CN206143154U - A device for being directed at fragrant flavor material of flower any of several hot spice plants oil is retrieved - Google Patents

A device for being directed at fragrant flavor material of flower any of several hot spice plants oil is retrieved Download PDF

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Publication number
CN206143154U
CN206143154U CN201620705782.3U CN201620705782U CN206143154U CN 206143154 U CN206143154 U CN 206143154U CN 201620705782 U CN201620705782 U CN 201620705782U CN 206143154 U CN206143154 U CN 206143154U
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China
Prior art keywords
oil
delivery chute
thread mixing
drainer
pericarpium zanthoxyli
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CN201620705782.3U
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Chinese (zh)
Inventor
陈吉江
安骏
陈刚
陈玉军
王立艳
丁庆波
王冶
钟鸣
李居南
杨学昊
黄珍
黄一珍
杨凯
苏晓霞
朱镜曦
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Cofco Food Sales & Distribution Co Ltd
Cofco Corp
Cofco Nutrition and Health Research Institute Co Ltd
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Cofco Food Sales & Distribution Co Ltd
Cofco Corp
Cofco Nutrition and Health Research Institute Co Ltd
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Priority to CN201620705782.3U priority Critical patent/CN206143154U/en
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Abstract

The utility model provides a device for being directed at fragrant flavor material of flower any of several hot spice plants oil is retrieved, the device includes: motor, spiral blending transportation groove, nonrust steel cage and drainer, spiral blending transportation inclines in the groove inclined and puts, it is inside have the accessible along with the parallel rotation axis in spiral blending transportation groove rotate and with the material to lifting auger delivery ware (2) sent, and by motor (1) drive auger delivery ware (2) make it wind axis of rotation, nonrust steel cage (6) install in spiral blending transportation groove top for the collection prepare flower any of several hot spice plants when oil produced vapor with the prickly ash fragrance essential oil composition of thereupon overflowing and transport extremely the drainer.

Description

For the device reclaimed to fresh zanthoxylum oil fragrance flavor substance
Technical field
This utility model is related to the recovery of fresh zanthoxylum oil fragrance flavor substance, is used for fresh pepper in particular to a kind of The device that oily fragrance flavor substance is reclaimed, belongs to food production field.
Background technology
Pericarpium Zanthoxyli is mainly used as foodstuff flavouring spice in China, there is long edible history, is the seasoning that people like One of product, at home sphere of consumption is very wide, and processing stage is mainly sold than relatively low in the form of granulate and coarse powder.In general day When often used in life, Pericarpium Zanthoxyli or Zanthoxyli Bungeani powder are mainly directly added into, but for the food enterprises, are directly added into mode Often the exterior beauty of produced product can be affected, therefore there are many food production processing enterprises to start to use aborning at present Aromatic oil from Chinese pepper replaces Pericarpium Zanthoxyli to make flavoring agent.
Not through drying or drying, the fragrance ingredient in Pericarpium Zanthoxyli retains intact to fresh pepper, and with fresh pepper Fructus Zanthoxyli oil is produced, The fragrant of Pericarpium Zanthoxyli is pure strong, not exclusively strong numb taste, also with delicate fragrance, pure Pericarpium Zanthoxyli aromatic odor.In addition, flower Chlorophyll in green pepper is the natural pigment that photosynthesis are produced, and is fat-soluble pigment, in process the chlorophyll in Pericarpium Zanthoxyli In dissolving in edible oil, so that the Fructus Zanthoxyli oil produced is in the dark green of natural fresh Zanthoxylum schinifolium, outward appearance is good.Therefore, fresh zanthoxylum oil Increasingly paid close attention to by people.
Oil soluble method is the traditional method for producing Fructus Zanthoxyli oil, is used by domestic overwhelming majority Fructus Zanthoxyli oil factory, and its way is:Will Pericarpium Zanthoxyli is directly placed in the edible vegetable oil of heat and seals, or Pericarpium Zanthoxyli is contained in container of the aperture less than Pericarpium Zanthoxyli diameter, The edible vegetable oil of heat is drenched in container slowly, its fragrance is blasted, effective ingredient is dissolved in oil, obtain final product Fructus Zanthoxyli oil.Generally During using oil soluble method processing fresh green zanthoxylum oil, Pericarpium Zanthoxyli fragrance ingredient (such as limonene, linalool, pyridoxol) with plus The vapor produced during work is discharged in environment by high-power air exhauster so that high added value, fragrant with natural Pericarpium Zanthoxyli The composition of fragrance volatilizees away in company with steam, causes product composition to lose and environmental pollution.
Utility model content
For the problems referred to above, this utility model provides one kind while Fructus Zanthoxyli oil is normally prepared, can be to fresh zanthoxylum oil The method that fragrant flavor substance is reclaimed.This utility model also provides the device for the recovery method.
It is described in the utility model that the method that fresh zanthoxylum oil fragrance flavor substance is reclaimed is comprised the following steps:
(1) the fresh Zanthoxylum schinifolium of raw material is prepared;
(2) the fresh Zanthoxylum schinifolium of step (1) is extracted with edible vegetable oil, obtains extraction Fructus Zanthoxyli oil;
(3) vapor produced in step (2) and the volatile oil for escaping therewith are collected;
(4) mixture rapid condensation collected in step (3) is made, condensing mixt is obtained;And
(5) condensing mixt to obtaining in step (4) carries out oil-water separation, collects oil phase product.
Preferably, in method of the present utility model, the step (1) is including following operation:
Fresh Zanthoxylum schinifolium is plucked, the fresh Zanthoxylum schinifolium is used to process fresh zanthoxylum oil in 24h;
The fresh Zanthoxylum schinifolium is selected, is removed and is gone rotten fruit and carry out spray washing;
With the residual moisture that fan blows away fresh Zanthoxylum schinifolium surface, subsequently fresh Zanthoxylum schinifolium surface residual is removed by hot-air seasoning Moisture.
Preferably, in method of the present utility model, the step (2) includes:
From the fresh Zanthoxylum schinifolium that the low side input step (1) of thread mixing delivery chute is obtained, and it is made with high-end input 100-200 DEG C of edible vegetable oil carries out adverse current mixing and is extracted, and extraction time is 5-10min.
Preferably, in method of the present utility model, the step (3) includes:
Stainless steel cage is installed at the top 10-30cm of step (2) the thread mixing delivery chute, above stainless steel cage Industrial exhaust fan is installed, the power of the industrial exhaust fan preferably >=3KW, so as to pass through the industrial exhaust fan by spiral shell The top of rotation blending transportation groove is extracted in the vapor and volatilization oil vapour suction drainer produced during fresh Zanthoxylum schinifolium.
Preferably, in method of the present utility model, the step (4) includes:
It is passed through condensed water in the interlayer of drainer, preferably 0 DEG C frozen water, so as to the vapor collected of step (3) and wave Hair oil steam generation rapid condensation, forms mixing liquid and flow to the condensation pot bottom, obtains the condensing mixt.
Preferably, in method of the present utility model, the step (5) includes:
The condensing mixt is stood into 18-24 hours, until lower floor's water phase is clearly layered with volatile oil, discard it is described under Layer water phase, obtains the oil water mixture based on upper oil phase;Subsequently, further by disc separator to the oil mixing with water Thing carries out oil-water separation, obtains oil-soluble fresh zanthoxylum oil fragrance flavor substance.
In a preferred embodiment, the edible oil is Semen Maydis oil, Oleum Brassicae campestriss and/or soybean oil.
On the other hand, this utility model additionally provides the fresh zanthoxylum oil virtue prepared by method described in the utility model Flavor material.
This utility model is further related to by the way that fresh zanthoxylum oil of the present utility model fragrance flavor substance time is added into into extraction flower The Fructus Zanthoxyli oil prepared in green pepper oil.
On the other hand, this utility model is additionally provided for the device of this utility model method, in preferred embodiment party In formula, described device includes:Motor, thread mixing delivery chute, stainless steel cage and drainer, wherein:
The thread mixing delivery chute slant setting, it is internal, and have can be by along flat with the thread mixing delivery chute The auger conveyor 2 that capable rotary shaft is rotated and upwards submits material, and the spiral transferring is driven by the motor 1 Device 2 is sent it is rotated around the rotary shaft;The stainless steel cage 6 is installed on the thread mixing delivery chute top, for collecting Produced vapor and the Pericarpium Zanthoxyli volatile oil composition for escaping therewith and the drainer is delivered to when producing fresh zanthoxylum oil.
Used as preferred embodiment, the rotation of the auger conveyor 2 is pivotally connected to the motor 1;It is described The top of thread mixing delivery chute is provided with edible oil-in 4, bottom and is provided with fresh pepper fruit entrance 3 and fresh zanthoxylum oil outlet 5.
As preferred embodiment, the stainless steel cage (6) is internal industrial exhaust fan (7) is housed and institute is connected to State the pipeline of drainer.
Used as preferred embodiment, the drainer has side wall interlayer, and the side wall interlayer is opened respectively in top and the bottom If the entrance 8 come in and gone out for condensed water and outlet 9;And the condensation pot bottom is opened up and derive successively bottom aqueous phase layer and Pericarpium Zanthoxyli The outlet 13 of volatile oil.
Used as preferred embodiment, the stainless steel cage is installed on the top 10-30cm of the thread mixing delivery chute Place.
As preferred embodiment, the power >=3KW of the industrial exhaust fan.
As preferred embodiment, the thread mixing delivery chute slant setting, it is internal have can by along with The auger conveyor 2 that the parallel rotary shaft of the thread mixing delivery chute is rotated and upwards submits material;The spiral The rotation of carrier is pivotally connected to the motor 1 and is rotated by the motor running;The thread mixing groove Top is provided with edible oil-in 4, bottom and is provided with fresh pepper fruit entrance 3 and fresh zanthoxylum oil outlet 5;The stainless steel cage 6 is installed on At the 10-30cm of thread mixing delivery chute top, the Pericarpium Zanthoxyli volatile oil composition 12 for escaping to vapor and therewith enters Row is collected, and the stainless steel cage inside is equipped with the industrial exhaust fan 7 of power >=3KW and is connected to the pipe of the drainer Road;The drainer has a side wall interlayer, and the side wall interlayer opens up respectively the entrance 8 that comes in and goes out for condensed water and goes out in top and the bottom Mouth 9;The condensation pot bottom opens up the outlet 13 that can successively derive bottom aqueous phase layer 11 and Pericarpium Zanthoxyli volatile oil 10.
Method and apparatus of the present utility model is taken and reclaims principle with conventional condensation, with equipment investment it is little, income is big, The features such as environmental friendliness.By method and apparatus of the present utility model, the fresh zanthoxylum oil aromatic oxy of high product added value can be obtained Taste material (after its condensation alternatively referred to as " Pericarpium Zanthoxyli volatile oil "), the flavor substance can be returned allotment, the mark for interpolating row Fructus Zanthoxyli oil Standardization, especially increases the pure QINGXIANG taste of fresh Zanthoxylum schinifolium, and it is not enough to make up numb taste, also or can use it for cosmetics, flavoring agent etc. Other purposes, realize waste reclaimation, produce economic benefit.The flavor substances reclaimed by method and apparatus of the present utility model The fresh zanthoxylum oil that matter Hui Tian is produced, its fragrance is full, rich in nutrition content, and rich in chlorophyll, color and luster is in natural dark green, is had There is the strong QINGXIANG taste of Zanthoxylum schinifolium, mouthfeel is soft, numb taste is pure.
Description of the drawings
Fig. 1 is the process chart of method of the present utility model.
Fig. 2 is the schematic diagram of device of the present utility model.
Fig. 3 shows an embodiment of the thread mixing delivery chute used in device of the present utility model.
Fig. 4 shows that the structure of the disc separator used in device of the present utility model and operation logic are illustrated Figure.
Wherein, each label is represented respectively:1 motor;2 auger conveyors;3 fresh pepper fruit entrances;4 edible oil-ins;5 is fresh Fructus Zanthoxyli oil outlet;6 stainless steel cages;7 industrial exhaust fans;8 condensing water inlets;9 condensation-water drains;10 Pericarpium Zanthoxyli volatile oil; 11 lower floor's aqueous layers;12 water vapour and Pericarpium Zanthoxyli fragrance volatilization mixture;13 lower floor's aqueous layers and Pericarpium Zanthoxyli volatile oil floss hole.
Specific embodiment
When producing fresh green zanthoxylum oil using immersion method, 100-200 DEG C of edible vegetable oil will be heated to from thread mixing The high-end injection of delivery chute, low side output;Fresh Zanthoxylum schinifolium be transported to from the low side of thread mixing delivery chute it is high-end, by high-end row Go out.
Because the fresh Zanthoxylum schinifolium for just having picked contains about 70% or so moisture, the food plant oil immersion of Jing 100-200 DEG C Process is put forward, the large quantity of moisture and part volatile oil in fresh Zanthoxylum schinifolium is opened in the way of steam (containing volatile oil and vapor) from top Discharge at mouthful, simultaneously containing substantial amounts of water solublity and oil-soluble Pericarpium Zanthoxyli fragrance ingredient (as limonene, linalool, pyrrole are trembled in steam Alcohol etc.).This utility model is to be arrived volatile oil (containing Pericarpium Zanthoxyli fragrance flavor substance) and water vapour extracting using industrial exhaust fan In the drainer of one customization, rapidly volatile oil and vapor steam are carried out into cooling and be condensed into liquid, due to condensed water and waving Hair oil (containing Pericarpium Zanthoxyli fragrance ingredient quintessence oil) between density variation, Jing natural subsidence for a period of time after profit layering, condensed water Density is big, is deposited in pot bottom bottom, floats over upper strata on the oil density that volatilizees light (quintessence oil containing Pericarpium Zanthoxyli fragrance ingredient), bottom of draining After condensed water, upper strata Pericarpium Zanthoxyli volatile oil is obtained.
In device of the present utility model, it is preferred to use single-pipe screw conveyer is conveyed to fresh Zanthoxylum schinifolium so as to food Extracted with oil contact.The structure of single-pipe screw conveyer is as shown in figure 3, it has simple structure, reliable, failure Rate is low, easy to maintenance, low cost the characteristics of, being especially suitable for conveying fresh Zanthoxylum schinifolium makes it be fully contacted with edible oil adverse current, realizes Excellent extracting effect.Because in this utility model, single-pipe screw conveyer is constantly in during fresh zanthoxylum oil is produced The condition of high temperature, therefore each part such as main shaft, housing, the spiral conveying blade of single-pipe screw conveyer added using stainless steel material Work.
Disc separator is also referred to as disk centrifuge, is a kind of efficiency high, the equipment that yield is big, automatization is advanced.Dish Sheet type separator has become a kind of centrifugation machinery being most widely used in current countries in the world oil and fat refining, is adapted to containing solid The less immiscible liquid of the relatively low suspension of the scale of construction, difference in specific gravity is separated.The principle of disc separator is according to centrifugation Power makes the material stress of different specific weight different, so as to reach detached purpose.Because suspension one is separated, light phase and heavy phase is just No longer contact, it is to avoid the impact that mixes once again.As shown in figure 4, motor does height by heating power coupled driving rotary drum around main shaft Speed revolution, feed liquid flow to bottom of the drum by central upper portion feed pipe, and the tap hole of seat surface tends to rotatory drum wall under Jing video discs, in centrifugation Under power effect, sink than the solid phase of liquid weight and form sediment, the lighter liquid phase of proportion (referred to as " light liquid ") Jing light liquids to drum inner wall Centripetal pump is discharged by light liquid outlet, and the heavier liquid phase of proportion (being accordingly referred to as " heavy-fluid ") tends to drum wall along video disc inner conical surface, then Flow up through heavy-fluid centripetal pump to be discharged by heavy liquid exit, separate with light liquid so as to complete heavy-fluid.
The edible vegetable oil that this utility model is adopted can be such as Semen Maydis oil, soybean oil, Oleum Brassicae campestriss or olive oil, or Any mixture of the above-mentioned edible vegetable oil of person.Examine in terms of odor impact from Pericarpium Zanthoxyli fragrance, numb taste and vegetable oil itself etc. Consider, preferred one-level Semen Maydis oil, one-level Oleum Brassicae campestriss, more preferably one-level Oleum Brassicae campestriss.
