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Fig. 2 is top view of the present utility model.
Fig. 3 is sectional view of the present utility model.
Fig. 4 is the structural representation of the utility model middle period chip magnet rotor.
In figure：1st, magnetic stirring apparatus；2nd, sealed extractor；3rd, bracket fixing bolt；4th, speed regulator；5th, temperature is adjusted
Section device；6th, feed tube；7th, blast pipe；2-1, vane type magnet rotor；2-1-1, magnetic stir bar；2-2, blade bolt；2-3, leaf
Piece nut；2-4, discharging tube；2-5, rotation liquid distribution sprayer.
Specific embodiment
Below in conjunction with the accompanying drawings and embodiment is described further to technical scheme described herein.
Embodiment 1：A kind of online magnetic force auxiliary stirring liquid liquid extraction plant, including sealed extractor 2, the sealing
The outside of formula extractor 2 is provided with the magnetic stirring apparatus 1 of reverse symmetry setting, wherein the top of the sealed extractor 2 is provided with
Feed tube 6, blast pipe 7, discharging tube 2-4 is provided with the bottom of sealed extractor 2, and described sealed extractor 2 is interior
Portion is provided with vane type magnet rotor 2-1 corresponding with magnetic stirring apparatus 1, and vane type magnet rotor 2-1 is provided with magnetic stir bar 2-1-
1。
Embodiment 2：A kind of online magnetic force auxiliary stirring liquid liquid extraction plant, including sealed extractor 2, the sealing
The outside of formula extractor 2 is provided with the magnetic stirring apparatus 1 of reverse symmetry setting, wherein the top of the sealed extractor 2 is provided with
Feed tube 6, blast pipe 7, discharging tube 2-4 is provided with the bottom of sealed extractor 2, and described sealed extractor 2 is interior
Portion is provided with vane type magnet rotor 2-1 corresponding with magnetic stirring apparatus 1, and vane type magnet rotor 2-1 is provided with magnetic stir bar 2-1-
1.The tail end of the feed tube 6 is provided with rotation liquid distribution sprayer 2-5, and rotation liquid distribution sprayer 2-5 is located at the top of sealed extractor 2
Portion.Speed regulator 4 is additionally provided with the sealed extractor 2, the speed regulator 4 is connected with magnetic stirring apparatus 1.It is described
Thermoregulator 5 is also equipped with sealed extractor 2, thermoregulator 5 is connected with temperature regulating device, temperature regulating device is located at sealing
In formula extractor 2.The vane type magnet rotor 2-1 is installed on the blade bolt 2-2 of both sides in sealed extractor 2.It is described
Sealed extractor 2 is made up of polytetrafluoroethylmaterial material.The rotating speed of the vane type magnet rotor 2-1 is less than or equal to 160r/min.
The structure of remainder is identical with the structure and annexation described in embodiment 1.
In actual use, feed tube 6 is connected with the pipeline of various reagents respectively, and in outside auto injection
Control device, including plunger displacement pump, Prorating valve, magnetic valve etc. in the presence of by the extraction at regular time and quantity of sample, extractant simultaneously
It is added in sealed extractor 2.Sealed extractor 2 is made of polytetrafluoroethylmaterial material.When sample to be extracted is entered into
After sealed extractor 2, magnetic stirring apparatus 1 can be acted on through sealed extractor 2 and is fixed on inside sealed extractor 2
Vane type magnet rotor 2-1, and cause vane type magnet rotor 2-1 rotating speed control within 160r/min.Vane type magnetic turns
Sub- 2-1 is fixed on the inside of sealed extractor 2, and vane type magnet rotor 2-1 by blade bolt 2-2 and blade nut 2-3
It is 2, is symmetricly set on the both sides of sealed extractor 2.
Sample to be extracted enters from feed tube 6.After extraction process starts, by the rotation cloth liquid positioned at the tail end of feed tube 6
Gradually equably be sprayed onto extract in extractor by shower nozzle 2-5, by external electrical magnet valve control blast pipe, the switch of feed tube,
So that feed liquor exhaust is smooth.Vane type magnet rotor 2-1 carries out magnetically-actuated by corresponding magnetic stirring apparatus 1, and symmetrically
The vane type magnet rotor 2-1 of setting can realize the rotation of different rotating speeds and direction in the presence of magnetic stirring apparatus 1, be used to stir
Mix extract and sample to be extracted.Attemperating unit can be realized in sealed extractor 2 in the presence of speed regulator 4
The regulation of fluid temperature.
