CN206027144U - Concentrated crystallizer of even crystallization material - Google Patents
Concentrated crystallizer of even crystallization material Download PDFInfo
- Publication number
- CN206027144U CN206027144U CN201620687738.4U CN201620687738U CN206027144U CN 206027144 U CN206027144 U CN 206027144U CN 201620687738 U CN201620687738 U CN 201620687738U CN 206027144 U CN206027144 U CN 206027144U
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- tank body
- shell
- tank
- cover
- jar body
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Abstract
The utility model provides a concentrated crystallizer of even crystallization material, including jar the body and a cover, be equipped with the breather valve on the cover and access to the nitrogen gas pipe of the internal portion of jar, the top of cover is equipped with agitator motor and supersonic generator, agitator motor is connected with the puddler, the puddler both sides are equipped with ultrasonic vibrator, the institute ultrasonic vibrator with supersonic generator links to each other, the outside of the jar body is equipped with the shell, the shell with be equipped with the steam coil pipe between the jar body, the import of steam coil pipe is located the lower part of shell, the export of steam coil pipe is located the upper portion of shell, the upper portion of the jar body is equipped with to be passed the shell with the inlet pipe of the jar body, the bottom of the jar body is equipped with the discharging pipe, the inside of the jar body is equipped with consistency transmitter, level sensor, temperature sensor and viewing mirror lamp, the upper portion of the jar body is equipped with the sight glass. The utility model discloses the heat transfer is fast, and the temperature and the concentration of jar internal material are even, the high quality of crystallization crystal.
Description
Technical field
This utility model is related to crystallization apparatus field, more particularly to a kind of homogeneously crystallized material condensing crystallizing tank.
Background technology
Crystallization technique be it is a kind of from liquid separate out solid product routine techniquess, be usually applied to various chemical industry, medicine,
In the production in the fields such as biology, such as chemical reagent, medicine, food etc. can be related to crystallization.Crystallization technique can be concentrated
Crystallization or crystallisation by cooling, conventional condensation crystallization method are that solvent is volatilized or evaporated, and make material be changed into saturation from unsaturation, after
Continuous to reduce solvent, superfluous solute will be separated out in crystal, and crystallisation by cooling refers to the reduction of the solubility with temperature of material and drops
It is low, so as to separate out crystal.
During evaporating, concentrating and crystallizing, the concentration of material, temperature and mixing speed have a significant impact to the quality of crystalline solid.
Existing condensing crystallizing tank crystallization time is long, and heat transfer is slow, usually makes as the material stirring in tank is uneven in crystallization process
The concentration and non-uniform temperature of material, cause separate out crystal formation it is not of uniform size, crystal morphology is not good enough, and granule is less, product quality
It is not high, many materials in heating process easily with air in oxygen, the material such as carbon dioxide there is chemical reaction, cause crystal
It is impure, and in evaporative crystallization, the moisture evaporating completely in material in order to avoid affecting the purity of crystal, or can not be caused quick-fried
People around boiling injury.
Utility model content
In view of above-mentioned condition, it is necessary to provide a kind of heat transfer block, the high homogeneously crystallized material condensing crystallizing of crystalline quality
Tank.
A kind of homogeneously crystallized material condensing crystallizing tank, it is including the cover that tank body and the tank body upper end are fastenedly connected, described
Cover is provided with breather valve and leads to the nitrogen tube of the tank interior, is provided with stirring motor and ultrasound wave above the cover
Generator, the stirring motor are connected with puddler, and the puddler both sides are provided with ultrasonic oscillator, the ultrasonic oscillator with
The supersonic generator is connected, and is provided with shell, is provided with steam disc between the shell and the tank body on the outside of the tank body
Pipe, from the bottom part ring of the tank body around the tank body spiral, the import of the steam pipe coil is located at institute to the steam pipe coil
State the bottom of shell, located at the top of the shell, the top of the tank body is provided through described for the outlet of the steam pipe coil
The feed pipe of shell and the tank body, the bottom of the tank body are provided with discharge nozzle, the inside of the tank body be provided with concentration sensor,
Liquid level sensor, temperature sensor and visor lamp, the tank body top are provided with visor.
The utility model proposes a kind of homogeneously crystallized material condensing crystallizing tank, by arrange steam-coil-heater tank body in
Material, heat transfer is fast, homogeneous heating；By arranging ultrasonic stirrer, make material stirring more uniform, be conducive to improving knot
The quality of Jingjing body；The situation of crystal growth is determined by arranging liquid level sensor, concentration sensor and visor, it is ensured that crystallization is anti-
That what is answered is smoothed out, and can be passed through nitrogen in obtaining uniform in size and pattern preferably crystal, and crystallization process, it is to avoid material is sent out
Biochemical reaction.
Above-mentioned homogeneously crystallized material condensing crystallizing tank, wherein, the inwall of the tank body is corrugated.
Above-mentioned homogeneously crystallized material condensing crystallizing tank, wherein, the import of the steam pipe coil is provided with for controlling steam stream
The control valve that amount and steam are entered,
Above-mentioned homogeneously crystallized material condensing crystallizing tank, wherein, the shell is externally provided with heat-insulation layer.
