CN206168410U - Intensification feed arrangement in production of MBS resin - Google Patents
Intensification feed arrangement in production of MBS resin Download PDFInfo
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- CN206168410U CN206168410U CN201621088340.5U CN201621088340U CN206168410U CN 206168410 U CN206168410 U CN 206168410U CN 201621088340 U CN201621088340 U CN 201621088340U CN 206168410 U CN206168410 U CN 206168410U
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- emulsion
- breakdown
- kettle
- intensification
- cauldron
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Abstract
The utility model provides an intensification feed arrangement in production of MBS resin, includes that one -level breakdown of emulsion cauldron, second grade breakdown of emulsion cauldron, tertiary breakdown of emulsion cauldron, discharge gate, cauldron are personally experienced sth. Part of the body, the feed inlet, one -level breakdown of emulsion cauldron, second grade breakdown of emulsion cauldron, tertiary breakdown of emulsion cauldron structure identical, the discharge gate of one -level breakdown of emulsion cauldron be connected with the feed inlet of second grade breakdown of emulsion cauldron, the discharge gate of second grade breakdown of emulsion cauldron be connected with the feed inlet of tertiary breakdown of emulsion cauldron, the internal portion of cauldron be provided with the agitator and be spiral helicine thermal exhaust pipe, the agitator be connected with the motor, thermal exhaust pipe one end be connected the other end with the admission valve and be connected with spherical exhaust head, cauldron body surface face be provided with feed inlet, discharge gate, pneumatic valve, demulsifier charge door, the discharge gate on be provided with the ejection of compact and detect mouthful, agitator bottom be provided with anchor slab formula stirring leaf, the agitator in the middle of be connected with spiral stirring leaf.
Description
Technical field
This utility model is related to the preparation method of macromolecular material, specifically a kind of production high-impact transparence MBS tree
Prepared by the part of fat, especially the intensification charging dress in a kind of MBS production of resins in MBS production of resins used by breakdown of emulsion process
Put.
Background technology
Breakdown of emulsion link in existing equipment in MBS production of resins, adopts one-pot jacket type heating mode mostly, and breaks
To the form of MBS naval stores powders, granularity and apparent size, one-pot demulsification technology is most simply easiest to behaviour to newborn procedure relation
Make, but work disposal ability is less, and MBS resin particles form and size are not easily controlled, and are not suitable for large-scale production, but its
Investment it is less, although have the series connection of many kettle demulsification technologies but actually multiple one-pots, have an advantage in that its seriality, be easy to into
Row industrialization large-scale production, the form and apparent density that are disadvantageous in that MBS do not have the raising of essence, traditional breakdown of emulsion
Process materials and demulsifier be from kettle above into kettle in, then in the top discharging in middle part of reactor, this feeding manner
Next stage breakdown of emulsion kettle is entered by material gravity flow, process is simple is operated well, but material circulation time in kettle is short, stopped in kettle
1-2 minutes are put in next kettle, react insufficient, density after dry materials（0.32-0.35g/cm³）It is apparent low, it is badly in need of
A kind of emulsion breaking device can be realized increasing the time of staying of the material in kettle, realize continuous demulsification, improve product quality, improves reaction
Efficiency.
The content of the invention
The purpose of this utility model is to provide the intensification feed arrangement in a kind of MBS production of resins, and the device is using broken
The series connection of newborn kettle formed three-level breakdown of emulsion reach more preferable demulsification and meanwhile increase residence time of material, adapt to large-scale production and
Feed blocking is prevented, the utilization rate of energy is improved by adding heat exhaust tube realization to be rapidly heated, is shortened the production cycle, effectively saved
About cost is reduced and wasted.
The technical scheme in the invention for solving the technical problem is：A kind of intensification in MBS production of resins is entered
Material device, including one-level breakdown of emulsion kettle, two grades of breakdown of emulsion kettles, three-level breakdown of emulsion kettle, discharging opening, kettle, charging apertures, described one-level breakdown of emulsion
Kettle, two grades of breakdown of emulsion kettles, three-level breakdown of emulsion kettle construction are identical, and the discharging opening of described one-level breakdown of emulsion kettle enters with two grades of breakdown of emulsion kettles
Material mouth connects, and the discharging opening of two grades of described breakdown of emulsion kettles is connected with the charging aperture of three-level breakdown of emulsion kettle, and described kettle inside is arranged
Have agitator and a spiral plus heat exhaust tube, described agitator and motor connection, described plus heat exhaust tube one end with
Intake valve connection the other end be connected with spherical exhaust head, described kettle surface be provided with charging aperture, discharging opening, air pressure valve, break
Emulsion charge door, is provided with discharging detection mouth on described discharging opening, described stirrer bottom is provided with anchor plate type paddle,
It is connected with screw mixing leaf in the middle of described agitator.
Used as optimization, described charging aperture is arranged at autoclave body bottom, and described discharging opening is arranged at kettle top, breakdown of emulsion kettle
Bottom feed coordinates upper outlet to break off relations feed blocking problem, increases the time of staying in material breakdown of emulsion kettle, makes reaction more
Fully.
Used as optimization, described kettle is internally provided with heat-insulation layer and temperature-detecting device, described temperature-detecting device
It is electrically connected with intake valve, reduces heat losses, it is optimal anti-so as to realize while breakdown of emulsion temperature in the kettle can be controlled well
Answer effect.
Used as optimization, described one-level breakdown of emulsion kettle, two grades of breakdown of emulsion kettles, three-level breakdown of emulsion kettle design temperatures are respectively 40 DEG C ~ 50
DEG C, 60 DEG C ~ 70 DEG C, 85 DEG C ~ 95 DEG C, the purpose of one-level breakdown of emulsion is emulsion form material Jing and acid reaction, forms granule mixed with water
Compound, this is the also no complete molding of granule, and this phase temperature automatically flows into two at 40 DEG C ~ 50 DEG C after one-level breakdown of emulsion kettle material is full
Level breakdown of emulsion kettle, opens the stirring of two grades of breakdown of emulsion kettles, starts simultaneously at intensification, temperature control at 60 DEG C ~ 70 DEG C, this stage be in order that
Grain further molding, two grades of breakdown of emulsion kettle material completely automatically flow into three-level breakdown of emulsion kettle, while temperature brings up to 85 DEG C ~ 95 DEG C, and add
Suitable quantity of water, this stage is that in order that material particles ripening sizing, and makes granule be hardened, so far granule is completely separated from the water.
Used as optimization, the described heat exhaust tube surface that adds is provided with the irregular column type hole of axis direction, can not only be quick
The cycle that uniform lifting breakdown of emulsion temperature in the kettle shortens material production can also play certain mixing effect, while breakdown of emulsion itself
Need to add suitable quantity of water, steam to enter in kettle and change into the water for needing to add before water instead of.
Used as optimization, described described screw mixing leaf external diameter prevents destruction from adding less than the internal diameter for adding heat exhaust tube
Heat exhaust tube, while available plus heat exhaust tube cleaning agitator during equipment cleaning.
As optimization, be provided with described discharging detection mouth can folding form, material situation can easily be detected with
Just timely adjusting device.
As optimization, the controllable agitator main story of described motor and reversion, realize that preferably stirring contributes to what is reacted
Fully carry out.
The beneficial effects of the utility model are：Compared with prior art, in a kind of MBS production of resins of the present utility model
Intensification feed arrangement, forms three-level breakdown of emulsion and reaches more preferable demulsification while when increasing material stop using the series connection of breakdown of emulsion kettle
Between, adapt to large-scale production and prevent feed blocking, by plus heat exhaust tube realize be rapidly heated improve energy utilization rate, contracting
Short production cycle, has effectively saved cost and has reduced waste.
Description of the drawings
Fig. 1 is this utility model overall construction drawing；
Fig. 2 is this utility model breakdown of emulsion container mechanism figure；
Fig. 3 is this utility model agitator structure figure；
Wherein, 1 one-level breakdown of emulsion kettle, 2 two grades of breakdown of emulsion kettles, 3 three-level breakdown of emulsion kettles, 4 motors, 5 air pressure valves, 6 intake valves, 7 dischargings
Detection mouth, 8 discharging openings, 9 plus heat exhaust tube, 10 kettlies, 11 agitators, 12 charging apertures, 13 spherical exhaust heads, the charging of 14 demulsifiers
Mouth, 15 anchor plate type paddles, 16 screw mixing leaves.
Specific embodiment
As Figure 1-3 in embodiment, the intensification feed arrangement in a kind of MBS production of resins, including one-level breakdown of emulsion kettle 1,
Two grades of breakdown of emulsion kettles 2, three-level breakdown of emulsion kettle 3, discharging opening 8, kettle 10, charging apertures 12, it is characterised in that：Described one-level breakdown of emulsion kettle 1,
Two grades of breakdown of emulsion kettles 2, three-level breakdown of emulsion kettle 3 construct the discharging opening 8 of identical, described one-level breakdown of emulsion kettle 1 and two grades of breakdown of emulsion kettles 2
Charging aperture 12 connects, and the discharging opening 8 of two grades of described breakdown of emulsion kettles 2 is connected with the charging aperture 12 of three-level breakdown of emulsion kettle 3, described kettle
10 are internally provided with agitator 11 and spiral plus heat exhaust tube 9, and described agitator 11 is connected with motor 4, described
Plus the one end of heat exhaust tube 9 is connected the other end and is connected with spherical exhaust head 13 with intake valve 6, the described surface of kettle 10 be provided with into
Material mouth 12, discharging opening 8, air pressure valve 5, demulsifier charge door 14, are provided with discharging detection mouth 7 on described discharging opening 8, described
The bottom of agitator 11 is provided with anchor plate type paddle 15, is connected with screw mixing leaf 16 in the middle of described agitator 11.
Used as optimization, described charging aperture 12 is arranged at the bottom of kettle 10, and described discharging opening 8 is arranged on kettle 10
Portion, breakdown of emulsion kettle bottom feed coordinates upper outlet to break off relations feed blocking problem, increases the time of staying in material breakdown of emulsion kettle, makes
Reaction is more abundant.
Used as optimization, described kettle 10 is internally provided with heat-insulation layer and temperature-detecting device, described temperature detection dress
Put and be electrically connected with intake valve 6, reduce heat losses, while breakdown of emulsion temperature in the kettle can be well controlled, it is optimal so as to realize
Reaction effect.
As optimization, described 1, two grades of breakdown of emulsion kettles 2 of one-level breakdown of emulsion kettle, the design temperature of three-level breakdown of emulsion kettle 3 be respectively 40 DEG C ~
50 DEG C, 60 DEG C ~ 70 DEG C, 85 DEG C ~ 95 DEG C, the purpose of one-level breakdown of emulsion is emulsion form material Jing and acid reaction, forms granule with water
Mixture, this is the also no complete molding of granule, and this phase temperature is automatically flowed at 40 DEG C ~ 50 DEG C after one-level breakdown of emulsion kettle material is full
Two grades of breakdown of emulsion kettles, open the stirring of two grades of breakdown of emulsion kettles, start simultaneously at intensification, temperature control at 60 DEG C ~ 70 DEG C, this stage be in order that
The further molding of granule, two grades of breakdown of emulsion kettle material completely automatically flow into three-level breakdown of emulsion kettle, while temperature brings up to 85 DEG C ~ 95 DEG C, and add
Enter suitable quantity of water, this stage is that in order that material particles ripening sizing, and makes granule be hardened, so far granule is completely separated from the water.
Used as optimization, the described surface of heat exhaust tube 9 that adds is provided with the irregular column type hole of axis direction, can not only be quick
The cycle that uniform lifting breakdown of emulsion temperature in the kettle shortens material production can also play certain mixing effect, while breakdown of emulsion itself
Need to add suitable quantity of water, steam to enter in kettle and change into the water for needing to add before water instead of.
Used as optimization, the described described external diameter of screw mixing leaf 16 prevents destruction less than the internal diameter for adding heat exhaust tube 9
Plus heat exhaust tube, while available plus heat exhaust tube cleaning agitator during equipment cleaning.
As optimization, be provided with described discharging detection mouth 7 can folding form, material situation can easily be detected with
Just timely adjusting device.
Used as optimization, described motor 4 can control the main story of agitator 11 and reversion, realize that preferably stirring contributes to reaction
Fully carry out.
Compared with prior art, the intensification feed arrangement in a kind of MBS production of resins of the present utility model, using breakdown of emulsion kettle
Series connection form three-level breakdown of emulsion and reach more preferable demulsification while increasing residence time of material, adapting to large-scale production and prevent
Feed blocking, the utilization rate of energy is improved by adding heat exhaust tube realization to be rapidly heated, shortens the production cycle, effectively saving
Cost is reduced and wasted.
Above-mentioned specific embodiment is only concrete case of the present utility model, and scope of patent protection of the present utility model includes
But it is not limited to the product form and style of above-mentioned specific embodiment, any one kind for meeting this utility model claims
The appropriate change that intensification feed arrangement and any person of an ordinary skill in the technical field in MBS production of resins is done to it
Or modification, should all fall into scope of patent protection of the present utility model.
