CN202496368U - Preparation equipment for food grade composite phospholipids rich in VE and sterol - Google Patents
Preparation equipment for food grade composite phospholipids rich in VE and sterol Download PDFInfo
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- CN202496368U CN202496368U CN2011205333027U CN201120533302U CN202496368U CN 202496368 U CN202496368 U CN 202496368U CN 2011205333027 U CN2011205333027 U CN 2011205333027U CN 201120533302 U CN201120533302 U CN 201120533302U CN 202496368 U CN202496368 U CN 202496368U
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Abstract
The utility model provides preparation equipment for food grade composite phospholipids rich in VE and sterol. The preparation equipment comprises a saponification purification device, a phospholipid purification device and a mixing purification device, wherein the outlet of a climbing film evaporator 1 (10) of the saponification purification device and the outlet of a stripping tower 1 (21) of the phospholipid purification device are communicated with the inlet of a mixing tank 3 (22) of the mixing purification device. Phosphatide products contain phospholipids, the VE and the sterol, and the VE and the sterol are from deodorization distillates produced in a deodorization procedure in the plant crude oil refining process, so that by-products produced in the deodorization procedure are better utilized.
Description
Technical field
The utility model relates to food or feed manufacturing machine field, especially relates to a kind of V of being rich in
EPreparation equipment with the food-grade composite phospholipid of sterol.
Technical background
V
EBeing tocopherol again, is a kind of natural in the vegetable oil, not only can improve the oxidation stability of grease; But also has certain medical care effect; Can guarantee the normal operation of function of human body, prevent human senility and artery sclerosis, reduce the incidence of disease of angiocardiopathy.
Sterol is the mixture of multiple sterol; Mainly be stigmasterol, cupreol, campesterol and brassicasterol etc.; Wherein sitosterol is one type of material with biological value; Through the synthetic metabolism of regulating water, protein, sugar and salt, can reduce the concentration of human serum cholesterol, the effect of prevention of arterial sclerosis is arranged.
Phosphatide is a kind of phosphorous lipid material; Mainly form by lecithin, cephalin, lipositol; It is the main component that constitutes lipoid in the biomembrane, can improve nerve fiber, improve the brain vigor, and hypertension, heart disease and cranial vascular disease are had prevention and therapeutic action.
Deodorization distillate is a kind of accessory substance that the deodorization procedures of plant crude oil in refining process produces.Be rich in V in the deodorization distillate
EAnd sterol, the oil foot that produces that comes unstuck can obtain concentrated phosphatide through processed, and grease production enterprise often directly sells single products such as deodorization distillate and concentrated phosphatide at present, and the product that these two kinds of nutriments are organically combined is not arranged.
The utility model content
The purpose of the utility model provides a kind of preparation equipment of food-grade composite phospholipid, contains phosphatide, V in the said phospholipid prod
EAnd sterol, V wherein
EWith sterol be the deodorization distillate that deodorization procedures produced that comes from the plant crude oil refining process.Accessory substance with the generation of better utilization deodorization procedures.
In order to achieve the above object, the technical scheme of the utility model employing is:
A kind of preparation equipment of food-grade composite phospholipid, to be used for suitability for industrialized production, it comprises saponification purifying plant, phosphatide purification devices and mixes purifying plant;
Said saponification purifying plant comprises the saponification jar that connects through gear pump successively, blending tank one, extract and separate jar; Bag filter one, film filter one, temporary jar one; Heater one, falling film evaporator one, heater two; With climbing film evaporator one, wherein between said blending tank one and extract and separate jar, also be provided with heat exchanger two;
Said phosphatide purification devices comprises the blending tank two that connects through gear pump successively, bleacher, bag filter two, film filter two, temporary jar two, heater three, falling film evaporator two, heater four, climbing film evaporator two, heater five, stripper one;
Said mixing purifying plant comprises the blending tank three that connects through pump successively, stripper two, and vacuum column, heater six, thin film evaporator, heat exchanger one, wherein blending tank three, and stripper two, the pump that connects between the vacuum column are gear pump; Heater six, thin film evaporator, the pump that connects between the heat exchanger one is a screw pump;
The outlet of the climbing film evaporator one of said saponification purifying plant is communicated to the said inlet that mixes the blending tank three of purifying plant with the outlet of the stripper one of said phosphatide purification devices.
Above-mentioned preparation equipment, the inlet of wherein said extract and separate jar is arranged on the middle and lower part of tank body, is provided with the n-hexane pans at the middle part, inside of tank body; The tank body bottom of extract and separate jar is provided with fluid level control device.After n-hexane, water and saponified completion mix, get into the extract and separate jar from extract and separate jar middle part, because n-hexane and water do not dissolve each other, the layering in the extract and separate jar of n-hexane and water, n-hexane is on the upper strata.When the n-hexane liquid level reached n-hexane pans mouth, n-hexane got into the hexane pans, realized separating of n-hexane and water.Through from extract and separate jar underfeed and the n-hexane pans are set, can farthest reduce the moisture that n-hexane has, alleviate the load of back thin film evaporator, improve extraction efficiency.The extract and separate jar is provided with fluid level control device, and when the liquid level of water in the extract and separate jar reached setting height, the valve of extract and separate jar bottom was opened automatically, and the water that will contain soap is discharged into temporary jar of soap lye.
In order to prolong the service time of film filter in the production process, the bag type filtering apparatus is set before film filter, this device can be removed partial impurities in advance, alleviates the production load of back film filter.
Utilize the preparation equipment of the utility model to prepare a kind of V of being rich in
EWith the food-grade composite phospholipid of sterol, the V in the wherein said composite phospholipid
EDerive from the deodorization distillate of vegetable oil with sterol.Said deodorization distillate is the deodorization distillate that deodorization procedures produced in the plant crude oil refining process, and it contains V
EAnd sterol, it is carried out adding in the phosphatide of back after certain processing, be prepared into composite phospholipid, not only new phospholipid prod can be provided, reduce the production cost of phospholipid prod; Can also make full use of the accessory substance of deodorization procedures, make full use of resource.Phosphatide wherein can be the phosphatide of any product form; Be preferably feed phosphatide, can reduce product cost.Wherein be used to provide V
EWith the deodorization distillate of the vegetable oil of sterol can be each vegetable oil of industrialization commonly used, like soybean oil, sunflower seed oil, palm oil and coconut wet goods, deodorization procedures is arranged all in its production process, resulting deodorization distillate all can use.
Description of drawings
Fig. 1 is that the utility model is rich in V
EPreparation equipment drawing with the food-grade composite phospholipid of sterol;
Fig. 2 is the structural representation of extract and separate jar 3 among the embodiment.
The specific embodiment
For further specifying the utility model, specify in conjunction with following examples:
V is rich in the preparation of using among the following embodiment
EAs shown in Figure 1 with the preparation equipment of the food-grade composite phospholipid of sterol, capital equipment has saponification jar 1, blending tank 1, extract and separate jar 3, bag filter 1, film filter 1; Temporary jar 1, heater 1, falling film evaporator 1, heater 29, climbing film evaporator 1, blending tank 2 11; Bleacher 12, bag filter 2 13, film filter 2 14, temporary jar 2 15, heater 3 16, falling film evaporator 2 17; Heater 4 18, climbing film evaporator 2 19, heater 5 20, stripper 1, blending tank 3 22, stripper 2 23; Vacuum column 24, heater 6 25, thin film evaporator 26, heat exchanger 1, heat exchanger 2 40.