Description of the drawings
Fig. 1 is the structural representation of the homogeneously crystallized material condensing crystallizing tank that this utility model first embodiment is proposed；
Fig. 2 is the structural representation of the homogeneously crystallized material condensing crystallizing tank that this utility model second embodiment is proposed；
Fig. 3 is the structural representation of the homogeneously crystallized material condensing crystallizing tank that this utility model 3rd embodiment is proposed；
Fig. 4 is the structural representation of the homogeneously crystallized material condensing crystallizing tank that this utility model fourth embodiment is proposed.
Main element symbol description
Specific embodiment
For the ease of understanding this utility model, this utility model is more fully retouched below with reference to relevant drawings
State.This utility model embodiment is given in accompanying drawing.But, this utility model can be realized in many different forms, and
It is not limited to embodiment described herein.On the contrary, the purpose for providing the embodiment is made to disclosure of the present utility model
It is more thorough comprehensive.
It should be noted that when element is referred to as " being fixedly arranged on " another element, it can directly on another element
Or can also there is element placed in the middle.When an element is considered as " connection " another element, it can be directly connected to
To another element or may be simultaneously present centering elements.Term as used herein " vertical ", " level ", " left side ",
" right side " and similar statement are for illustrative purposes only.
Unless otherwise defined, all of technology used herein and scientific terminology are led with technology of the present utility model is belonged to
The implication that the technical staff in domain is generally understood that is identical.In term used in the description of the present utility model it is simply herein
The purpose of description specific embodiment, it is not intended that in limiting this utility model.Term as used herein " and/or " include
The arbitrary and all of combination of one or more related Listed Items.
Fig. 1 is referred to, a kind of homogeneously crystallized material condensing crystallizing tank that this utility model first embodiment is proposed, including tank
The cover 2 that body 1 and 1 upper end of tank body are fastenedly connected.The cover 2 is provided with breather valve 3 and the nitrogen tube 4 led to inside tank body 1,
The inside of tank body 1 is provided with concentration sensor 9, liquid level sensor 10, temperature sensor 12 and visor lamp 111.Tank body 1 is provided with and stirs
Device is mixed, the agitator includes puddler 6, paddle 7 and stirring motor 5.Puddler 6 is located at the inside of tank body 1, paddle 7
Located at the both sides of puddler 6, puddler 6 is connected with the stirring motor 5 of 2 upper end of cover.1 top of tank body is additionally provided with visor 11, institute
The top that visor 11 and visor lamp 111 are located at material liquid surface is stated, the visor 11 is used for observing the crystallization feelings of 1 materials inside of tank body
Condition.
The outside of the tank body 1 is provided with shell 13, and the top of tank body 1 is provided through 1 tank of the shell 13 and the tank body
The feed pipe 14 of wall, the bottom of tank body 1 are provided with discharge nozzle 15.
Heater is provided between the shell 13 and tank body 1, and the heat transfer that the heater is produced is in tank body 1
Material, by material condensing crystallizing.Heater described in the present embodiment is heated using steam.Between shell 13 and tank body 1
Steam pipe coil 16 is set, steam pipe coil 16 from the bottom part ring of the tank body 1 around 1 spiral of the tank body, steam pipe coil 16
Located at the bottom of the shell 13, the outlet of steam pipe coil 16 is located at the top of the shell 13 for import.16 import of steam pipe coil
It is provided with for controlling the control valve that steam flow and steam are entered.
When being embodied as, the solvent in material is evaporated by the heat transfer in steam pipe coil 16 to the material in tank body 1.
Start to separate out crystal when material reaches saturated concentration, when continuing heating, crystal is constantly separated out.But during evaporating, concentrating and crystallizing, no
Solvent evaporating completely in material in order to avoid affecting the purity of crystal, or can be caused bumping.Material is detected by liquid level sensor
Liquid level, can tentatively judge the situation of liquid evaporation, then be observed by visor 11, when material concentrated solution occur a large amount of crystal when,
Stop heating, natural cooling makes remaining liq volatilize and can obtain crystal.
The inwall of the tank body 1 is corrugated, to increase the heating surface area of material.The shell 13 is externally provided with heat-insulation layer,
Reduce heat losses.
Refer to Fig. 2, a kind of homogeneously crystallized material condensing crystallizing tank that this utility model second embodiment is provided, which is with the
The one homogeneously crystallized material condensing crystallizing jar structure basic simlarity for implementing proposition, difference are to stir in the present embodiment
Device increased the function of ultrasonic stirring, and the agitator includes puddler 6a, stirring motor 5a, supersonic generator 8 and ultrasound
Ripple oscillator 81.Stirring motor 5a and supersonic generator 8 are located at the top of cover 2, and ultrasonic oscillator 81 is positioned at puddler 6a's
Both sides, ultrasonic oscillator 81 are connected with supersonic generator 8.Corresponding to this, second embodiment of the present utility model is relative to
One embodiment eliminates paddle.In the present embodiment, electric rotating machine promotes ultrasonic oscillator to rotate, so as to stir material, but also
Supersonic generator is provided with, makes material stirring more uniform, promote crystal quickly and evenly to grow.
