CN206033276U - Polyferric sulfate reaction unit - Google Patents
Polyferric sulfate reaction unit Download PDFInfo
- Publication number
- CN206033276U CN206033276U CN201620658583.1U CN201620658583U CN206033276U CN 206033276 U CN206033276 U CN 206033276U CN 201620658583 U CN201620658583 U CN 201620658583U CN 206033276 U CN206033276 U CN 206033276U
- Authority
- CN
- China
- Prior art keywords
- reactor
- reation kettle
- charge door
- reaction unit
- sulfate reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 24
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 title abstract 3
- 238000001514 detection method Methods 0.000 claims abstract description 26
- MHAJPDPJQMAIIY-UHFFFAOYSA-N hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000007788 liquid Substances 0.000 claims abstract description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 6
- 235000011149 sulphuric acid Nutrition 0.000 claims abstract description 6
- 239000001117 sulphuric acid Substances 0.000 claims abstract description 6
- YZHUMGUJCQRKBT-UHFFFAOYSA-M Sodium chlorate Chemical compound [Na+].[O-]Cl(=O)=O YZHUMGUJCQRKBT-UHFFFAOYSA-M 0.000 claims abstract description 4
- 229940080281 sodium chlorate Drugs 0.000 claims abstract description 4
- RUTXIHLAWFEWGM-UHFFFAOYSA-H Iron(III) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 claims description 16
- 229940032950 ferric sulfate Drugs 0.000 claims description 16
- 229910000360 iron(III) sulfate Inorganic materials 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 9
- 239000007789 gas Substances 0.000 claims description 8
- 238000007599 discharging Methods 0.000 claims description 7
- 238000009826 distribution Methods 0.000 claims description 7
- 229910000975 Carbon steel Inorganic materials 0.000 claims description 4
- 239000010962 carbon steel Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000002355 dual-layer Substances 0.000 claims description 3
- 238000010025 steaming Methods 0.000 claims 1
- 238000000034 method Methods 0.000 description 5
- 238000007254 oxidation reaction Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 230000001590 oxidative Effects 0.000 description 3
- 239000012295 chemical reaction liquid Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000003301 hydrolyzing Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000004044 response Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000007259 addition reaction Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000003197 catalytic Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001419 dependent Effects 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000010842 industrial wastewater Substances 0.000 description 1
- 229920000592 inorganic polymer Polymers 0.000 description 1
- 230000000877 morphologic Effects 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
Abstract
The utility model discloses a polyferric sulfate reaction unit, including reation kettle and detecting tube, the reation kettle top is equipped with sulphuric acid charge door, sodium chlorate charge door, hydrogen peroxide solution charge door, and the reation kettle bottom is equipped with the discharge gate, the reation kettle tank bottom inclines towards the discharge gate, and reation kettle top center is equipped with gear motor, gear motor is continuous with the agitator in the reation kettle, is equipped with a plurality of baffle on the reation kettle lateral wall, is equipped with the charge door on the baffle, is equipped with reation kettle 0 in the reation kettle, and reation kettle 0 is equipped with reation kettle 2 and vapour entry, the detecting tube is taken out reation kettle bottom liquid to detecting the bucket through detection pump, installs the PH meter in detecting the bucket, detects the bucket through top intercommunication in back flow and the reation kettle. The utility model relates to a, ejection of compact structure reinforced through optimizing, the cooperation detects the bucket, has guaranteed high efficiency, stability of polyferric sulfate reaction, and is with low costs, move controllablely, has guaranteed product quality.
Description
Technical field
This utility model is related to reaction unit technical field, and in particular to a kind of bodied ferric sulfate reaction unit.
Background technology
Bodied ferric sulfate is a kind of inorganic polymer flocculant of superior performance, and morphological characters is faint yellow unformed powdery
Solid, is highly soluble in water, and 10%（Quality）Aqueous solution be rufous clear solution, hygroscopicity.Bodied ferric sulfate is widely used in
The purified treatment of drinking water, water for industrial use, various industrial wastewaters, municipal sewage, sludge dewatering etc..
The preparation of bodied ferric sulfate mainly has direct oxidation method method and catalytic oxidation, the preparation of most of bodied ferric sulfates
Using direct oxidation method, this method process route is simpler, can reduce equipment investment and production link for commercial production, reduces
Equipment cost, but this production technology is necessarily dependent upon oxidant, and reaction unit is that the key core for producing bodied ferric sulfate sets
It is standby, its 3 dominant response：Oxidation reaction, hydrolysis, polyreaction are all carried out wherein, while be present in a system working as
In, influence each other, mutually promote.Particularly react very sensitive, material feed postition, material addition, material add the time,
The various factors such as stirring intensity, gas distribution, reaction temperature, response time have to the effect of polyreaction and the quality of product
Very big impact, but existing reaction unit is unable to effective detection course of reaction, there is provided accurately control.
The content of the invention
Goal of the invention：For the deficiencies in the prior art, this utility model provides a kind of bodied ferric sulfate reaction unit, can
Continuous detection is provided and is controlled.
Technical scheme：Bodied ferric sulfate reaction unit described in the utility model, including reactor and detection pipe, reactor
Top is provided with sulphuric acid charge door, sodium chlorate charge door, hydrogen peroxide charge door, and reactor bottom is provided with discharging opening, reactor bottom land
Incline towards discharging opening, reactor top center is provided with reducing motor, reducing motor and is connected with the agitator in reactor, react
Kettle side wall is provided with several baffle plates, and baffle plate is provided with charge door, is provided with gas distribution tube in reactor, and gas distribution tube is provided with
Air intake and vapour inlet；Reactor bottom liquid is evacuated to detection bucket by detecting pump by detection pipe, is provided with detection bucket
PH is counted, and detection bucket is connected with reactor inner top by return duct.In reactor, the pH value of liquid is with sulphuric acid, addition
Speed, oxidizing process, hydrolytic process and change, arrange detection pipe by reaction liquid continuous pump to detection bucket carry out detection can standard
Really understand reaction process, control course of reaction, detection bucket can also be used as observation slip color, the observation panel of state and sampling
Mouthful.
Further, the baffle plate is 4 groups, is evenly distributed on reactor side wall.In side, wall arranges baffle plate, centrifugal force
Maximum, the speed of acquisition are maximum, are conducive to continuous, uniform, the quick addition reaction of material
Further, the reactor adopts carbon steel material, and wall thickness is 120mm.Using carbon steel material, the applicable longevity is increased
Life, wall thickness is 120mm, with good steadiness.
Further, the reactor bottom land angle of inclination is 3 °.Bottom land inclined design, reaction material liquid energy are enough all arranged
Go out, it is to avoid primary first-order equation under the influence of legacy, improve device efficiency.
Further, the reactor periphery is provided with fixed column, and inner tip is provided with support beam.Fixed column and support are set
Beam can improve equipment steadiness.
Further, the agitator is provided with Dual-layer stirring vane.
Beneficial effect：Compared with prior art, advantage of the present utility model：This utility model design by optimize charging,
Discharging structure, coordinates detection bucket, it is ensured that it is efficient, stable that bodied ferric sulfate reacts, and low cost, operation are controllable, it is ensured that produce
Quality；Maintenance difficult and a continuous-stable feed difficult problem is solved simultaneously, improves Yield and quality and the equipment life of device.
Description of the drawings
Fig. 1 is structural representation of the present utility model.
Specific embodiment
Technical solutions of the utility model are described in detail below by accompanying drawing.