This utility model is conducted further description below by way of specific embodiment, institute in this utility model embodiment The test method for using if no special instructions, is conventional method;Raw material, reagent for being used etc., if no special instructions, are Can be from the raw material obtained by the routinely commercial sources such as commercial and reagent.
Embodiment
Such as illustrate without other, the raw material and equipment for being used in the examples below is listed below:Fresh Zanthoxylum schinifolium (the 7-8 months Part is plucked from Sichuan Province Ziyang City Yuezhi County, the Zanthoxylum schinifolium demonstration plant base of handsome green zanthoxylum oil factory), one-level Oleum Brassicae campestriss/Semen Maydiss Oil (good fortune near the house brand);
Single-pipe screw conveyer:Spiral nominal diameter 63cm, pitch 45cm, rotating speed 20r/min, conveying capacity 60m3/ h, shell Body overall length 1200cm;
Disc separator:Join pharmaceutical machine, model in Liaoyang:DHC500
The fresh zanthoxylum oil of embodiment 1 is prepared and fragrant flavor substance retracting device
Being used for the device that prepared by fresh zanthoxylum oil and fragrant flavor substance is reclaimed described in the present embodiment includes:Motor, spiral Blending transportation groove, stainless steel cage and drainer, wherein:
The thread mixing delivery chute slant setting, it is internal, and have can be by along flat with the thread mixing delivery chute The auger conveyor 2 that capable axle is rotated and upwards submits material;The rotation of the auger conveyor is pivotally connected to described Motor 1 is simultaneously rotated by the motor running;The top of the thread mixing groove is provided with edible oil-in 4, bottom It is provided with fresh pepper fruit entrance 3 and fresh zanthoxylum oil outlet 5;The stainless steel cage 6 is installed on the thread mixing delivery chute top, uses It is collected in the Pericarpium Zanthoxyli volatile oil composition for escaping to vapor and therewith, the stainless steel cage inside has industrial pumping Fan 7 and be connected to the pipeline of the drainer;The drainer has side wall interlayer, and the interlayer is opened up respectively in top and the bottom The entrance 8 come in and gone out for condensed water and outlet 9;The condensation pot bottom is opened up for deriving bottom aqueous phase layer 11 and Pericarpium Zanthoxyli successively The outlet 13 of volatile oil 10.
Embodiment 2
The fresh zanthoxylum oil fragrance flavor substance for carrying out the present embodiment using the device of embodiment 1 is reclaimed.The side of the present embodiment Method concrete steps include:
(1) fresh Zanthoxylum schinifolium is plucked, it is desirable to plucked in the case of fine day, is plucked when preferably having sunlight, never overcast and rainy Or band dew is plucked, the fresh Zanthoxylum schinifolium after harvesting is processed in 24h for Fructus Zanthoxyli oil, to ensure the color and luster and pure wind of Fructus Zanthoxyli oil Taste;
(2) fresh Zanthoxylum schinifolium removes the fruit that goes rotten, then Jing spray washings except spot, the dust on fresh Zanthoxylum schinifolium surface through selecting Deng impurity;Subsequently the moisture of fresh Zanthoxylum schinifolium remained on surface is blown off in order to fresh blue and white using industrial powerful fan (power 3KW) The oil immersion of green pepper is carried;Then the fresh Zanthoxylum schinifolium surface most of moisture of short time hot-air seasoning, cleaned, dry after fresh Zanthoxylum schinifolium Produce for Fructus Zanthoxyli oil;
(3) the fresh Zanthoxylum schinifolium from after low side input cleaning, the drying of thread mixing delivery chute, with the 100 of high-end input DEG C one-level Oleum Brassicae campestriss carry out adverse current mixing, Zanthoxylum schinifolium is 1 with the mass ratio of one-level Oleum Brassicae campestriss:2, extraction time is 10min, ginseng See example 3 below -4, extraction temperature, time are suitably adjusted, can correspondingly to the perfume (or spice) of resulting fresh green zanthoxylum oil The impact that taste, numb taste degree and color and luster are produced is studied.Fructus Zanthoxyli oil is kept in from the low side output suction of thread mixing delivery chute Tank, is cooled to after room temperature and is passed through Fructus Zanthoxyli oil holding vessel storage 5 days or so, extracts upper strata 3 layers of cloth bag mistake of limpid 200 mesh of Fructus Zanthoxyli oil Jing Filter, Jing plate and frames filter is filtrated to get the Fructus Zanthoxyli oil of clear with after;
