CN206184453U - Molecular sieve developments synthesizer - Google Patents
Molecular sieve developments synthesizer Download PDFInfo
- Publication number
- CN206184453U CN206184453U CN201621249933.5U CN201621249933U CN206184453U CN 206184453 U CN206184453 U CN 206184453U CN 201621249933 U CN201621249933 U CN 201621249933U CN 206184453 U CN206184453 U CN 206184453U
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- connecting rod
- sliding block
- synthesizer
- rivet
- cover
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Abstract
The utility model provides a molecular sieve developments synthesizer, belongs to molecular sieve synthesis experiment equipment technical field. The utility model relates to a solve present synthesizer reactant and mix unevenly, product purity is low, synthetic stability is low, the crystallization is chronic, the poor problem of repeatability. First slider is connected with first connecting rod, and first connecting rod is connected through the first rivet and the one end of second connecting rod, and the other end of second connecting rod passes through the second rivet and is connected with the second slider, circular motion is to first rivet in the OVAL groove slide, the second slider slides on last vertical slide way, and synthetic reation kettle passes through vertical slide way sliding fit down with an electric heating jacket section of thick bamboo in arranging an electric heating jacket section of thick bamboo in, install compression spring between reation kettle base and synthesizer base, the third connecting rod passes electric heating jacket cover and casing, and the second slider is connected to the upper end, and synthetic reaction kettle cover is connected to the lower extreme. The utility model discloses synthetic cauldron and heating sleeve slide way type design, stable sliding, the suitability is strong, simple structure, easily operation.
Description
Technical field
The utility model is related to a kind of Zeolite synthesis device, and in particular to a kind of molecular sieve dynamic synthesizer, belongs to
Zeolite synthesis technical field of experiment equipment.
Background technology
At present, the synthesis mode of molecular sieve is mainly static crystallization synthetic method and dynamic crystallization synthetic method.Static monitor
Device is mainly reactor and baking oven, and the synthesis materials such as silicon source, silicon source, template are added in synthesis reaction vessel, then will
Reactor is placed into baking oven.Whole synthetic reaction process is static all the time, there are reaction raw materials and mixes uneven, the molecule of synthesis
Sieve has stray crystal, and purity is low, and crystallization time is long, and controls temperature using baking oven, and temperature control precision is inadequate.Dynamic synthetic method
Device is mainly the synthesis reactor with heater and is furnished with agitating device again, although can improve the crystallization of crystallization rate and product
Degree, but under specific conditions of mixture ratios, stirring dynamic crystallization method, crystallization product grains size is uneven, product poor repeatability.
Utility model content
It has been given below on brief overview of the present utility model, to provide on some sides of the present utility model
The basic comprehension in face.It should be appreciated that this general introduction is not on exhaustive general introduction of the present utility model.It is not intended to really
Fixed crucial or pith of the present utility model, nor intended limitation scope of the present utility model.Its purpose is only with letter
The form of change provides some concepts, in this, as the preamble in greater detail discussed after a while.
In consideration of it, the purpose of this utility model is directed to existing synthesizer reaction raw materials mixing inequality, product purity
Low, synthesising stability is low, and crystallization time is long, the problem of poor repeatability, and then provides a kind of simple structure, easy to install
Molecular sieve dynamic synthesizer.
The scheme that the utility model is taken is：A kind of molecular sieve dynamic synthesizer, including rotation system and heating system
System；
Rotation system includes the first sliding block, oval-shaped groove slideway, first connecting rod, rivet, second connecting rod, upper vertical cunning
Road, the second sliding block, third connecting rod, synthetic reaction kettle cover, synthesis reaction vessel, lower vertical slideway, reactor base, compression spring,
Synthesizer base and housing；
Heating system is electrical heating sleeve；
First sliding block, oval-shaped groove slideway, first connecting rod, rivet, second connecting rod, upper vertical slideway, second are slided
Block is placed in housing；
First sliding block is connected with one end of first connecting rod, and the other end of first connecting rod is connected by the first rivet and second
One end connection of bar, the other end of second connecting rod is connected by the second rivet with the second sliding block；First rivet is in oval-shaped groove
Moved in a circle in slideway；Upper vertical slideway is arranged on the base plate of housing, and the second sliding block is slided on upper vertical slideway, oval
Connected in star slideway is placed in the surface of the second sliding block；
Electric heating cover cover is arranged on electric heating cover upper end, and electrical heating sleeve is placed on synthesizer base；Synthesis reaction vessel
It is placed in electrical heating sleeve, and is slidably matched by lower vertical slideway with electrical heating sleeve；The bottom of synthesis reaction vessel is provided with instead
Bottom seat is answered, compression spring is installed between reactor base and synthesizer base；The top of synthesis reaction vessel is provided with synthetic reaction
Kettle cover；Third connecting rod passes through electric heating cover cover and housing, and its upper end connects the second sliding block, its lower end connection synthesis reaction vessel
Lid.
Further：The third connecting rod is provided with sealing ring through the position of electric heating cover cover.It is arranged such, prevents
Heat is excessive, it is ensured that do not lose to thermal environment stabilization, heating-up temperature.
Further：First sliding block is rotated by motor, and the motor is buncher.It is arranged such, can leads to
Cross motor speed control mixing rate.
The effect that the utility model is reached is：
The sliding block of the utility model first drives the first connecting rod being connected, second connecting rod to do circumference in oval-shaped groove slideway
Motion, because the ellipse radii moment is in change, so as to drive on the second sliding block, third connecting rod, synthetic reaction kettle cover and reactor
Lower motion, reaching is well mixed the raw material of synthesis of molecular sieve, realizes that molecular sieve dynamically synthesizes.Electrical heating sleeve can realize synthesis
Process temperature is precisely controlled.Furthermore it is possible to passing through motor speed controls mixing rate.Heating muff can be opened after crystallization synthesis
Lid, realizes charging, takes out the cleaning of synthetic product and reactor.More specifically：
1st, synthesis reactor and heating muff chute type are designed, and are slided steady.
2nd, present apparatus strong applicability, simple structure, easily operated, user need to only set reaction time and temperature rotating speed
, it is capable of achieving crystallization whole process unattended.
3rd, cause that the medium in hydrothermal reaction kettle is sufficiently mixed because rotation system moves up and down, thus reaction speed
Degree is fast, and fully thoroughly, zeolite product is reproducible than simple static effects more preferably for reaction.
4th, the reaction molecular sieves state synthesizer small volume, save space.
Brief description of the drawings
Fig. 1 is a kind of structural representation of molecular sieve dynamic synthesizer of the present utility model.
Specific embodiment
For clarity and conciseness, all features of actual implementation method are not described in the description.However, should
Understand, many decisions specific to implementation method must be made during any this practical embodiments are developed, so as to reality
The objectives of existing developer, for example, meet those restrictive conditions related to system and business, and these restrictive conditions
May be changed with the difference of implementation method.Additionally, it also should be appreciated that, although development is likely to be very multiple
It is miscellaneous and time-consuming, but for having benefited from those skilled in the art of the utility model disclosure, this development is only
It is routine task.
Herein, in addition it is also necessary to which explanation is a bit, in order to avoid having obscured the utility model because of unnecessary details, in Shen
Please illustrate only in file with according to the closely related apparatus structure of scheme of the present utility model and/or process step, and save
The other details little with the utility model relation are omited.
A kind of molecular sieve dynamic synthesizer of present embodiment, including rotation system and heating system；
Institute's rotation system include the first sliding block 1, oval-shaped groove slideway 2, first connecting rod 3, rivet 4, second connecting rod 5, on
Vertical slideway 6, the second sliding block 7, third connecting rod 8, synthetic reaction kettle cover 11, synthesis reaction vessel 14, lower vertical slideway 12, reactor
Base 15, compression spring 16, synthesizer base 17 and housing 20；
Heating system includes electrical heating sleeve 13；
First sliding block 1, oval-shaped groove slideway 2, first connecting rod 3, rivet 4, second connecting rod 5, upper vertical slideway 6,
Second sliding block 7 is placed in housing 20；
First sliding block 1 is connected with one end of first connecting rod 3, and the other end of first connecting rod 3 is by the first rivet 4 and the
One end connection of two connecting rods 5, the other end of second connecting rod 5 is connected by the second rivet 41 with the second sliding block 7；First rivet 4 exists
Moved in a circle in oval-shaped groove slideway 2；Upper vertical slideway 6 is arranged on the base plate of housing 20, and the second sliding block 7 is upper vertical
Slided on slideway 6, oval-shaped groove slideway 2 is placed in the surface of the second sliding block 7；
Electric heating cover cover 10 is arranged on the upper end of electrical heating sleeve 13, and electrical heating sleeve 13 is placed on synthesizer base 17；
Synthesis reaction vessel 14 is placed in electrical heating sleeve 13, and is slidably matched by lower vertical slideway 12 with electrical heating sleeve 13；Synthesis
The bottom of reactor 14 is provided with reactor base 15, and compression spring 16 is provided between reactor base 15 and synthesizer base 17；
The top of synthesis reaction vessel is provided with synthetic reaction kettle cover 11；Third connecting rod 8 passes through electric heating cover cover 10 and housing 20, its upper end
The second sliding block 7 is connected, its lower end connects synthetic reaction kettle cover 11.
More specifically：The third connecting rod 8 is provided with sealing ring 9 through the position of electric heating cover cover 10.It is arranged such,
Prevent heat excessive, it is ensured that not lose to thermal environment stabilization, heating-up temperature.
More specifically：First sliding block 1 is rotated by motor, and the motor is buncher.It is arranged such, can leads to
Cross motor speed control mixing rate.
Present embodiment can also include control system, and control system includes temperature sensor, electric machine controller and control
Panel, can set switch, display instrument, indicator lamp on control panel, alarm lamp, wherein display instrument show including temperature
Device, temperature adjustment buttons, speed display, rotational speed regulation button.Thermostatic digital display meter shows that user can be real according to reaction
Test required temperature sets itself.Motor speed can need any adjustment according to experiment, and with power interruption recovering function, in dispatch from foreign news agency
After the unexpected dead electricity in source is sent a telegram here again, equipment can resume operation by former setting program automatically；Additionally, control parameter has exception, meeting
Start alarm, send sound.
Although the implementation method disclosed in the utility model is as above, its content is only to facilitate understand the utility model
Technical scheme and the implementation method that uses, be not intended to limit the utility model.Any the utility model art
Interior technical staff, on the premise of the core technology scheme disclosed in the utility model that do not depart from, can be in the form implemented
With any modification and change are made in details, but the protection domain that the utility model is limited still must be with appending claims
The scope of restriction is defined.
Claims (3)
1. a kind of molecular sieve dynamic synthesizer, it is characterised in that：Including rotation system and heating system；
The rotation system includes that the first sliding block (1), oval-shaped groove slideway (2), first connecting rod (3), rivet (4), second connect
Bar (5), upper vertical slideway (6), the second sliding block (7), third connecting rod (8), synthetic reaction kettle cover (11), synthesis reaction vessel (14),
Vertical slideway (12), reactor base (15), compression spring (16), synthesizer base (17) and housing (20) down；
Heating system includes electrical heating sleeve (13)；
First sliding block (1), oval-shaped groove slideway (2), first connecting rod (3), rivet (4), second connecting rod (5), it is upper vertically
Slideway (6), the second sliding block (7) are placed in housing (20)；
First sliding block (1) is connected with one end of first connecting rod (3), and the other end of first connecting rod (3) passes through the first rivet (4)
One end with second connecting rod (5) is connected, and the other end of second connecting rod (5) is connected by the second rivet (41) with the second sliding block (7)；
First rivet (4) moves in a circle in oval-shaped groove slideway (2)；Base plate of the upper vertical slideway (6) installed in housing (20)
On, the second sliding block (7) is slided on upper vertical slideway (6), and oval-shaped groove slideway (2) is placed in the surface of the second sliding block (7)；
Electric heating cover cover (10) is placed in synthesizer base (17) installed in electrical heating sleeve (13) upper end, electrical heating sleeve (13)
On；Synthesis reaction vessel (14) is placed in electrical heating sleeve (13), and sliding by lower vertical slideway (12) with electrical heating sleeve (13)
It is dynamic to coordinate；The bottom of synthesis reaction vessel (14) is provided with reactor base (15), reactor base (15) and synthesizer base (17)
Between compression spring (16) is installed；The top of synthesis reaction vessel is provided with synthetic reaction kettle cover (11)；Third connecting rod (8) adds through electricity
Hot jacket cover (10) and housing (20), its upper end connect the second sliding block (7), and its lower end connects synthetic reaction kettle cover (11).
2. a kind of molecular sieve dynamic synthesizer according to claim 1, it is characterised in that：The third connecting rod 8 is passed through
The position of electric heating cover cover (10) is provided with sealing ring (9).
3. a kind of molecular sieve dynamic synthesizer according to claim 1 and 2, it is characterised in that：First sliding block (1)
It is rotated by motor, the motor is buncher.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621249933.5U CN206184453U (en) | 2016-11-18 | 2016-11-18 | Molecular sieve developments synthesizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621249933.5U CN206184453U (en) | 2016-11-18 | 2016-11-18 | Molecular sieve developments synthesizer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206184453U true CN206184453U (en) | 2017-05-24 |
Family
ID=58727326
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621249933.5U Withdrawn - After Issue CN206184453U (en) | 2016-11-18 | 2016-11-18 | Molecular sieve developments synthesizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206184453U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106378082A (en) * | 2016-11-18 | 2017-02-08 | 黑龙江省能源环境研究院 | Molecular sieve dynamic synthesis device |
-
2016
- 2016-11-18 CN CN201621249933.5U patent/CN206184453U/en not_active Withdrawn - After Issue
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106378082A (en) * | 2016-11-18 | 2017-02-08 | 黑龙江省能源环境研究院 | Molecular sieve dynamic synthesis device |
| CN106378082B (en) * | 2016-11-18 | 2018-04-27 | 黑龙江省能源环境研究院 | A kind of molecular sieve dynamic synthesizer |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20170524 Effective date of abandoning: 20180427 |