Claims (8)
1. a kind of intensification feed arrangement in MBS production of resins, including one-level breakdown of emulsion kettle（1）, two grades of breakdown of emulsion kettles（2）, three-level break
Newborn kettle（3）, discharging opening（8）, kettle（10）, charging aperture（12）, it is characterised in that：Described one-level breakdown of emulsion kettle（1）, two grades of breakdowns of emulsion
Kettle（2）, three-level breakdown of emulsion kettle（3）Identical, the described one-level breakdown of emulsion kettle of construction（1）Discharging opening（8）With two grades of breakdown of emulsion kettles（2）
Charging aperture（12）Connection, two grades of described breakdown of emulsion kettles（2）Discharging opening（8）With three-level breakdown of emulsion kettle（3）Charging aperture（12）Even
Connect, described kettle（10）It is internally provided with agitator（11）With spiral plus heat exhaust tube（9）, described agitator
（11）With motor（4）Connection, described adds heat exhaust tube（9）One end and intake valve（6）The connection other end and spherical exhaust head
（13）Connection, described kettle（10）Surface is provided with charging aperture（12）, discharging opening（8）, air pressure valve（5）, demulsifier charge door
（14）, described discharging opening（8）On be provided with discharging detection mouth（7）, described agitator（11）Bottom is provided with anchor plate type and stirs
Mix leaf（15）, described agitator（11）Middle and screw mixing leaf（16）Connection.
2. the intensification feed arrangement in a kind of MBS production of resins according to claim 1, it is characterised in that：Described enters
Material mouth（12）It is arranged at kettle（10）Bottom, described discharging opening（8）It is arranged at kettle（10）Top.
3. the intensification feed arrangement in a kind of MBS production of resins according to claim 1, it is characterised in that：Described kettle
Body（10）It is internally provided with heat-insulation layer and temperature-detecting device, described temperature-detecting device and intake valve（6）It is electrically connected with.
4. the intensification feed arrangement in a kind of MBS production of resins according to claim 3, it is characterised in that：Described one
Level breakdown of emulsion kettle（1）, two grades of breakdown of emulsion kettles（2）, three-level breakdown of emulsion kettle（3）Design temperature is respectively 40 DEG C ~ 50 DEG C, 60 DEG C ~ 70 DEG C, 85 DEG C
~95℃。
5. the intensification feed arrangement in a kind of MBS production of resins according to claim 1, it is characterised in that：Described adds
Heat exhaust tube（9）Surface is provided with the irregular column type hole of axis direction.
6. the intensification feed arrangement in a kind of MBS production of resins according to claim 1, it is characterised in that：Described institute
The screw mixing leaf stated（16）External diameter is less than plus heat exhaust tube（9）Internal diameter.
7. the intensification feed arrangement in a kind of MBS production of resins according to claim 1, it is characterised in that：Described goes out
Material detection mouth（7）On be provided with can folding form.
8. the intensification feed arrangement in a kind of MBS production of resins according to claim 1, it is characterised in that：Described electricity
Machine（4）Controllable agitator（11）Main story and reversion.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621088340.5U CN206168410U (en) | 2016-09-29 | 2016-09-29 | Intensification feed arrangement in production of MBS resin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621088340.5U CN206168410U (en) | 2016-09-29 | 2016-09-29 | Intensification feed arrangement in production of MBS resin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206168410U true CN206168410U (en) | 2017-05-17 |
Family
ID=58677048
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621088340.5U Active CN206168410U (en) | 2016-09-29 | 2016-09-29 | Intensification feed arrangement in production of MBS resin |
Country Status (1)
| Country | Link |
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| CN (1) | CN206168410U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108721946A (en) * | 2018-05-17 | 2018-11-02 | 新疆中泰新鑫化工科技股份有限公司 | Continuous demulsification method in chlorinated polyether resin production |
| CN111138018A (en) * | 2020-01-19 | 2020-05-12 | 上海天成环境保护有限公司 | Emulsion treatment method and system |
-
2016
- 2016-09-29 CN CN201621088340.5U patent/CN206168410U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108721946A (en) * | 2018-05-17 | 2018-11-02 | 新疆中泰新鑫化工科技股份有限公司 | Continuous demulsification method in chlorinated polyether resin production |
| CN111138018A (en) * | 2020-01-19 | 2020-05-12 | 上海天成环境保护有限公司 | Emulsion treatment method and system |
| CN111138018B (en) * | 2020-01-19 | 2022-08-12 | 上海天成环境保护有限公司 | Emulsion treatment method and system |
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