CN206033279U - High -purity polyferric sulfate production system - Google Patents
High -purity polyferric sulfate production system Download PDFInfo
- Publication number
- CN206033279U CN206033279U CN201620658651.4U CN201620658651U CN206033279U CN 206033279 U CN206033279 U CN 206033279U CN 201620658651 U CN201620658651 U CN 201620658651U CN 206033279 U CN206033279 U CN 206033279U
- Authority
- CN
- China
- Prior art keywords
- reactor
- inlet
- ferric sulfate
- sodium chlorate
- entrance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Abstract
The utility model discloses a high -purity polyferric sulfate production system, including the feed tank that connects gradually, the polymerization device, the solidification equipment, the polyferric sulfate storage tank, the polymerization device is equipped with the sulphuric acid entry, catalyst inlet, air inlet, the oxidant entry, steam inlet, the sodium chlorate entry, the feed tank pours into ferrous sulfate into to the polymerization device, the steam inlet steaming heats, catalyst inlet and air inlet let in the catalyst, the air carries out the oxidation, oxidant entry and sodium chlorate entry let in the hydrogen peroxide solution and sodium chlorate carries out deep oxidation at the synthetic polyferric sulfate of polymerization device cohesion, it obtains solid polyferric sulfate and preserves the storage tank to polyferric sulfate to get into the solidification equipment after the polyferric sulfate decompression evaporation. The utility model discloses use earlier air catalytic oxidation, then with sodium chlorate, hydrogen peroxide solution deep oxidation, synthetic polyferric sulfate, it is with low costs, move and stabilize.
Description
Technical field
This utility model is related to reaction unit technical field, and in particular to a kind of high-purity bodied ferric sulfate production system.
Background technology
Bodied ferric sulfate is a kind of inorganic polymer flocculant of superior performance, and morphological characters is faint yellow unformed powdery
Solid, is highly soluble in water, and 10%（Quality）Aqueous solution be rufous clear solution, hygroscopicity.Bodied ferric sulfate is widely used in
The purified treatment of drinking water, water for industrial use, various industrial wastewaters, municipal sewage, sludge dewatering etc..
The preparation of bodied ferric sulfate mainly has direct oxidation method method and catalytic oxidation, the preparation of most of bodied ferric sulfates
Using direct oxidation method, this method process route is simpler, can reduce equipment investment and production link for commercial production, reduces
Equipment cost, but this production technology is necessarily dependent upon oxidant, and reaction unit is that the key core for producing bodied ferric sulfate sets
It is standby, its 3 dominant response：Oxidation reaction, hydrolysis, polyreaction are all carried out wherein, while be present in a system working as
In, influence each other, mutually promote.Particularly react very sensitive, material feed postition, material addition, material add the time,
The various factors such as stirring intensity, gas distribution, reaction temperature, response time have to the effect of polyreaction and the quality of product
Very big impact, but existing reaction unit is unable to effective detection course of reaction, there is provided accurately control.
The content of the invention
Goal of the invention：For the deficiencies in the prior art, this utility model provides a kind of high-purity bodied ferric sulfate production system,
It is low cost, stable.
Technical scheme：High-purity bodied ferric sulfate production system described in the utility model, including the feeder channel being sequentially connected,
Polymerizing reactor, solidification equipment, bodied ferric sulfate storage tank, polymerizing reactor are provided with sulphuric acid entrance, catalyst inlet, air
Entrance, oxidant inlet, steam inlet, sodium chlorate entrance, feeder channel inject ferrous sulfate, steam inlet to polymerizing reactor
It is passed through steam to be heated, catalyst inlet and air intake are passed through catalyst, air and are aoxidized, oxidant inlet and chloric acid
Sodium entrance is passed through hydrogen peroxide and sodium chlorate and carries out deep oxidation in the cohesion synthesizing polymeric ferric sulfate of polymerizing reactor, polyaluminum sulfate
Ferrum obtains solid ferric polysulfate into solidification equipment after being evaporated under reduced pressure and preserves to bodied ferric sulfate storage tank.
Further, the polymerizing reactor includes reactor, and the sulphuric acid entrance, sodium chlorate entrance, oxidant enter
Mouthful be arranged at the top of reactor, reactor bottom is provided with discharging opening, reactor bottom land and inclines towards discharging opening, at the top of reactor in
The heart is provided with reducing motor, reducing motor and is connected with the agitator in reactor, and reactor side wall is provided with several baffle plates, baffle plate
Entrance is provided with, gas distribution tube in reactor, is provided with, gas distribution tube is provided with air intake and vapour inlet.
Further, the reactor is connected with detection pipe, and reactor bottom liquid is evacuated to by detection pipe by detecting pump
Detection bucket, is provided with PH meters in detection bucket, detection bucket is connected with reactor inner top by return duct.
Further, the solidification equipment includes that the vacuum pump being sequentially connected, exsiccator, filter, condenser, vacuum are done
Dry case, exsiccator are connected with the bottom of filter, and filter top is connected with condenser.
Beneficial effect：Compared with prior art, advantage of the present utility model：This utility model first uses air catalytic oxidation,
Then sodium chlorate, hydrogen peroxide deep oxidation is used, synthesizing polymeric ferric sulfate, low cost are stable；Design by optimize charging,
Discharging structure, coordinates detection bucket, it is ensured that it is efficient, stable that bodied ferric sulfate reacts, and low cost, operation are controllable, it is ensured that produce
Quality；Maintenance difficult and a continuous-stable feed difficult problem is solved, Yield and quality and the equipment life of device is improved；Have simultaneously
The caking difficult problem for reducing energy consumption, solving in solidification process of effect, it is ensured that the quality of product.
Description of the drawings
Fig. 1 is structural representation of the present utility model；
Structural representations of the Fig. 2 for polymerizing reactor；
Structural representations of the Fig. 3 for solidification equipment.
Specific embodiment
Technical solutions of the utility model are described in detail below by accompanying drawing.
Embodiment 1：High-purity bodied ferric sulfate production system as shown in Figure 1, it is anti-including the feeder channel, polymerization being sequentially connected
Answer device, solidification equipment, bodied ferric sulfate storage tank.
As shown in Fig. 2 polymerizing reactor includes reactor 1 and detection pipe 9, reactor 1 adopts the carbon steel material, wall thickness to be
120mm, 1 periphery of reactor are provided with fixed column, and inner tip is provided with support beam；Sulphuric acid charge door 2, chlorine is provided with the top of reactor 1
Sour sodium charge door 10, hydrogen peroxide charge door 3,1 bottom of reactor are provided with discharging opening 12,1 bottom land 11 of reactor and incline towards discharging opening
Tiltedly, 11 angle of inclination of bottom land is 3 °, and 1 top center of reactor is provided with the stirring in reducing motor 1, reducing motor 1 and reactor 1
Device 7 is connected, and agitator 7 is provided with Dual-layer stirring vane；1 side wall of reactor is evenly distributed with 4 groups baffle plates, and baffle plate is provided with
Charge door；Gas distribution tube is provided with reactor 1, gas distribution tube is provided with air intake and vapour inlet；Detection pipe 9 is by inspection
Survey pump 8 and 1 bottom liquid of reactor is evacuated to into detection bucket 5 from detection mouth 13, detection bucket is provided with catalyst charging hole and PH meters 6, inspection
Survey bucket 5 to connect with 1 inner top of reactor by return duct.In reactor 1, the pH value of liquid is with sulphuric acid, addition speed
Degree, oxidizing process, hydrolytic process and change, arrange detection pipe by reaction liquid continuous pump to detect bucket carry out detection can be accurate
Understand reaction process, control course of reaction.
