CN206014935U - The equipment of manufacture Structure grease - Google Patents

The equipment of manufacture Structure grease Download PDF

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Publication number
CN206014935U
CN206014935U CN201621039497.9U CN201621039497U CN206014935U CN 206014935 U CN206014935 U CN 206014935U CN 201621039497 U CN201621039497 U CN 201621039497U CN 206014935 U CN206014935 U CN 206014935U
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China
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reaction
reaction unit
equipment
blending tank
discharging opening
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CN201621039497.9U
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Chinese (zh)
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李翔宇
汪志明
杨刚
陆姝欢
周强
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Limited By Share Ltd Biotechnology (wuhan) Co Ltd
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Limited By Share Ltd Biotechnology (wuhan) Co Ltd
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Abstract

The equipment of manufacture Structure grease includes blending tank, and the blending tank is provided with charging aperture, air inlet and discharging opening;Reaction unit, the reaction unit include being filled with 1,3 specific lipases at least 2 reaction columns, at least 2 reaction columns;The discharging opening of at least 2 reaction columns is connected with threeway, and the one outlet of the threeway is connected with sampling valve;The reaction unit is connected by conduit assembly with the discharging opening;Collection device, the collection device are connected with the discharge end of the reaction unit.This utility model is connected using reaction of high order post, monitors the activity of enzyme in reaction column by the sampling valve timing sampling of threeway, so as to the order of connection of reasonable adjusting reaction column, improves the yield of OPO Structure greases, reduces cost.

Description

The equipment of manufacture Structure grease
Technical field
This utility model is related to a kind of equipment of manufacture Structure grease, especially a kind of equipment of manufacture OPO structured lipids.
Background technology
Main oils and fatss composition of the triglyceride for human consumption.Modern nutriology has confirmed that human body is in devils brew three During ester, can selective hydrolysis Sn-1, the fatty acid on 3, formation β-monoglyceride and substantial amounts of free fatty.These trips Two kinds of reactions occur in human body from fatty acid:1st, by own absorption;2 and it is discharged after other substance reactions in vivo.Research Show, compared with free unsaturated fatty acid, satisfied fatty acid absorption rate of dissociating is slow, it is easier to react with calcium, is formed Insoluble soap calcium, and then be excreted.As can be seen here, relative to the triglyceride for producing free satisfied fatty acid, produce The triglyceride of free unsaturated fatty acid is more conducive to the absorption of human body.Presently commercially available edible oil is mainly derived from plant, its Satisfied fatty acid is mainly distributed on sn-1,3, and human body lost substantial amounts of fat and calcium, Er Qieqi in digestion process, not only The soap calcium of generation can increase the hardness of feces, cause part population constipation and stomachache, or even cause intestinal obstruction.If by saturated fat Acid concentrates on the sn-2 positions of triglyceride(Also referred to as " β positions "), then can effectively solving this problem, empty especially for body Weak, for the bad individuality of gastrointestinal function, effect becomes apparent from.
In breast milk, 98% or so fat in the form of triglyceride, wherein Palmic acid(Palmitic acid, C16:0, satisfied fatty acid)Content account for 20-25%, Oleic acid(Oleic acid, C18:1, unsaturated fatty acid)Content is accounted for 30-38%.Further, most Palmic acid is distributed in the β positions of triglyceride, and Oleic acid be then mainly distributed on Sn-1 and On Sn-3 positions, in breast milk, this unique triglyceride structure is referred to as OPO structured lipids.At present, the baby formula on market The component content of milk powder and breast milk relatively, but, substantial amounts of experiment has confirmed that, the absorption of human milk fat is better than infant Formula milk, one of major reason are that in breast milk and contain substantial amounts of OPO structured lipids.
Inspired by this, had part manufacturer at present using producing OPO structured lipids to the modification of natural oil, and by its It is added in baby milk powder or special diet, this can not only improve human body to fat and the absorption efficiency of calcium, moreover it is possible to reduce The hardness of feces, reduces constipation and ileac probability of happening.
It is raw material using Adeps Sus domestica that Chinese granted patent CN102229866B is disclosed a kind of, adopts 1,3 regioselectivity fat Fat enzyme catalysiss acidolysis process, prepares low cholesterol, the process of high OPO structures oil/fat composition.But lard component is complicated, Preparation equipment is more complicated, and manufacturing cost is also higher.
Chinese granted patent CN104099240B disclose a kind of manufacture structure oil fat standby, using single-column fill 1,3 Put selected fat enzyme to be reacted, the process of OPO structure oil/fat compositions is obtained.But single-column reaction column enzyme amount fills great talent The OPO of qualified content can be reached, short circuit is easily caused, material is contacted with enzyme not enough fully, and the utilization rate to enzyme is not high, and yield is not Enough height, due to the price expensive of enzyme, directly influence production cost.This patent further referred in an embodiment, can be with By some reaction column series, parallel or mixing connection in series-parallel, but, when being connected using multiple reaction columns, enzyme in each reaction column Utilization rate differ.Under normal circumstances, in the reaction column of charging aperture, the utilization rate of enzyme is higher, and near receipts In the reaction column of collection tank, than relatively low, this scheme still can increase manufacturing cost, and cause the wasting of resources for the utilization rate of enzyme.
Therefore, there is still a need for providing a kind of equipment of improved manufacture Structure grease.
Content of the invention
The purpose of this utility model is to provide a kind of simple structure, the equipment of manufacture Structure grease with low cost.
For achieving the above object, the equipment of manufacture Structure grease of the present utility model includes:Blending tank, on the blending tank It is provided with charging aperture, air inlet and discharging opening;Reaction unit, the reaction unit include at least 2 reaction columns, described at least 2 1,3 specific lipases are filled with reaction column;The discharging opening of at least 2 reaction columns is connected with threeway, the threeway One outlet is connected with sampling valve;The reaction unit is connected by conduit assembly with the discharging opening;Collection device, the receipts Acquisition means are connected with the discharge end of the reaction unit.
The equipment of manufacture Structure grease of the present utility model has the advantages that:Connected using reaction of high order post, led to Cross the sampling valve timing sampling of threeway to monitor the activity of enzyme in reaction column, so as to the order of connection of reasonable adjusting reaction column, can To ensure that 1,3 specific reaction enzymes are fully utilized in each reaction column, so as to improve the yield of OPO Structure greases, reduce into This, reduces the waste of resource.
Further, blending tank and collecting tank are designed with logical air inlet, for being passed through nitrogen, so as to protect compound lard not Oxidized, prevent the activity of 1,3 specific reaction enzymes from reducing or even lossing.
Description of the drawings
Fig. 1 is the equipment workflow schematic diagram that this utility model manufactures Structure grease.
Specific embodiment
Referring to Fig. 1, the equipment for manufacturing Structure grease mainly includes mixing arrangement, reaction unit and collecting tank.The present embodiment In, mixing arrangement includes:Blending tank 1, the blending tank 1 are provided with thermometer 61 with chuck temperature regulating device 2 on temperature regulating device 2, It is used for the temperature for adjusting and controlling blending tank 1.1 upper end of blending tank is provided with charging aperture 81 and air inlet 71, and bottom is provided with discharging opening 91.Hard Fat can will be reset by charging aperture 81 and oleic acid mixture is added in blending tank 1, air inlet 71 is used for being passed through nitrogen. Agitating device is connected with blending tank 1, and the agitating device includes the electric rotating machine 41 being fixed on tank body and stretches into stirring for blending tank 1 Mix blade 31.Discharging opening 91 passes through globe valve 92, the first pipeline 10, gear pump 11 and second pipe 12(It is collectively referred to as conduit assembly) It is delivered to reaction unit.Reaction unit includes:4 reaction columns being sequentially connected in series(141,142,143,144), reaction column(141, 142,143,144)1,3 specific reaction enzymes of interior filling.Reaction column(141,142,143,144)Pressure gauge is housed(51,52,53, 54), for monitoring the post pressure of reaction column, judged in post in time with the presence or absence of abnormal conditions such as blockings.Reaction column(141,142, 143,144)Charging aperture be provided with valve module(131,132,133,134), reaction column(141,142,143,144)Discharging opening with Threeway(171,172,173,174)Connection.Threeway(171,172,173,174)One outlet and sampling valve(181,182, 183,184)Connection.Blending tank 1 is connected with reaction unit by the first pipeline 10, gear pump 11, second pipe 12.Reaction unit It is integrally placed at calorstat(Not shown in figure)In, to ensure which maintains stationary temperature, the discharge end of reaction unit and collection Tank 21 connects, and the structure of collecting tank is identical with blending tank 1.
The technological process for preparing OPO Structure greases using this equipment further explained below.First, by commercially available shortening The oils and fatss that ester exchange obtains rich in three ester of palmitic acid are carried out with Palmic acid, the step is by the equipment system beyond this utility model ?.Secondly, by the aforementioned obtained oils and fatss rich in three ester of palmitic acid and Oleic acid according to 1:Blending tank of 3 weight than loading In 1, start agitating device, while being heated to blending tank 1 by temperature regulating device 2, and temperature control is made rich in Petiolus Trachycarpi at 60 DEG C Acid glycerol three ester forms uniform liquefied mixture with Oleic acid.Calorstat 20 is opened, it is 60 DEG C to arrange temperature.Starter receiver pump 11, the liquefied mixture in blending tank 1 is delivered in reaction unit by globe valve 92, the first pipeline 10, second pipe 12. Liquefied mixture and 4 grades of cascade reaction posts(141,142,143,144)In 1,3 specific reaction enzymes fully react after, enter Collecting tank 21.Product in collecting tank 21 is the mixture containing Oleic acid, Palmic acid and OPO structured lipids.Subsequently through conventional deacidification Technique, such as molecular distillation, remove the Oleic acid in mixture and Palmic acid, that is, OPO Structure greases are obtained.Actual production process In, periodically pass through sampling valve(181,182,183,184)Sampling, detects reaction column(141,142,143,144)Discharge hole for discharge OPO contents in thing, determine whether reaction column(141,142,143,144)In 1,3 specific reaction enzymes activity, usual feelings Under condition, the activity decrease of 1,3 specific reaction enzymes in the reaction column 141 of charging aperture is most fast, is reacted by reasonable adjusting Post(141,142,143,144)Order, it is ensured that reaction column(141,142,143,144)1,3 specific reaction enzyme quilts Make full use of, so as to improve the yield of OPO Structure greases.Blending tank 1 and collecting tank 21 are designed with logical air inlet 71,72, are used for Nitrogen is passed through, so as to protect compound lard not oxidized, prevents the activity of 1,3 specific reaction enzymes from reducing or even lossing.
In the equipment of this utility model manufacture Structure grease, the quantity of reaction column is at least 2, and is serially connected, and passes through The regulation of order during use, can improve the utilization rate of 1,3 specific lipases.
The equipment of this utility model manufacture Structure grease is not limited to manufacture OPO Structure greases, can be also used for manufacturing DHA types Phospholipid, ARA type phospholipid isostructuralism oils and fatss.

Claims (4)

1. the equipment of Structure grease is manufactured, it is characterised in that:Including
Blending tank, the blending tank are provided with charging aperture, air inlet and discharging opening;The blending tank carries temperature regulating device;
Reaction unit, the reaction unit include being filled with 1,3 specificitys at least 2 reaction columns, at least 2 reaction columns Digestive Enzyme, the discharging opening of at least 2 reaction columns are connected with threeway, and the one outlet of the threeway is connected with sampling valve, institute State reaction unit to connect by conduit assembly with the discharging opening, the reaction unit is put and is integrally placed in calorstat;
Collection device, the collection device are connected with the discharge end of the reaction unit.
2. according to claim 1 manufacture Structure grease equipment, it is characterised in that:The reaction column is equipped with pressure gauge.
3. according to claim 1 manufacture Structure grease equipment, it is characterised in that:The conduit assembly includes spherical Valve, the first pipeline, gear pump and second pipe.
4. according to claim 1 manufacture Structure grease equipment, it is characterised in that:The collection device is provided with air inlet Mouthful.
CN201621039497.9U 2016-09-06 2016-09-06 The equipment of manufacture Structure grease Active CN206014935U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621039497.9U CN206014935U (en) 2016-09-06 2016-09-06 The equipment of manufacture Structure grease

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621039497.9U CN206014935U (en) 2016-09-06 2016-09-06 The equipment of manufacture Structure grease

Publications (1)

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CN206014935U true CN206014935U (en) 2017-03-15

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CN201621039497.9U Active CN206014935U (en) 2016-09-06 2016-09-06 The equipment of manufacture Structure grease

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114403948A (en) * 2022-01-10 2022-04-29 烟台美神科美医疗美容门诊部有限公司 Increase autologous fat transplantation equipment of adipocyte survival rate
CN118126822A (en) * 2024-05-07 2024-06-04 南昌大学 Continuous synthesis equipment and synthesis process of breast milk structural lipid analogue

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114403948A (en) * 2022-01-10 2022-04-29 烟台美神科美医疗美容门诊部有限公司 Increase autologous fat transplantation equipment of adipocyte survival rate
CN118126822A (en) * 2024-05-07 2024-06-04 南昌大学 Continuous synthesis equipment and synthesis process of breast milk structural lipid analogue
CN118126822B (en) * 2024-05-07 2024-09-13 南昌大学 Continuous synthesis equipment and synthesis process of breast milk structural lipid analogue

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