CN206103895U - Gas reaction unit is united to liquid - Google Patents
Gas reaction unit is united to liquid Download PDFInfo
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- CN206103895U CN206103895U CN201620590566.9U CN201620590566U CN206103895U CN 206103895 U CN206103895 U CN 206103895U CN 201620590566 U CN201620590566 U CN 201620590566U CN 206103895 U CN206103895 U CN 206103895U
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- reactor
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- solution
- association response
- response device
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Abstract
The utility model discloses a gas reaction unit is united to liquid, it belongs to chemical industry equipment technical field. The device includes: the reation kettle, 1# circulating pump, one -level absorption reaction tower, absorption liquid transfer jar, 2# circulating pump, the gas that have mechanical agitator, clamp cover and a plurality of charge cavities the mixed reactor of liquid, gas feed, external heat exchanger, direct condenser, one -level tail gas pipeline, the tower of absorb the remnant air combination. The utility model provides a gas reaction unit is united to liquid can provide good reaction condition for reaction medium more than 2 kinds or 2 kinds, the utility model has the advantages of rate of equipment utilization is high, high, the no exhaust emissions of reaction efficiency.
Description
Technical field
This utility model is related to technical field of chemical, the equipment of more particularly to a kind of solution-air association response device and
Technology.
Background technology
Gas and liquid phase reactor mainly has 1. filler tower reactors, 2. board-like tower reactor, 3. falling film reactor, 4. spraying
Tower reactor, 5. bubbling column reactor, 6. stirring bubbling tank reactor, 7. venturi reactor.This several reactor is being changed
The application of work industry field is than wide, but respectively has advantage and deficiency.
Especially small-sized Fine Chemical and pharmaceuticals industry, naturally enough select in the lectotype selection of gas-liquid reaction
Stirring bubbling tank reactor. its advantage is：In reactor, gas can preferably be dispersed into tiny bubble, and increase gas-liquid connects
Contacting surface is accumulated.Its obvious deficiency is：Energy consumption is higher, and temperature should not be controlled, and gas effciency is low, and exhaust emissions amount is larger.
Based on above reason, it is desirable to which we must research and develop, and a kind of temperature is preferably controlled, gas effciency is high, reaction rate
The little gas-liquid reaction device of high, exhaust emissions amount.
The content of the invention
This utility model provides a kind of association response device of gas-liquid reaction, it is characterised in that the device collection mixing drum
, in one, it has temperature for bubble tank reactor, venturi reactor, three kinds of gas-liquid reaction device advantages of filler tower reactor
Degree preferably control, gas effciency is high, reaction rate height, exhaust emissions amount are little, to it is environment-friendly the advantages of.
A kind of solution-air association response device that this utility model is provided, it is characterised in that include：Band mechanical agitator, folder
Set, and the reactor of multiple charging apertures, 1# circulating pumps, first order absorption reaction tower, absorbing liquid transfer tank, 2# circulating pumps, solution-air mix
Close reactor, gas feed, external heat exchanger, reflux condenser, one-level exhaust pipe, tail gas absorber combination.
Preferably, described in solution-air association response device of the present utility model band mechanical agitator, chuck and it is multiple plus
The reactor in material hole, is stainless steel or enamel material, and volume is 1-30m3.
Preferably, the 1# circulating pumps and 2# circulating pumps described in solution-air association response device of the present utility model is rustless steel
Material or acidproof, alkaline-resisting lining plastic structure, pressure-bearing 0.1-0.4MPa.
Preferably, the gas-liquid mixing reactor described in solution-air association response device of the present utility model belongs to venturi reaction
One kind of device, is connected with the gas raw material of the gas bomb, cylinder for liquefied gas or other forms of participating in reaction by gas pipeline.
It is stainless steel or steel construction lining plastic material, pressure-bearing 0.1-0.2MPa.
Preferably, the first order absorption reaction tower and tail gas absorber described in solution-air association response device of the present utility model
Combination, belongs to one kind of filler tower reactor, and tower body is enamel material or PP plastic materials, and filler is PE Ball-type packings or ripple
Stricture of vagina filler.
Preferably, the external heat exchanger described in solution-air association response device of the present utility model, be graphite, enamel or
Stainless steel condenser or condenser combination, its heat exchange area is 10-100m2.
Preferably, the reflux condenser described in solution-air association response device of the present utility model is installed on reactor and just goes up
Side, is connected with first order absorption reaction tower by one-level exhaust pipe. and it is glass, graphite or enamel material, heat exchange area
1.5-10m2。
A kind of solution-air association response device of the present utility model, has an advantage in that.
This utility model can be that 2 kinds or two or more reaction medium provide good reaction condition.
This utility model is conventional equipment, with make it is simple, install easy the characteristics of.
This utility model has the characteristics of easy temperature control system, raw material availability are high, reaction efficiency is high.
This utility model has exhaust emissions amount little, the characteristics of environmentally friendly.
Description of the drawings
In order to be illustrated more clearly that technical scheme in this utility model embodiment or prior art, below will to embodiment or
Needed for description of the prior art, accompanying drawing to be used is briefly described, it should be apparent that, drawings in the following description are only
Some embodiments of the present utility model, for those skilled in the art, can be obtaining which according to these accompanying drawings
Its accompanying drawing.
Fig. 1 is the schematic diagram of solution-air association response device in this utility model embodiment.
In Fig. 1：
01- reactor main bodies, 04- liquid charging stock A imports, 05- gas raw material B imports, 06- thermometer boss, 07- reactions
Kettle chuck, 08- reactors bottom bottom valve, 09- reflux condensers, 10- liquid charging stock B imports, 11-1# circulating pumps, 12- sampling and into
Product are exported, 13- first order absorption reaction towers, 14- absorbing liquid transfer tanks, 15-2# circulating pumps, 16- gas-liquid mixed reactors, 17- gas
Body raw material A import, 18- external heat exchangers, 21- one-level exhaust pipes, the combination of 22- tail gas absorbers, after 23- purifications, tail gas goes out
Mouthful.
Specific embodiment
Below in conjunction with the accompanying drawings this utility model embodiment is described further.
As shown in figure -1, solution-air association response device of the present utility model, it is characterised in that include：01- reactor masters
Body, 04- liquid charging stock A imports, 05- gas raw material B imports, 06- thermometer boss, 07- reacting kettle jacketings, 08- reactors bottom
Bottom valve, 09- reflux condensers, 10- liquid charging stock B imports, 11-1# circulating pumps, 12- samplings and product outlet, 13- first order absorptions
Reaction tower, 14- absorbing liquid transfer tanks, 15-2# circulating pumps, 16- gas-liquid mixed reactors, 17- gas raw material A imports, 18- are external
Heat exchanger, 21- one-level exhaust pipes, the combination of 22- tail gas absorbers, offgas outlet after 23- purifications.
Further, the reactor main body -01 described in the solution-air association response device of this specific embodiment embodiment has
There are steam inlet or circulating water outlet 02, circulating water intake or hot water outlet 03, thermometer boss 06 and reacting kettle jacketing 07, body
Product is 1-30m3.
Further, the 1# circulating pumps -11 and 2# described in the solution-air association response device of this specific embodiment embodiment
Circulating pump -15 is stainless steel or acidproof, alkaline-resisting lining plastic structure, pressure-bearing 0.1-0.4MPa.
Further, the gas-liquid mixing reactor described in the solution-air association response device of this specific embodiment embodiment
One kind of category venturi reactor, by gas pipeline and gas bomb, cylinder for liquefied gas or the other forms of participating in reaction
Gas raw material is connected. and it is stainless steel or steel construction lining plastic material, pressure-bearing 0.1-0.2MPa.
Further, the first order absorption reaction tower described in the solution-air association response device of this specific embodiment embodiment
13, belong to one kind of filler tower reactor, tower body is enamel material or PP plastic materials, and filler is that PE Ball-type packings or ripple are filled out
Material.
Further, the external heat exchanger 18 described in the solution-air association response device of this specific embodiment embodiment, tool
There are circulating water intake 19 and circulating water outlet 20, be that graphite, enamel or stainless steel condenser or condenser are combined, its heat-transfer surface
Product is 10-100m2.
Further, the reflux condenser 09 described in the solution-air association response device of this specific embodiment embodiment is pacified
Directly over reactor, it is connected with first order absorption reaction tower 13 by one-level exhaust pipe 21. it is glass, graphite or wards off glass
Glass material, it is connected with less than 15 °C of cooling water, heat exchange area 1.5-10m2.
Further, the tail gas absorber combination described in the solution-air association response device of this specific embodiment embodiment
22 are in series by 4-10 platform packing material absorbing reaction towers, built-in PE Ball-type packings or ripple packing, and its end is connected with vacuum pump.
Generic principles defined herein, can in the case of without departing from spirit or scope of the present utility model,
Realize in other embodiments.Therefore, this utility model will not be limited to the embodiments shown herein, every practical new
Within type spirit and principle, any modification, equivalent substitution and improvements made etc. should be included in protection model of the present utility model
Within enclosing.This utility model institute protection domain is to fit to consistent with principles disclosed herein and features of novelty most wide
Scope.
Claims (8)
1. a kind of solution-air association response device, it includes：With mechanical agitator, the reactor of chuck and multiple charging apertures,
1# circulating pumps, first order absorption reaction tower, absorbing liquid transfer tank, 2# circulating pumps, gas-liquid mixing reactor, gas feed, outer displacement
Hot device, reflux condenser, one-level exhaust pipe, tail gas absorber combination, it is characterised in that with mechanical agitator, chuck and
The reactor of multiple charging apertures is connected with first order absorption reaction tower by 1# circulating pumps, and first grade absorption tower passes through absorbing liquid transfer
Tank, 2# circulating pumps are connected with gas-liquid mixing reactor, and gas-liquid mixing reactor one end is connected to gas feed and first order absorption
Tower, the other end are connected with reactor by external heat exchanger, and reflux condenser one end is ined succession reactor, and the other end passes through one-level tail
Feed channel is connected with first grade absorption tower, and first grade absorption tower is combined with tail gas absorber and is connected.
2. solution-air association response device according to claim 1, it is characterised in that described mechanical agitator, chuck,
Reactor with multiple charging apertures is stainless steel or enamel material, and volume is 1-30m3。
3. solution-air association response device according to claim 1, it is characterised in that described 1# circulating pumps and reactor,
First order absorption reaction tower is connected, and is stainless steel or acidproof, alkaline-resisting lining plastic structure, pressure-bearing 0.1-0.4MPa.
4. solution-air association response device according to claim 1, it is characterised in that described first order absorption reaction tower leads to
Cross reaction residual air pipeline, reflux condenser to be connected with reactor, absorption tower body is enamel material or PP plastic materials, absorption tower
Built with ripple packing or spherical PE fillers.
5. solution-air association response device according to claim 1, it is characterised in that described gas-liquid mixing reactor leads to
Cross 2# circulating pumps to be connected with absorbing liquid transfer tank, be connected with reactor by external heat exchanger, it is anti-with participation by gas pipeline
The gas bomb answered or cylinder for liquefied gas are connected, and it is stainless steel or steel construction lining plastic material. pressure-bearing 0.1-0.2MPa.
6. solution-air association response device according to claim 1, it is characterised in that described external heat exchanger and solution-air
Mixing reactor is connected with reactor, and it is that graphite, enamel or stainless steel condenser or condenser are combined, and its heat exchange area is
10-100m2。
7. solution-air association response device according to claim 1, it is characterised in that described reflux condenser is installed on
Directly over reactor, it is connected with first order absorption reaction tower by one-level exhaust pipe, it is graphite, enamel or stainless steel
Matter, heat exchange area 1.5-10m2。
8. solution-air association response device according to claim 1, it is characterised in that described tail gas absorber combination is
Refer to that 4-10 platforms absorption tower is in series, every absorption tower is built with ripple packing or spherical PE fillers.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620590566.9U CN206103895U (en) | 2016-06-17 | 2016-06-17 | Gas reaction unit is united to liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620590566.9U CN206103895U (en) | 2016-06-17 | 2016-06-17 | Gas reaction unit is united to liquid |
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| CN206103895U true CN206103895U (en) | 2017-04-19 |
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| CN201620590566.9U Active CN206103895U (en) | 2016-06-17 | 2016-06-17 | Gas reaction unit is united to liquid |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106166470A (en) * | 2016-07-23 | 2016-11-30 | 河南新天地药业股份有限公司 | A kind of dynamic hydraulic combined reaction unit |
-
2016
- 2016-06-17 CN CN201620590566.9U patent/CN206103895U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106166470A (en) * | 2016-07-23 | 2016-11-30 | 河南新天地药业股份有限公司 | A kind of dynamic hydraulic combined reaction unit |
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