(4) stainless steel cage is installed at the about 15cm of the top of thread mixing delivery chute, is provided with above stainless steel cage The industrial exhaust fan of power 3KW, for collecting the surface that thread mixing delivery chute is resulted from when fresh Zanthoxylum schinifolium is extracted A large amount of vapor and volatilization oil vapour, will be condensed into liquid and further cool down in its suction drainer;
(5) 0 DEG C of frozen water is passed through in the interlayer of drainer, so as to form mixed after vapor and volatilization oil vapour rapid condensation Liquid flow is closed to condensation pot bottom;
(6) due to volatile oil, condensed water density variation, condensed water is in tank bottoms layer, and volatile oil (Pericarpium Zanthoxyli volatile oil) exists Upper strata lower section;24 hours natural subsidence of Jing, condensed water is clearly layered with volatile oil, bleeds off after bottom condensed water to water and fragrance essence Oil is separated, and obtains thick Pericarpium Zanthoxyli volatile oil;
(7) thick volatile oil is further separated by decanter type disc separator, obtains Pericarpium Zanthoxyli volatile oil;Further Ground, subsequently returning to insert in the Fructus Zanthoxyli oil that step (3) is produced by the Pericarpium Zanthoxyli volatile oil of gained carries out perfumery.
The Fructus Zanthoxyli oil fragrance that embodiment 2 is produced is strong, moderate in dark green, numb taste;Pericarpium Zanthoxyli volatile oil quality and outward appearance It is stable.In the present embodiment, for the fresh Zanthoxylum schinifolium of every 100kg, using 200kg Oleum Brassicae campestriss, 100 DEG C of Jing, 10min extraction can Collect about 2.8kg Pericarpium Zanthoxyli volatile oil, Jing high effective liquid chromatography for measuring, its Pericarpium Zanthoxyli main flavor component content is, limonene 5.3wt%, linalool 18.1wt%;The Pericarpium Zanthoxyli volatile oil fragrant of acquisition is long, numb lightly seasoned.
Embodiment 3
The fresh zanthoxylum oil fragrance flavor substance for carrying out the present embodiment using the method for embodiment 2 is reclaimed and Fructus Zanthoxyli oil is adjusted Perfume (or spice), difference is:In step (3), the Semen Allii Tuberosi oil temperature for being used is 150 DEG C, and Pericarpium Zanthoxyli is extracted with Oleum Brassicae campestriss Time is 8min.
The Fructus Zanthoxyli oil fragrance that embodiment 3 is produced is fine, moderate in yellow green, numb taste, but then poor compared with Example 2. This is primarily due to as oil temperature is improved, the perfume (or spice), leprosy although extracting efficiency has been lifted, but under high oil temperature, in Pericarpium Zanthoxyli The volatilization of taste material composition is more, and chlorophyll is destroyed under high-temperature condition, affects product color.
In the present embodiment, for the fresh Zanthoxylum schinifolium of every 100kg, using 200kg Oleum Brassicae campestriss, 150 DEG C of Jing, 8min extraction can Collect about 3.4kg Pericarpium Zanthoxyli volatile oil, Jing high effective liquid chromatography for measuring, its main flavor component content is, limonene 4.1wt%, linalool 14.3wt%;The Pericarpium Zanthoxyli volatile oil fragrant of acquisition is pure, numb taste is denseer compared with Example 2.
It can be seen from the result of the present embodiment, the temperature of extraction Oleum Brassicae campestriss is higher, and the aromatic substance volatilized by Pericarpium Zanthoxyli is got over Many, the Pericarpium Zanthoxyli volatile oil collected is also more;The amount that amide-type spicy components in Pericarpium Zanthoxyli are evaporated increases, therefore numb taste Strengthen.
Embodiment 4
The fresh zanthoxylum oil fragrance flavor substance for carrying out the present embodiment using the method for embodiment 2 is reclaimed and Fructus Zanthoxyli oil is adjusted Perfume (or spice), difference is:In step (3), the Semen Allii Tuberosi oil temperature for being used is 200 DEG C, and Pericarpium Zanthoxyli is extracted with Oleum Brassicae campestriss Time is 5min.
The Fructus Zanthoxyli oil QINGXIANG gas that embodiment 4 is produced is thin out, moderate in yellow (without dark green), numb taste, with embodiment 1 and reality Applying the Fructus Zanthoxyli oil that example 2 produces, to compare quality worse.This is primarily due to, 200 DEG C of high oil temperatures, although extracting efficiency is lifted, but Under too high oil temperature, the perfume (or spice), leprosy taste material composition in Pericarpium Zanthoxyli volatilizees in a large number, and in the case of too high oil temperature, chlorophyll is subject to Heavy damage, affects product color.
In the present embodiment, for the fresh Zanthoxylum schinifolium of every 100kg, using 200kg Oleum Brassicae campestriss, 200 DEG C of Jing, 5min extraction can Collect about 3.8kg Pericarpium Zanthoxyli volatile oil, Jing high effective liquid chromatography for measuring, its main flavor component content is, limonene 3.5%th, linalool 12%;The Pericarpium Zanthoxyli volatile oil fragrant of acquisition is entrained with stir-baked PERICARPIUM ZANTHOXYLI fragrant not as good as embodiment 2 and embodiment 3 Gas;Numb taste is compared slightly dense with embodiment 2 with embodiment 3.It can be seen from the result of the present embodiment, extraction Semen Allii Tuberosi oil temperature enters one Step is raised, and the aromatic substance volatilized by Pericarpium Zanthoxyli further increases, and the Pericarpium Zanthoxyli volatile oil collected also increases;Amide in Pericarpium Zanthoxyli The amount that class spicy components are evaporated increases, therefore numb taste is further enhanced.
In the present embodiment, when oil temperature is up to 200 DEG C, the fresh Zanthoxylum schinifolium oil immersion time can not be long, and otherwise Pericarpium Zanthoxyli can occur It is charred, causes the Fructus Zanthoxyli oil produced to be charred taste;In the case where extraction time is less than 5min, the Fructus Zanthoxyli oil for being obtained has Light stir-baked PERICARPIUM ZANTHOXYLI fragrance.

Claims (8)

1. a kind of for the fresh zanthoxylum oil fragrance device that reclaimed of flavor substance, described device to include:Motor, spiral are mixed Close delivery chute, stainless steel cage and drainer, it is characterised in that:
The thread mixing delivery chute slant setting, it is internal, and have can be by along parallel with the thread mixing delivery chute The auger conveyor (2) that rotary shaft is rotated and upwards submits material, and the spiral transferring is driven by the motor (1) Device (2) is sent it is rotated around the rotary shaft;The stainless steel cage (6) is installed on the thread mixing delivery chute top, is used for Produced vapor when producing fresh zanthoxylum oil of collection and the Pericarpium Zanthoxyli volatile oil composition for escaping therewith are simultaneously delivered to the condensation Tank.
2. device as claimed in claim 1, it is characterised in that the rotation of the auger conveyor (2) is pivotally connected to institute State motor (1);The top of the thread mixing delivery chute is provided with edible oil-in (4), bottom and is provided with fresh pepper fruit entrance (3) (5) are exported with fresh zanthoxylum oil.
3. device as claimed in claim 1 or 2, it is characterised in that industrial exhaust fan is housed inside the stainless steel cage (6) (7) and it is connected to the pipeline of the drainer.
4. device as claimed in claim 1 or 2, it is characterised in that the drainer has side wall interlayer, the side wall interlayer Open up the entrance (8) and outlet (9) come in and gone out for condensed water respectively in top and the bottom;And the condensation pot bottom is opened up derives successively The outlet (13) of bottom aqueous phase layer and Pericarpium Zanthoxyli volatile oil.
5. device as claimed in claim 1 or 2, it is characterised in that it is defeated that the stainless steel cage (6) is installed on the thread mixing Send at the top 10-30cm of groove.
6. device as claimed in claim 3, it is characterised in that the power >=3KW of the industrial exhaust fan (7).
7. device as claimed in claim 1, it is characterised in that the thread mixing delivery chute slant setting, has inside it Can be by the helical feed that rotated and upwards submit material along the rotary shaft parallel with the thread mixing delivery chute Device (2);The rotation of the auger conveyor is pivotally connected to the motor (1) and is rotated by the motor running; The top of the thread mixing groove is provided with edible oil-in (4), bottom and is provided with fresh pepper fruit entrance (3) and fresh zanthoxylum oil outlet (5);The stainless steel cage (6) is installed at the 10-30cm of thread mixing delivery chute top, for escaping to vapor and therewith The Pericarpium Zanthoxyli volatile oil composition (12) for going out is collected, the industrial exhaust fan of the stainless steel cage inside equipped with power >=3KW (7) and it is connected to the pipeline of the drainer;The drainer has side wall interlayer, and the side wall interlayer is distinguished in top and the bottom Open up the entrance (8) and outlet (9) come in and gone out for condensed water;It is described condensation pot bottom open up successively derive bottom aqueous phase layer (11) with And the outlet (13) of Pericarpium Zanthoxyli volatile oil (10).
8. device as claimed in claim 3, it is characterised in that the thread mixing delivery chute slant setting, has inside it Can be by the helical feed that rotated and upwards submit material along the rotary shaft parallel with the thread mixing delivery chute Device (2);The rotation of the auger conveyor is pivotally connected to the motor (1) and is rotated by the motor running; The top of the thread mixing groove is provided with edible oil-in (4), bottom and is provided with fresh pepper fruit entrance (3) and fresh zanthoxylum oil outlet (5);The stainless steel cage (6) is installed at the 10-30cm of thread mixing delivery chute top, for escaping to vapor and therewith The Pericarpium Zanthoxyli volatile oil composition (12) for going out is collected, the industrial exhaust fan of the stainless steel cage inside equipped with power >=3KW (7) and it is connected to the pipeline of the drainer;The drainer has side wall interlayer, and the side wall interlayer is distinguished in top and the bottom Open up the entrance (8) and outlet (9) come in and gone out for condensed water;It is described condensation pot bottom open up successively derive bottom aqueous phase layer (11) with And the outlet (13) of Pericarpium Zanthoxyli volatile oil (10).
CN201620705782.3U 2016-07-06 2016-07-06 A device for being directed at fragrant flavor material of flower any of several hot spice plants oil is retrieved Active CN206143154U (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108094571A (en) * 2017-11-23 2018-06-01 洪雅县和鑫农业科技发展有限公司 A kind of Chinese prickly ash active water production technology
CN108117923A (en) * 2017-11-23 2018-06-05 洪雅县和鑫农业科技发展有限公司 A kind of Zanthoxylum essential oil production technology
CN108179064A (en) * 2017-12-25 2018-06-19 洪雅县和鑫农业科技发展有限公司 A kind of pepper aroma essential oil production technology
CN108315097A (en) * 2018-02-09 2018-07-24 程勇 A kind of charging/discharging device and its application method refining essential oil
CN111218334A (en) * 2020-03-18 2020-06-02 洪雅县和鑫农业科技发展有限公司 Seasoning oil refining device with oil-water separation system

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108094571A (en) * 2017-11-23 2018-06-01 洪雅县和鑫农业科技发展有限公司 A kind of Chinese prickly ash active water production technology
CN108117923A (en) * 2017-11-23 2018-06-05 洪雅县和鑫农业科技发展有限公司 A kind of Zanthoxylum essential oil production technology
CN108179064A (en) * 2017-12-25 2018-06-19 洪雅县和鑫农业科技发展有限公司 A kind of pepper aroma essential oil production technology
CN108315097A (en) * 2018-02-09 2018-07-24 程勇 A kind of charging/discharging device and its application method refining essential oil
CN111218334A (en) * 2020-03-18 2020-06-02 洪雅县和鑫农业科技发展有限公司 Seasoning oil refining device with oil-water separation system

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