Solidification equipment as shown in Figure 3, including the vacuum pump 21, exsiccator 22, filter 23, condenser that are sequentially connected
24th, vacuum drying oven 26, exsiccator 22 are connected with the bottom of filter 23, are connected with condenser 24 at the top of filter 23, condensation
Device 24 is provided with three-way valve 25 with the connecting pipe of vacuum drying oven 26.
Although as described above, having represented and having described this utility model with reference to specific preferred embodiment, which must not
It is construed to the restriction to this utility model itself.In the spirit and scope of the present utility model defined without departing from claims
Under the premise of, can various changes can be made in the form and details to which.
Claims (4)
1. a kind of high-purity bodied ferric sulfate production system, it is characterised in that：Including feeder channel, the polyreaction dress being sequentially connected
Put, solidification equipment, bodied ferric sulfate storage tank, polymerizing reactor is provided with sulphuric acid entrance, catalyst inlet, air intake, oxidation
Agent entrance, steam inlet, sodium chlorate entrance, feeder channel inject ferrous sulfate to polymerizing reactor, and steam inlet is passed through steam
Heated, catalyst inlet and air intake are passed through catalyst, air and are aoxidized, oxidant inlet and sodium chlorate entrance are logical
Entering hydrogen peroxide and sodium chlorate carries out deep oxidation in the cohesion synthesizing polymeric ferric sulfate of polymerizing reactor, and bodied ferric sulfate decompression is steamed
Solid ferric polysulfate is obtained into solidification equipment after sending out to preserve to bodied ferric sulfate storage tank.
2. high-purity bodied ferric sulfate production system according to claim 1, it is characterised in that：The polymerizing reactor bag
Reactor is included, the sulphuric acid entrance, sodium chlorate entrance, oxidant inlet are arranged at the top of reactor, and reactor bottom is provided with out
Material mouth, reactor bottom land are inclined towards discharging opening, and reactor top center is provided with reducing motor, reducing motor and reactor
Agitator is connected, and reactor side wall is provided with several baffle plates, and baffle plate is provided with entrance, is provided with gas distribution tube in reactor,
Gas distribution tube is provided with air intake and vapour inlet.
3. high-purity bodied ferric sulfate production system according to claim 2, it is characterised in that：The reactor is connected with inspection
Reactor bottom liquid is evacuated to detection bucket by detecting pump by test tube, detection pipe, is provided with PH meters in detection bucket, and detection bucket passes through
Return duct is connected with reactor inner top.
4. high-purity bodied ferric sulfate production system according to claim 1, it is characterised in that：The solidification equipment include according to
The vacuum pump of secondary connection, exsiccator, filter, condenser, vacuum drying oven, exsiccator are connected with the bottom of filter, are filtered
It is connected with condenser at the top of device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620658651.4U CN206033279U (en) | 2016-06-29 | 2016-06-29 | High -purity polyferric sulfate production system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620658651.4U CN206033279U (en) | 2016-06-29 | 2016-06-29 | High -purity polyferric sulfate production system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206033279U true CN206033279U (en) | 2017-03-22 |
Family
ID=58313140
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620658651.4U Expired - Fee Related CN206033279U (en) | 2016-06-29 | 2016-06-29 | High -purity polyferric sulfate production system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206033279U (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108640241A (en) * | 2018-05-03 | 2018-10-12 | 武汉轻工大学 | A kind of processing method of preparation method and starch from sweet potato the processing slag charge of polymeric ferric sulfate flocculant |
| CN108751369A (en) * | 2018-06-08 | 2018-11-06 | 高密博宇环保科技有限公司 | A kind of production method of bodied ferric sulfate |