Refer to Fig. 3, a kind of homogeneously crystallized material condensing crystallizing tank that this utility model 3rd embodiment is provided, which is with the
The one homogeneously crystallized material condensing crystallizing jar structure basic simlarity for implementing proposition, difference is, described in the present embodiment
Heater is heated using resistive heater, arranges resistive heater 17, be provided with tank body 1 between shell 13 and tank body 1
Heating controller, the heating controller are connected with temperature sensor 12 and resistive heater 17.When temperature sensor 12 is detected
When temperature in tank body 1 is less than preset value, controller control resistive heater 17 is heated, and when preset temperature is heated to, is kept
Constant temperature.Heating-up temperature constant in tank body 1 is kept in crystallization process, makes material condensing crystallizing uniform.
Refer to Fig. 4, a kind of homogeneously crystallized material condensing crystallizing tank that this utility model fourth embodiment is provided, which is with the
The one homogeneously crystallized material condensing crystallizing jar structure basic simlarity for implementing proposition, difference is, described in the present embodiment
Heater is heated using resistive heater, and agitator increased the function of ultrasonic stirring.Shell 13 and tank body 1 it
Between resistive heater 17b is set, be provided with heating controller on tank body 1, the heating controller and temperature sensor 12 and heating
Resistance wire 17b is connected.When the temperature in temperature sensor 12 detects tank body 1 is less than preset value, controller control heating electricity
The 17b heating of resistance silk, keeps heating-up temperature constant in tank body 1, makes material condensing crystallizing uniform.Agitator bag in the present embodiment
Include puddler 6b, stirring motor 5b, ultrasonic oscillator 81b and supersonic generator 8b.Stirring motor 5b and supersonic generator
8b is located at the top of cover 2, and ultrasonic oscillator 81b is positioned at the both sides of puddler 6b, ultrasonic oscillator 81b and supersonic generator
8b is connected.In the present embodiment, by arranging controller, constant heating-up temperature is kept in control tank body, by ultrasound wave to material
It is stirred, makes material stirring uniform, promotes crystal quickly and evenly to grow.
Embodiment described above only expresses embodiment of the present utility model, and its description is more concrete and detailed, but and
Therefore the restriction to this utility model the scope of the claims can not be interpreted as.It should be pointed out that for the ordinary skill of this area
For personnel, without departing from the concept of the premise utility, some deformations and improvement can also be made, these belong to this
The protection domain of utility model.Therefore, the protection domain of this utility model patent should be defined by claims.
Claims (3)
1. a kind of homogeneously crystallized material condensing crystallizing tank, including the cover that tank body and the tank body upper end are fastenedly connected, the tank
Cover the nitrogen tube for being provided with breather valve He leading to the tank interior, it is characterised in that above the cover, be provided with stirring electricity
Machine and supersonic generator, the stirring motor are connected with puddler, and the puddler both sides are provided with ultrasonic oscillator, described super
Acoustic wave transducer is connected with the supersonic generator, is provided with shell, sets between the shell and the tank body on the outside of the tank body
There is a steam pipe coil, from the bottom part ring of the tank body around the tank body spiral, the steam pipe coil enters the steam pipe coil
Located at the bottom of the shell, located at the top of the shell, the top of the tank body is provided with mouth for the outlet of the steam pipe coil
Through the shell and the feed pipe of the tank body, the bottom of the tank body is provided with discharge nozzle, and the inside of the tank body is provided with dense
Degree sensor, liquid level sensor, temperature sensor and visor lamp, the top of the tank body is provided with visor, the inwall of the tank body
It is corrugated.
2. homogeneously crystallized material condensing crystallizing tank as claimed in claim 1, it is characterised in that the import of the steam pipe coil sets
Have for controlling the control valve that steam flow and steam are entered.
3. homogeneously crystallized material condensing crystallizing tank as claimed in claim 1, it is characterised in that the shell is externally provided with insulation
Layer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620687738.4U CN206027144U (en) | 2016-07-02 | 2016-07-02 | Concentrated crystallizer of even crystallization material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620687738.4U CN206027144U (en) | 2016-07-02 | 2016-07-02 | Concentrated crystallizer of even crystallization material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206027144U true CN206027144U (en) | 2017-03-22 |
Family
ID=58310226
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620687738.4U Expired - Fee Related CN206027144U (en) | 2016-07-02 | 2016-07-02 | Concentrated crystallizer of even crystallization material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206027144U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107961557A (en) * | 2017-10-24 | 2018-04-27 | 湖北民族学院 | The apparatus and method of rapid crystallization of biomolecules |
-
2016
- 2016-07-02 CN CN201620687738.4U patent/CN206027144U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107961557A (en) * | 2017-10-24 | 2018-04-27 | 湖北民族学院 | The apparatus and method of rapid crystallization of biomolecules |
| CN107961557B (en) * | 2017-10-24 | 2020-03-17 | 湖北民族大学 | Apparatus and method for rapid crystallization of biomolecules |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170322 Termination date: 20180702 |