It can be divided into three parts, is respectively saponification purifying plant, phosphatide purification devices and mixes purifying plant;
Said saponification purifying plant comprises the saponification jar 1 that connects through gear pump successively, blending tank 1, extract and separate jar 3; Bag filter 1, film filter 1, temporary jar 1; Heater 1, falling film evaporator 1, heater 29; With climbing film evaporator 1, wherein between said blending tank 1 and extract and separate jar 3, also be provided with heat exchanger 2 40; Be used for the deodorization gold-plating go out after the thing saponification will be wherein aliphatic acid and V
EWith separate after the sterol extraction, to obtain V
EWith the sterol bullion;
Blending tank 1 is equipped with agitating device, and whipping process is to carry out through the overflow mode of low in and high out;
There are n-hexane pans 31 extract and separate jar 3 inside, can realize separating of n-hexane and water to greatest extent, reduce the moisture in the n-hexane, alleviate the load of back thin film evaporator;
Said phosphatide purification devices comprises the blending tank 2 11 that connects through gear pump successively, bleacher 12, bag filter 2 13, film filter 2 14; Temporary jar 2 15, heater 3 16, falling film evaporator 2 17, heater 4 18; Climbing film evaporator 2 19, heater 5 20, stripper 1; It is used for obtaining the phosphatide bullion behind the feed phosphatide purifying, to meet the final products needs;
Said mixing purifying plant comprises the blending tank 3 22 that connects through pump successively, stripper 2 23, and vacuum column 24, heater 6 25, thin film evaporator 26, heat exchanger 1, wherein blending tank 3 22, stripper 2 23, the pump that connects between the vacuum column 24 is a gear pump; Heater 6 25, thin film evaporator 26, the pump that connects between the heat exchanger 1 is a screw pump; The outlet of the climbing film evaporator 1 of said saponification purifying plant is communicated to the said inlet that mixes the blending tank 3 22 of purifying plant with the outlet of the stripper 1 of said phosphatide purification devices.It is used for V that the front is obtained
EFurther purify again after mixing with sterol bullion and phosphatide bullion, to obtain the composite phospholipid of ultimate food level.
At heater 7,9,16,18,20,25, falling film evaporator 8,17, climbing film evaporator 10,19, stripper 21,23, vacuum column 24, insulation material is equipped with in thin film evaporator 26 outsides, makes device that effect of heat insulation preferably arranged.
The engineering goods great majority that use in the said equipment can be buied from the market, perhaps carry out small improvement through the product that the market is buied and get final product.
With a kind of concrete implementation method is example, and the method for using of the preparation equipment of the utility model is described:
After measuring the soybean oil deodorizer distillate acid value; With soybean oil deodorizer distillate and concentration is 25%; Addition be 60% sodium hydroxide solution after pipeline is accomplished premix, in saponification jar 1, carrying out saponification under 52 ℃ the condition, remove the aliphatic acid in the deodorization distillate.In blending tank 1, add n-hexane and water (volume of n-hexane and water is 1: 1.6) in the solution after saponification, be under 52 ℃ the condition, to extract sterol, V respectively in temperature
EAnd soap.Contain sterol, V
EHexane solution and the aqueous solution that contains soap at 26 ℃ of temperature (through heat exchanger 2 40), flow velocity 6m
3Advance extract and separate jar 3 under the condition of/h, through demixing, and n-hexane is on the upper strata, and water is realized the separation of soap in lower floor.Contain sterol, V after the separation
EHexane solution under 0.43bar pressure, advance bag filter 1, under 0.36bar pressure, advance film filter 1, remove the impurity that contains.Contain sterol, V then
EHexane solution heater via 1 be heated to 68 ℃ after, advance falling film evaporator 1, be 400mmbar in vacuum, remove the part n-hexane under the condition of time 12min.What go out falling film evaporator 1 contains sterol, V
EN-hexane mixture heater via 29 be heated to 112 ℃ of laggard climbing film evaporators 1, be 206mmbar in vacuum, further remove n-hexane under the condition of time 15min.Obtain sterol and V
EBullion.
After feed phosphatide and n-hexane advance blending tank 2 11 and mix, under 53 ℃ condition, in bleacher 12,, remove the pigment that phosphatide contains through hydrogen peroxide solution (the hydrogen peroxide solution addition is 3.5%, bleaching time 55min) effect.The phosphatide that decolours then advances bag filter 2 13 under 0.42bar pressure, under 0.35bar pressure, advance film filter 2 14, removes impurity.After phosphatide heater via 3 16 after the purification is heated to 68 ℃, advancing falling film evaporator 2 17, is 400mmbar in vacuum, removes the part n-hexane in the phosphatide under the condition of time 12min.After going out falling film evaporator 2 17, phosphatide and n-hexane mixture heater via 4 18 are heated to 123 ℃ of laggard climbing film evaporators 2 19, are 306mmbar in vacuum, further remove the n-hexane in the phosphatide under the condition of time 16min.Going out the phosphatide heater via 5 20 laggard strippers 1 behind the climbing film evaporator 2 19, is 206mmbar in vacuum, removes n-hexane remaining in the phosphatide under the condition of time 13min.Obtain the phosphatide bullion.
The sterol that obtains, V
EBullion and phosphatide bullion advance blending tank 3 22, are after mixing under the condition of 206mmbar in vacuum, admission stripper 2 23, and be 105mmbar in vacuum, remove n-hexane and part moisture under the condition of stripping time 12min.The composite phospholipid that goes out stripper 2 23 is to advance vacuum column 24 under the 100mmbar condition in vacuum, is residual solvent and the part moisture of further removing in the 8min in the product in the time.After composite phospholipid heater via 6 25 is heated to 123 ℃ then, advancing thin film evaporator 26, is 108mmbar in vacuum, removes the moisture in the product under the condition of time 7min.Contain sterol, V at last
EPhosphatide complexes cooled to 40 ℃ through heat exchanger 1, and get into the composite phospholipid tank stores.
Detect the compound index, the result is following, acetone insoluble matter content: 62.9%, and sterol content: 123.6g/kg, V
EContent: 88.1g/kg, color and luster, Gardner:8, moisture: 0.35%, acid value: 20.2mgKOH/g, residual solvent: 3.2mg/kg, As:1.3mg/kg, peroxide value: 8.9meq/kg.
Claims (1)
1. one kind is rich in V
EPreparation equipment with the food-grade composite phospholipid of sterol is characterized in that: comprise saponification purifying plant, phosphatide purification devices and mix purifying plant;
Said saponification purifying plant comprises the saponification jar (1) that connects through gear pump successively, blending tank one (2), extract and separate jar (3); Bag filter one (4), film filter one (5), temporary jar one (6); Heater one (7), falling film evaporator one (8), heater two (9); With climbing film evaporator one (10), wherein between said blending tank one (2) and extract and separate jar (3), also be provided with heat exchanger two (40); The inlet of said extract and separate jar (3) is arranged on the middle and lower part of extract and separate tank, is provided with n-hexane pans (31) at the middle part, inside of extract and separate tank; The tank body bottom of extract and separate jar (3) is provided with fluid level control device;
Said phosphatide purification devices comprises the blending tank two (11) that connects through gear pump successively, bleacher (12), bag filter two (13); Film filter two (14), temporary jar two (15), heater three (16); Falling film evaporator two (17), heater four (18), climbing film evaporator two (19); Heater five (20), stripper one (21);
Said mixing purifying plant comprises the blending tank three (22) that connects through pump successively, stripper two (23), vacuum column (24); Heater six (25), thin film evaporator (26), heat exchanger one (27); Wherein blending tank three (22), stripper two (23), and the pump that connects between the vacuum column (24) is a gear pump; Heater six (25), thin film evaporator (26), the pump that connects between the heat exchanger one (27) is a screw pump;
The outlet of the climbing film evaporator one (10) of said saponification purifying plant is communicated to the said inlet that mixes the blending tank three (22) of purifying plant with the outlet of the stripper one (21) of said phosphatide purification devices.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011205333027U CN202496368U (en) | 2011-12-20 | 2011-12-20 | Preparation equipment for food grade composite phospholipids rich in VE and sterol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011205333027U CN202496368U (en) | 2011-12-20 | 2011-12-20 | Preparation equipment for food grade composite phospholipids rich in VE and sterol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202496368U true CN202496368U (en) | 2012-10-24 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011205333027U Expired - Lifetime CN202496368U (en) | 2011-12-20 | 2011-12-20 | Preparation equipment for food grade composite phospholipids rich in VE and sterol |
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| Country | Link |
|---|---|
| CN (1) | CN202496368U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102511649A (en) * | 2011-12-20 | 2012-06-27 | 山东渤海实业股份有限公司 | Food-grade composite phospholipid rich in VE and sterol, preparation method and preparation equipment for composite phospholipid |
| CN107474948A (en) * | 2017-09-21 | 2017-12-15 | 安徽元创科技有限公司 | Decolouring phosphatide process units and its application method |
-
2011
- 2011-12-20 CN CN2011205333027U patent/CN202496368U/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102511649A (en) * | 2011-12-20 | 2012-06-27 | 山东渤海实业股份有限公司 | Food-grade composite phospholipid rich in VE and sterol, preparation method and preparation equipment for composite phospholipid |
| CN107474948A (en) * | 2017-09-21 | 2017-12-15 | 安徽元创科技有限公司 | Decolouring phosphatide process units and its application method |
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| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term |
Granted publication date: 20121024 |
|
| CX01 | Expiry of patent term |