| CN111573800A (en) * | 2020-04-30 | 2020-08-25 | 广西夏阳环保科技有限公司 | Natural composite polymeric molten iron sulfate treatment agent and preparation method thereof |
| CN111592081A (en) * | 2020-04-30 | 2020-08-28 | 广西夏阳环保科技有限公司 | Preparation method of biomass composite polymeric molten iron sulfate treatment agent |
| CN112110496A (en) * | 2020-09-25 | 2020-12-22 | 安徽工业大学 | Preparation method of polymeric ferric sulfate |
-
2016
- 2016-06-29 CN CN201620658651.4U patent/CN206033279U/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108640241A (en) * | 2018-05-03 | 2018-10-12 | 武汉轻工大学 | A kind of processing method of preparation method and starch from sweet potato the processing slag charge of polymeric ferric sulfate flocculant |
| CN108640241B (en) * | 2018-05-03 | 2021-04-20 | 武汉轻工大学 | Preparation method of polymeric ferric sulfate flocculant and treatment method of sweet potato starch processing slag |
| CN108751369A (en) * | 2018-06-08 | 2018-11-06 | 高密博宇环保科技有限公司 | A kind of production method of bodied ferric sulfate |
| CN108751369B (en) * | 2018-06-08 | 2021-03-26 | 高密博宇环保科技有限公司 | Production method of polymeric ferric sulfate |
| CN111573800A (en) * | 2020-04-30 | 2020-08-25 | 广西夏阳环保科技有限公司 | Natural composite polymeric molten iron sulfate treatment agent and preparation method thereof |
| CN111592081A (en) * | 2020-04-30 | 2020-08-28 | 广西夏阳环保科技有限公司 | Preparation method of biomass composite polymeric molten iron sulfate treatment agent |
| CN112110496A (en) * | 2020-09-25 | 2020-12-22 | 安徽工业大学 | Preparation method of polymeric ferric sulfate |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206033279U (en) | High -purity polyferric sulfate production system | |
| CN103466829B (en) | High-concentration ammonia nitrogen waste water treatment method and system thereof | |
| CN109336271A (en) | Depressurize the biogas slurry ammonia nitrogen film recovery system and method for auxiliary | |
| CN206033276U (en) | Polyferric sulfate reaction unit | |
| CN106865757A (en) | A kind of anerobic sowage treatment reactor heating system based on Direct fired absorption heat pump | |
| CN112939216B (en) | Organic wastewater built-in block anaerobic reactor | |
| CN204873880U (en) | Two catalytic oxidation preparations of iron and steel pickling water increase production system of gathering molysite water purification agent | |
| CN205472658U (en) | High -efficient sulfur trioxide transition system | |
| CN107434343A (en) | Method without Matter Transfer in mechanical agitation Treatment of Sludge anaerobic reactor and reactor | |
| CN207941383U (en) | Chloracetyl chloride tail gas by-product sulfuric acid apparatus | |
| CN206325543U (en) | Polymeric ferric sulfate production apparatus | |
| CN213885048U (en) | Waste water recovery system of fosetyl-aluminum esterification reaction | |
| CN211688672U (en) | Waste water treatment device in pyrazole production process | |
| CN206033278U (en) | Polyferric sulfate apparatus for producing | |
| CN204294104U (en) | A kind of CO that is carrier with anaerobic fermentation natural pond liquid 2absorption and storage utilize system | |
| CN209352747U (en) | Anaerobic sludge digestion processing unit | |
| CN209276512U (en) | High concentration organic waste dry-type anaerobic system | |
| CN208694286U (en) | It is a kind of for synthesizing the reaction unit of pseudocumene | |
| CN206901870U (en) | A kind of efficient compound anaerobic reactor | |
| CN201971677U (en) | Augmentin strain enrichment and expanded culture reactor | |
| CN206721005U (en) | Without mechanical agitation Treatment of Sludge anaerobic reactor | |
| CN108728336A (en) | A kind of superhigh temperature biological hydrolysis synchronizes the anaerobic fermentation processing system and method for deamination | |
| CN206352097U (en) | A kind of processing unit of high salinity organic wastewater with difficult degradation thereby | |
| CN206927646U (en) | One kind processing ammonia still of ammonia waste water containing metal complex | |
| CN206502727U (en) | One kind dehydration excess sludge anaerobic digestion integrated equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170322 Termination date: 20180629 |