After the completion of extraction, the magnetic valve of the connection of blast pipe 7 is opened so that the liquid stratification in sealed extractor 2,
Extract and waste liquid after stratification can respectively be flowed out by discharging tube 2-4.After the completion of discharge opeing, cleaning fluid passes through feed tube 6
By rotation liquid distribution sprayer 2-5, rotation is cleaned to the inwall of sealed extractor 2 automatically under the pressure of outer flowpath.
In the utility model, sealed extractor 2 is processed using polytetrafluoroethylmaterial material, and magnetic stirring apparatus 1 can
Magnetic stir bar 2-1-1 on vane type magnet rotor 2-1, driving blade formula magnetic are acted directly on to penetrate sealed extractor 2
Rotor 2-1 is rotated with different rotating speeds and direction.Wherein, the vane type magnet rotor 2-1 is equally made of polytetrafluoroethylene (PTFE).
Magnetic stir bar 2-1-1 is sealed in vane type magnet rotor 2-1, and leaf structure can increase the intensity of stirring, while poly- four
PVF material surface is smooth, corrosion-resistant, is easy to cleaning and noresidue.
Claims (7)
1. a kind of online magnetic force auxiliary stirring liquid liquid extraction plant, including sealed extractor (2), it is characterised in that：It is described
The outside of sealed extractor (2) is provided with the magnetic stirring apparatus (1) of reverse symmetry setting, wherein the sealed extractor (2)
Top be provided with feed tube (6), blast pipe (7), be provided with discharging tube (2-4) in the bottom of sealed extractor (2), and described
The inside of sealed extractor (2) is provided with vane type magnet rotor (2-1) corresponding with magnetic stirring apparatus (1), vane type magnet rotor
(2-1) is provided with magnetic stir bar (2-1-1).
2. online magnetic force auxiliary according to claim 1 stirs liquid liquid extraction plant, it is characterised in that：The feed tube
(6) tail end is provided with rotation liquid distribution sprayer (2-5), and rotation liquid distribution sprayer (2-5) is located at the top of sealed extractor (2).
3. online magnetic force auxiliary according to claim 1 stirs liquid liquid extraction plant, it is characterised in that：It is described sealed
Speed regulator (4) is additionally provided with extractor (2), the speed regulator (4) is connected with magnetic stirring apparatus (1).
4. online magnetic force auxiliary according to claim 1 stirs liquid liquid extraction plant, it is characterised in that：It is described sealed
Thermoregulator (5) is also equipped with extractor (2), thermoregulator (5) is connected with temperature regulating device, temperature regulating device is located at sealing
In formula extractor (2).
5. online magnetic force auxiliary according to claim 1 stirs liquid liquid extraction plant, it is characterised in that：The vane type
Magnet rotor (2-1) is installed on the blade bolt (2-2) of sealed extractor (2) interior both sides.
6. the online magnetic force auxiliary according to any claim in claim 1 to 5 stirs liquid liquid extraction plant, and it is special
Levy and be：The sealed extractor (2) and vane type magnet rotor (2-1) are made up of polytetrafluoroethylmaterial material.
7. the online magnetic force auxiliary according to any claim in claim 1 to 5 stirs liquid liquid extraction plant, and it is special
Levy and be：The rotating speed of the vane type magnet rotor (2-1) is less than or equal to 160r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621333475.3U CN206228983U (en) | 2016-12-06 | 2016-12-06 | Online magnetic force auxiliary stirring liquid liquid extraction plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621333475.3U CN206228983U (en) | 2016-12-06 | 2016-12-06 | Online magnetic force auxiliary stirring liquid liquid extraction plant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206228983U true CN206228983U (en) | 2017-06-09 |
Family
ID=58979034
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621333475.3U Expired - Fee Related CN206228983U (en) | 2016-12-06 | 2016-12-06 | Online magnetic force auxiliary stirring liquid liquid extraction plant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206228983U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107746952A (en) * | 2017-10-16 | 2018-03-02 | 包头稀土研究院 | The method for avoiding attachment crystal in mixed zone in Liquid-liquid Extraction Processes |
| CN110118680A (en) * | 2019-05-08 | 2019-08-13 | 山东省计量科学研究院 | The oily efficient extraction plant of the infrared full-automatic survey of one kind and extracting process |
-
2016
- 2016-12-06 CN CN201621333475.3U patent/CN206228983U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107746952A (en) * | 2017-10-16 | 2018-03-02 | 包头稀土研究院 | The method for avoiding attachment crystal in mixed zone in Liquid-liquid Extraction Processes |
| CN110118680A (en) * | 2019-05-08 | 2019-08-13 | 山东省计量科学研究院 | The oily efficient extraction plant of the infrared full-automatic survey of one kind and extracting process |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170609 Termination date: 20191206 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |