CN206083865U - Device of tiny powder of titanium alloy is at high proportion prepared in continuous smelting atomizing - Google Patents

Device of tiny powder of titanium alloy is at high proportion prepared in continuous smelting atomizing Download PDF

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Publication number
CN206083865U
CN206083865U CN201621146908.4U CN201621146908U CN206083865U CN 206083865 U CN206083865 U CN 206083865U CN 201621146908 U CN201621146908 U CN 201621146908U CN 206083865 U CN206083865 U CN 206083865U
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China
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titanium alloy
heating coil
powder
high proportion
alloy bar
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CN201621146908.4U
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Inventor
陈仕奇
王闻迪
张越
刘国库
王惠斌
张超
张爱平
穆守业
孔秀云
刘红虎
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Harbin three ground Additive Manufacturing Co., Ltd.
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Harbin Three Add Material Manufacturing Materials Co Ltd
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Abstract

The utility model provides a device of tiny powder of titanium alloy is at high proportion prepared in continuous smelting atomizing, which comprises a housin, the top of casing is real empty room, real empty room's top is provided with the feeder, the feeder is used for carrying titanium alloy bar, titanium alloy bar's bottom cover is equipped with and melts heating coil the top of melting heating coil just is in titanium alloy bar's outside cover is equipped with heating coil in advance, heating coil is connected with heating power adjusting device in advance, real empty room's below sets up the atomizer chamber, the bottom intercommunication of atomizer chamber has the powder of receipts jar. The advantage does: fully improve the super -heated rate of liquid titanium alloy, reduce viscosity, form and stabilize continuous liquid stream, avoid the atomizing waste of argon gas, reduced argon gas use cost, improve the productivity of powder simultaneously.

Description

Continuous smelting atomization prepares the device of titanium alloy fine powder at high proportion
Technical field
The utility model belongs to high activity metal powder preparing technical field, and in particular to prepared by a kind of continuous smelting atomization The device of titanium alloy fine powder at high proportion.
Background technology
Titanium elements the whole world distribution than wide, its content exceedes the 0.4% of earth crustal mass, global proved reserves about 34 Hundred million tons, content occupies the 10th in all elements, and front 10 bit is plain to be ordered as:Oxygen, silicon, aluminium, iron, calcium, sodium, potassium, magnesium, hydrogen, Titanium.Titanium is less than steel density by 40%, and the intensity of the intensity of titanium and steel is quite, and this can improve structure efficiency.Meanwhile, titanium it is heat-resisting Property, corrosion resistance, elasticity, elastoresistance and shaping processability are good.Titanium alloy is just applied to aircraft industry from occurring.Space shuttle It is main, applied range airborne vehicle.Titanium is the primary structural material of aircraft, is also aerial engine fan, compressor The preferred material of the important component such as wheel disc and blade, is described as " space metal ".Aircraft is more advanced, and titanium consumption is more, such as the U.S. F22 forth generation machines Ti content is 41% (mass fraction), and its F119 engines Ti content is 39%, is to use Ti content at present High aircraft.In aviation, the development of aircraft industry also promotes the development of titanium alloy to titanium alloy research origin.Titanium Alloys for Aviation Research be always important in a titanium alloy field, active branch.
In aerospace field, have many titanium alloy parts all have labyrinth characteristic, adopt powder metallurgy more with And the manufacture of the method such as 3D printing.Therefore, titanium alloy needs are previously prepared into powder morphology, could use in above-mentioned field.Titanium is closed Gold has a very high activity under high-temperature atmosphere, and reacts with multiple element in the molten state, causes titanium alloy powder Preparation it is different from the preparation method of conventional metal powder.
At present, prepare titanium alloy powder is equipped with rotary electrode method and gas atomization.Rotary electrode method is adapted to production Granularity is the powder between 75~150 μm, due to unstability of the titanium alloy electrode bar under high speed rotation status, current nothing Method produces powder of the granularity less than 50 μm by improving rotating speed;And powder size prepared by gas atomization can be 0~150 Adjust between μm, especially produce powder of the granularity less than 50 μm and there is advantage, be the unique production method of current titanium alloy fine powder.Should Method is made special equipment and is produced in Europe (such as Germany) and North America (such as Canada) country.
Prepare titanium alloy powder field in aerosolization, the major way for adopting at present for:Arrange in the bottom of titanium alloy bar Fusing heating coil, the bottom of titanium alloy bar is directly heated by melting heating coil, until titanium alloy bar is fused into liquid drop Fall.The Jing atomizations again of the titanium alloy drop of drippage, form powder.But, the subject matter that said method is present is:Titanium alloy is from admittedly The incubation period of state to liquid is long, will gutter down in an instant after titanium alloy melts, it is difficult to by titanium alloy liquid temperature Degree brings up to fusing point above much higher value;In addition, the viscosity of liquid titanium alloy is also very high, it is impossible to form continuous flow, so as to affect Follow-up gas atomization effect, causes the recovery rate of fine powder relatively low, although less than 50 μm of fine powder can be prepared, this Specification powder proportion is generally below 40%, low production efficiency;Further, since liquid titanium alloy cannot form continuous flow, And it is continual to be atomized the high-purity argon gas for entering, part argon gas is necessarily caused to act on drop, so as to cause argon gas Waste, increase argon gas use cost.
Utility model content
For the defect that prior art is present, the utility model provides a kind of continuous smelting atomization and prepares titanium alloy at high proportion The device of fine powder, can effectively solving the problems referred to above.
The technical solution adopted in the utility model is as follows:
The utility model provides the device that a kind of continuous smelting atomization prepares titanium alloy fine powder at high proportion, including shell Body, the top of the housing is vacuum chamber, and feed appliance is provided with the top of the vacuum chamber, and the feed appliance is used to convey titanium conjunction Golden rod;Fusing heating coil is arranged with the bottom of the titanium alloy bar, in the top of the fusing heating coil and described The outside of titanium alloy bar is arranged with pre-heating coil;The pre-heating coil is connected with heating power adjusting means;
The lower section of the vacuum chamber arranges spray chamber, and the bottom of the spray chamber is communicated with receipts powder tank.
Preferably, the pre-heating coil is located at the position of 20~40 millimeters of the fusing heating coil top.
Preferably, the pre-heating coil is located at the position of 30 millimeters of the fusing heating coil top.
Preferably, the titanium alloy bar is using the titanium alloy bar with diameter greater than 80 millimeters.
The continuous smelting atomization that the utility model is provided prepare the device of titanium alloy fine powder at high proportion have it is following excellent Point:
The utility model can fully improve the degree of superheat of liquid titanium alloy, reduce viscosity, form the liquid stream of steady and continuous, The waste for avoiding argon gas from being atomized, reduces argon gas use cost, while improving the yield of powder.
Description of the drawings
Fig. 1 shows for the structure that the continuous smelting atomization that prior art is provided prepares the device of titanium alloy fine powder at high proportion It is intended to;
Fig. 2 is the arrangement schematic diagram of pre-heating coil of the present utility model;
The schematic diagram that Fig. 3 increases for the diameter of titanium alloy bar;
Wherein:1- feed appliances;2- titanium alloy bars;3- vacuum chambers;4- melts heating coil;5- spray chambers;6- atomizers; 7- powder;8- receives powder tank;9- pre-heating coils.
Specific embodiment
In order that technical problem, technical scheme and beneficial effect that the utility model is solved become more apparent, below With reference to drawings and Examples, the utility model is further elaborated.It should be appreciated that described herein be embodied as Example only to explain the utility model, is not used to limit the utility model.
The utility model provides the device that a kind of continuous smelting atomization prepares titanium alloy fine powder at high proportion, using enhancing Heating and the technology of expansion alloy liquid surface adhesion, can increase substantially the fine grain recovery rate of titanium alloy powder, and Argon gas use cost is reduced, profit margin is improved.Can shape as following titanium alloy injection moulding and various mode increasing material manufacturings Powder stock preparation facilities.
With reference to Fig. 2, the continuous smelting atomization that the utility model is provided prepares the device of titanium alloy fine powder at high proportion, bag Housing is included, the top of the housing is vacuum chamber, feed appliance is provided with the top of the vacuum chamber, the feed appliance is used to convey Titanium alloy bar;Be arranged with fusing heating coil in the bottom of the titanium alloy bar, it is described fusing heating coil top and The outside of the titanium alloy bar is arranged with pre-heating coil;The pre-heating coil is connected with heating power adjusting means;It is described The lower section of vacuum chamber arranges spray chamber, and the bottom of the spray chamber is communicated with receipts powder tank.
As can be seen here, in the top addition pre-heating coil of fusing heating coil, position is in fusing heating for the utility model Coil top 20-40mm, pre-heating coil is made up of a circle coil, and heating power adjustable range is 20-100KW.Pre-add hot line The purpose of circle is:Heating is near the titanium alloy bar part of fusing heating coil so as to reaches the temperature of close fusing point, mainly there is two Individual effect:One is that the heat for blocking titanium alloy bar melting end is axially upwardly transmitted to unfused part, keeps the temperature of melting end; Two is the raw material for conveying close titanium alloy fusing point in advance for melting end.When the feedstock portions of close titanium alloy bar fusing point enter fusing When in the sphere of action of heating coil, in a short period of time, titanium alloy bar surface liquid temperature i.e. exceed titanium alloy fusing point compared with High temperature (more than 200 DEG C), and the heat blocking for passing through preliminary heating section, higher than can be protected in the temperature short time of fusing point Hold.
Additionally, with reference to Fig. 3, the utility model is by the enlarged diameter of raw material titanium alloy bar to more than 80mm, it is therefore intended that:When Overheated titanium alloy liquid faces down when trickling along the taper that melting end is formed, the diameter due to increasing titanium alloy bar, taper The area size in face also can be increased, and so as to increased the bond area and adhesive force of liquid, titanium alloy liquid will not trickle easily Fall, can equally increased time of the titanium alloy by electromagnetic induction, fully improve the degree of superheat of liquid titanium alloy, reduce viscosity, Form the liquid stream of steady and continuous, it is to avoid the waste of argon gas atomization, reduce argon gas use cost, while improving the yield of powder.
In sum, the continuous smelting atomization that the utility model is provided prepares the device tool of titanium alloy fine powder at high proportion Have the advantage that:
The utility model can fully improve the degree of superheat of liquid titanium alloy, reduce viscosity, form the liquid stream of steady and continuous, The waste for avoiding argon gas from being atomized, reduces argon gas use cost, while improving the yield of powder.
The above is only preferred embodiment of the present utility model, it is noted that for the common skill of the art For art personnel, on the premise of without departing from the utility model principle, some improvements and modifications can also be made, these improve and Retouching should also regard protection domain of the present utility model.

Claims (4)

1. a kind of continuous smelting atomization prepares the device of titanium alloy fine powder at high proportion, it is characterised in that described including housing The top of housing is vacuum chamber, and feed appliance is provided with the top of the vacuum chamber, and the feed appliance is used to convey titanium alloy bar; The bottom of the titanium alloy bar is arranged with fusing heating coil, in the top of the fusing heating coil and in the titanium alloy bar Outside be arranged with pre-heating coil;The pre-heating coil is connected with heating power adjusting means;
The lower section of the vacuum chamber arranges spray chamber, and the bottom of the spray chamber is communicated with receipts powder tank.
2. continuous smelting atomization according to claim 1 prepares the device of titanium alloy fine powder at high proportion, and its feature exists In the pre-heating coil is located at the position of 20~40 millimeters of the fusing heating coil top.
3. continuous smelting atomization according to claim 2 prepares the device of titanium alloy fine powder at high proportion, and its feature exists In the pre-heating coil is located at the position of 30 millimeters of the fusing heating coil top.
4. continuous smelting atomization according to claim 1 prepares the device of titanium alloy fine powder at high proportion, and its feature exists In the titanium alloy bar is using the titanium alloy bar with diameter greater than 80 millimeters.
CN201621146908.4U 2016-10-21 2016-10-21 Device of tiny powder of titanium alloy is at high proportion prepared in continuous smelting atomizing Active CN206083865U (en)

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CN201621146908.4U CN206083865U (en) 2016-10-21 2016-10-21 Device of tiny powder of titanium alloy is at high proportion prepared in continuous smelting atomizing

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107234245A (en) * 2017-08-12 2017-10-10 长沙唯特冶金工程技术有限公司 The equipment that a kind of use bar continuous feed produces spherical powder

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107234245A (en) * 2017-08-12 2017-10-10 长沙唯特冶金工程技术有限公司 The equipment that a kind of use bar continuous feed produces spherical powder

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Address after: 150028 Room 302, zone A, innovation and entrepreneurship Plaza, No. 60 Shi Mao Avenue, science and technology innovation city, Harbin high tech Industrial Development Zone, Heilongjiang, China (60)

Patentee after: Harbin three ground Additive Manufacturing Co., Ltd.

Address before: 150028 Heilongjiang high tech Industrial Development Zone, Harbin science and technology innovation city enterprise accelerator building, No. 12, wisdom Valley, No. two, room 4058, No.

Patentee before: Harbin three add material manufacturing materials Co., Ltd.

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