Embodiment 1：Bodied ferric sulfate reaction unit as shown in Figure 1, including reactor 1 and detection pipe 9, reactor 1 is adopted
With carbon steel material, wall thickness is 120mm, and 1 periphery of reactor is provided with fixed column, and inner tip is provided with support beam；Set at the top of reactor 1
There are sulphuric acid charge door 2, sodium chlorate charge door 10, hydrogen peroxide charge door 3,1 bottom of reactor is provided with discharging opening 12,1 groove of reactor
Bottom 11 is inclined towards discharging opening, 11 angle of inclination of bottom land is 3 °, and 1 top center of reactor is provided with reducing motor 1, reducing motor 1
It is connected with the agitator 7 in reactor 1, agitator 7 is provided with Dual-layer stirring vane；1 side wall of reactor is evenly distributed with 4 groups
Individual baffle plate, baffle plate are provided with charge door；Gas distribution tube is provided with reactor 1, gas distribution tube is provided with air intake and steam
Entrance；1 bottom liquid of reactor is evacuated to detection bucket 5 from detection mouth 13 by detecting pump 8 by detection pipe 9, and detection bucket is provided with catalysis
Agent charge door and PH meters 6, detection bucket 5 are connected with 1 inner top of reactor by return duct.In reactor 1 pH value of liquid with
Sulphuric acid, add speed, oxidizing process, hydrolytic process and change, arrange detection pipe by reaction liquid continuous pump to detect
Bucket carries out detection and can accurately understand reaction process, control course of reaction.
Although as described above, having represented and having described this utility model with reference to specific preferred embodiment, which must not
It is construed to the restriction to this utility model itself.In the spirit and scope of the present utility model defined without departing from claims
Under the premise of, can various changes can be made in the form and details to which.
Claims (6)
1. a kind of bodied ferric sulfate reaction unit, it is characterised in that：Including reactor and detection pipe, sulphuric acid at the top of reactor, is provided with
Charge door, sodium chlorate charge door, hydrogen peroxide charge door, reactor bottom are provided with discharging opening, reactor bottom land and incline towards discharging opening
Tiltedly, reactor top center is provided with reducing motor, reducing motor and is connected with the agitator in reactor, and reactor side wall is provided with
Several baffle plates, baffle plate are provided with charge door, are provided with gas distribution tube in reactor, and gas distribution tube is provided with air intake and steaming
Gas entrance；Reactor bottom liquid is evacuated to detection bucket by detecting pump by detection pipe, is provided with PH meters in detection bucket, and detection bucket leads to
Cross return duct to connect with reactor inner top.
2. bodied ferric sulfate reaction unit according to claim 1, it is characterised in that：The baffle plate is 4 groups, is uniformly distributed
In reactor side wall.
3. bodied ferric sulfate reaction unit according to claim 1, it is characterised in that：The reactor adopts carbon steel material
Matter, wall thickness are 120mm.
4. bodied ferric sulfate reaction unit according to claim 1, it is characterised in that：The reactor bottom land angle of inclination
For 3 °.
5. bodied ferric sulfate reaction unit according to claim 1, it is characterised in that：The reactor periphery is provided with fixation
Post, inner tip are provided with support beam.
6. bodied ferric sulfate reaction unit according to claim 1, it is characterised in that：The agitator is provided with Dual-layer
Stirring vane.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620658583.1U CN206033276U (en) | 2016-06-29 | 2016-06-29 | Polyferric sulfate reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620658583.1U CN206033276U (en) | 2016-06-29 | 2016-06-29 | Polyferric sulfate reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206033276U true CN206033276U (en) | 2017-03-22 |
Family
ID=58313086
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620658583.1U Expired - Fee Related CN206033276U (en) | 2016-06-29 | 2016-06-29 | Polyferric sulfate reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206033276U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112108102A (en) * | 2020-10-09 | 2020-12-22 | 马鞍山健鼎化工有限公司 | Novel polymeric ferric sulfate reation kettle |
| CN112110496A (en) * | 2020-09-25 | 2020-12-22 | 安徽工业大学 | Preparation method of polymeric ferric sulfate |
-
2016
- 2016-06-29 CN CN201620658583.1U patent/CN206033276U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112110496A (en) * | 2020-09-25 | 2020-12-22 | 安徽工业大学 | Preparation method of polymeric ferric sulfate |
| CN112108102A (en) * | 2020-10-09 | 2020-12-22 | 马鞍山健鼎化工有限公司 | Novel polymeric ferric sulfate reation kettle |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170322 Termination date: 20170629 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |