CN206168406U - Reaction device - Google Patents
Reaction device Download PDFInfo
- Publication number
- CN206168406U CN206168406U CN201621009678.7U CN201621009678U CN206168406U CN 206168406 U CN206168406 U CN 206168406U CN 201621009678 U CN201621009678 U CN 201621009678U CN 206168406 U CN206168406 U CN 206168406U
- Authority
- CN
- China
- Prior art keywords
- conduction oil
- filter
- reactor
- valve
- rectifying column
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 26
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 238000004062 sedimentation Methods 0.000 claims abstract description 10
- 230000007062 hydrolysis Effects 0.000 claims abstract description 9
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 9
- 238000005273 aeration Methods 0.000 claims abstract description 5
- 239000000706 filtrate Substances 0.000 claims description 18
- 239000002994 raw material Substances 0.000 claims description 14
- 239000000047 product Substances 0.000 claims description 12
- 239000010802 sludge Substances 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 10
- 230000020477 pH reduction Effects 0.000 claims description 6
- 230000000249 desinfective effect Effects 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims 1
- 239000002699 waste material Substances 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 239000012295 chemical reaction liquid Substances 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 238000004659 sterilization and disinfection Methods 0.000 abstract 1
- 238000011084 recovery Methods 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- -1 by filter Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model belongs to the chemical industry equipment field specifically is a reaction device, include the reactor that connects gradually through the pipeline, the filter, the rectifying column, the lye dissolving tank, hydrolysis -acidification pool, good oxygen pond, primary sedimentation basin, the anaerobism pond, the biological pond of aeration, sedimentation tank and contact disinfection pond, the outside of reactor is equipped with the one deck shell, input conduction oil in the space between shell and the reactor, the lower part of casing is equipped with the conduction oil entry, is equipped with the conduction oil inlet valve on the conduction oil entry, and the upper portion of casing is equipped with the conduction oil export, is equipped with the conduction oil outlet valve in the conduction oil export. Realized the rational utilization to reaction liquid through being equipped with separator and rectifying column, realized being favorable to doing benefit to the protection of environment to the processing of reaction waste liquid through being equipped with equipment such as lye dissolving tank and hydrolysis -acidification pool.
Description
Technical field
The utility model belongs to field of chemical equipment, specially a kind of reaction unit.
Background technology
At present, the use of reactor is all be unable to do without in numerous industrialized productions, existing reactor is to throw reactant
Enter in reactor and reacted, reaction carries out isolated product to reaction solution after terminating, the reaction solution extracted after product is a lot
In the case of all cannot get good recycle and reuse, often directly or indirectly discharge reach, so not only bad for the guarantor of environment
Shield, and resource suffers serious waste.
The content of the invention
In order to solve the above-mentioned technical problem, this application provides a kind of reaction unit.
The application is realized by following proposal：
A kind of reaction unit, including the reactor being sequentially connected by pipeline, filter, rectifying column, lye dissolving tank, hydrolysis acid
Change pond, Aerobic Pond, primary sedimentation basin, anaerobic pond, aeration and biological pond, sedimentation basin and disinfecting tank, the outside of reactor is provided with
Crust, is input into conduction oil in the space between shell and reactor, the bottom of housing is provided with heat conduction oil-in, and conduction oil enters
Mouth is provided with conduction oil inlet valve, and the top of housing is provided with conduction oil outlet, and conduction oil outlet is provided with conduction oil outlet valve.
Preferably, stirring motor is provided with the top of reactor, agitating shaft is provided with below stirring motor, agitating shaft is located at anti-
Answer device interior and straight down, agitating shaft is provided with stirring vane, and the top of reactor is provided with feed(raw material)inlet pipe, on the pipe of feed(raw material)inlet
Be provided with branch pipe, feed(raw material)inlet pipe is provided with inlet valve I and inlet valve II, inlet valve I and inlet valve II be located at feed(raw material)inlet pipe with
The both sides of branch pipe junction, the bottom of reactor is provided with product exit, and product exit is provided with outlet valve.
Preferably, branch pipe is provided with manifold valve, and branch pipe is connected with vacuum plant.
Preferably, the top of reactor is provided with visor, and reactor is provided with temperature testing device and pressure gauge.
Preferably, the top of filter is provided with filter inlet, and filter inlet wound is provided with filter inlet valve, the mistake
Filter is provided with filter, filter is 15-30 ° with the angle of horizontal plane, and filter is provided with sludge outlet, on sludge outlet
Sludge outlet valve is provided with, the bottom of filter is provided with filtrate (liquid, and filtrate (liquid is provided with filtrate (liquid valve.
Preferably, rectifying column feed pipe is provided with the middle part of rectifying column, rectifying column feed pipe is provided with rectifying column feed pipe valve,
The filtrate (liquid is connected with rectifying column feed pipe, and the rectifying column feed pipe in rectifying column is provided with more than one
Liquid distribution trough.
The principle of the application is：If the product that obtains of reaction is solid, by filter, solid product is from filter for reaction solution
Slag outlet is obtained, and filtrate reaches rectifying column and separated, and unreacted raw material is reclaimed in filtrate, remaining raffinate after recovery
Lye dissolving tank, hydrolysis acidification pool etc. is sequentially passed through to be processed；If the product that reaction is obtained is liquid, reaction solution is by filtering
Device is filtered, and the filter residue for obtaining carries out subsequent treatment, and filtrate reaches rectifying column and separated, according to each component boiling point in filtrate not
With recovery product and the reactant for reaction, remaining raffinate sequentially passes through lye dissolving tank, hydrolysis acidification pool etc. and is located after recovery
Reason.
Some reaction need under gaseous state react, the setting of vacuum plant can reduce such reaction needed for temperature
Degree.
The beneficial effects of the utility model are：By being provided with separator and rectifying column realizes reasonable profit to reaction solution
With, treatment to waste reaction solution is realized by being provided with the equipment such as lye dissolving tank and hydrolysis acidification pool, be conducive to the guarantor beneficial to environment
Shield.
Brief description of the drawings
Fig. 1 is the utility model structural representation；
Fig. 2 is structure of reactor schematic diagram；
Fig. 3 is filter structure schematic representation；
Fig. 4 is rectifying tower structure schematic diagram；
In figure, 1, reactor, 2, filter, 3, rectifying column, 4, lye dissolving tank, 5, hydrolysis acidification pool, 6, Aerobic Pond, 7, once
Sedimentation basin, 8, anaerobic pond, 9, aeration and biological pond, 10, sedimentation basin, 11, disinfecting tank, 12, housing, 13, inlet valve I, 14, branch
Pipe, 15, manifold valve, 16, inlet valve II, 17, feed(raw material)inlet pipe, 18, stirring motor, 19, rotating shaft, 20, pressure gauge, 21, temperature
Test device, 22, visor, 23, conduction oil outlet valve, 24, conduction oil outlet, 25, outlet valve, 26, product exit, 27, heat conduction
Oil-in, 28, conduction oil inlet valve, 29, stirring vane, 30, filter inlet, 31, filter inlet valve, 32, filter,
33rd, sludge outlet, 34, sludge outlet valve, 35, filtrate (liquid, 36, filtrate (liquid valve, 37, rectifying column enter pipe, 38, rectifying column enters
Expects pipe valve, 39, distributor, 40 vacuum plants.
Specific embodiment
Embodiment
A kind of reactor, including the reactor 1 being sequentially connected by pipeline, filter 2, rectifying column 3, lye dissolving tank 4, hydrolysis
Acidification pool 5, Aerobic Pond 6, primary sedimentation basin 7, anaerobic pond 8, aeration and biological pond 9, sedimentation basin 10 and disinfecting tank 11, reactor
1 outside is provided with crust 12, and conduction oil is input into the space between shell 12 and reactor 1, and the bottom of housing 1 is provided with leads
Deep fat entrance 27 and conduction oil inlet valve 28, the top of housing are provided with conduction oil outlet 24, and conduction oil outlet 24 is provided with heat conduction
Oil export valve 23, the top of reactor 1 is provided with stirring motor 18, and the lower section of stirring motor 18 is provided with agitating shaft 19, agitating shaft 19
In reactor 1 and straight down, agitating shaft 19 is provided with stirring vane 29, and the top of reactor 1 is provided with feed(raw material)inlet pipe
17, feed(raw material)inlet pipe 17 is provided with branch pipe 14, and feed(raw material)inlet pipe 17 is provided with inlet valve I 13 and inlet valve II 16, inlet valve I 13
With inlet valve II 16 positioned at the both sides of feed(raw material)inlet pipe 17 with the junction of branch pipe 14, the bottom of reactor 1 is provided with product exit 26,
Product exit 26 is provided with outlet valve 25, and branch pipe 14 is provided with manifold valve 15, and branch pipe 14 is connected with vacuum plant 40, reactor
1 top is provided with visor 22, and reactor 1 is provided with temperature testing device 21 and pressure gauge 20, and the top of filter 2 is provided with filtering
Device entrance 30, filter inlet 30 is provided with filter inlet valve 31, and filter, filter and horizontal plane are provided with filter
Angle is 25 °, and filter 2 is provided with sludge outlet 33, and sludge outlet 33 is provided with sludge outlet valve 31, the bottom of filter 2
Filtrate (liquid 35 is provided with, filtrate (liquid 35 is provided with filtrate (liquid valve 36, and the middle part of rectifying column 3 is provided with rectifying column feed pipe 37,
Rectifying column feed pipe 37 is provided with rectifying column and enters pipe valve 38, and the filtrate (liquid 35 is connected with rectifying column feed pipe 37, is located at
In rectifying column 3 more than one liquid distribution trough 39 is provided with positioned at rectifying column feed pipe 37.
Claims (6)
1. a kind of reaction unit, it is characterised in that including the reactor being sequentially connected by pipeline, filter, rectifying column, molten alkali
Groove, hydrolysis acidification pool, Aerobic Pond, primary sedimentation basin, anaerobic pond, aeration and biological pond, sedimentation basin and disinfecting tank, reactor
Outside is provided with crust, and conduction oil is input into the space between shell and reactor, and the bottom of housing is provided with heat conduction oil-in,
Heat conduction oil-in is provided with conduction oil inlet valve, and the top of housing is provided with conduction oil outlet, and conduction oil outlet is provided with conduction oil
Outlet valve.
2. a kind of reaction unit as claimed in claim 1, it is characterised in that be provided with stirring motor at the top of the reactor,
Agitating shaft is provided with below stirring motor, agitating shaft is located in reactor body and straight down, agitating shaft is provided with paddle
Piece, the top of reactor is provided with feed(raw material)inlet pipe, and feed(raw material)inlet pipe is provided with branch pipe, and feed(raw material)inlet pipe is provided with the He of inlet valve I
Inlet valve II, inlet valve I and inlet valve II are located at the both sides of feed(raw material)inlet pipe and branch pipe junction respectively, and the bottom of reactor sets
There is product exit, product exit is provided with outlet valve.
3. a kind of reaction unit as claimed in claim 2, it is characterised in that the branch pipe is provided with manifold valve, branch pipe with it is true
Empty device is connected.
4. a kind of reaction unit as claimed in claim 1, it is characterised in that the top of the reactor is provided with visor, reaction
Device is provided with temperature testing device and pressure gauge.
5. a kind of reaction unit as claimed in claim 1, it is characterised in that the top of the filter is provided with filter and enters
Mouthful, filter inlet wound is provided with filter inlet valve, and filter is provided with the filter, and filter is with the angle of horizontal plane
15-30 °, filter is provided with sludge outlet, and sludge outlet is provided with sludge outlet valve, and the bottom of filter is provided with filtrate and goes out
Mouthful, filtrate (liquid is provided with filtrate (liquid valve.
6. a kind of reaction unit as claimed in claim 5, it is characterised in that rectifying column charging is provided with the middle part of the rectifying column
Pipe, rectifying column feed pipe is provided with rectifying column feed pipe valve, and the filtrate (liquid is connected with rectifying column feed pipe, positioned at rectifying
Rectifying column feed pipe in tower is provided with more than one liquid distribution trough.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621009678.7U CN206168406U (en) | 2016-08-31 | 2016-08-31 | Reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621009678.7U CN206168406U (en) | 2016-08-31 | 2016-08-31 | Reaction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206168406U true CN206168406U (en) | 2017-05-17 |
Family
ID=58674898
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621009678.7U Expired - Fee Related CN206168406U (en) | 2016-08-31 | 2016-08-31 | Reaction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206168406U (en) |
-
2016
- 2016-08-31 CN CN201621009678.7U patent/CN206168406U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170517 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |