CN206008677U - A kind of resin reaction kettle system - Google Patents

A kind of resin reaction kettle system Download PDF

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Publication number
CN206008677U
CN206008677U CN201620921830.2U CN201620921830U CN206008677U CN 206008677 U CN206008677 U CN 206008677U CN 201620921830 U CN201620921830 U CN 201620921830U CN 206008677 U CN206008677 U CN 206008677U
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China
Prior art keywords
horizontal
chuck
condenser
outlet
vessel
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Active
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CN201620921830.2U
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Chinese (zh)
Inventor
张著
王自新
黄杰
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WUYI CHEMICAL CO Ltd HENAN
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WUYI CHEMICAL CO Ltd HENAN
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Abstract

The utility model proposes a kind of resin reaction kettle system, including reactor, horizontal separator, thinning vessel, holding vessel, the reactor top gas outlet is connected with vertical condenser, and vertical condenser is connected by horizontal condenser with horizontal separator;Coalescence filter core is provided with the horizontal separator, backflow in horizontal separator is back in reactor by desiccant box, the wastewater outlet of horizontal separator is connected with thinning vessel chuck water inlet, thinning vessel chuck outlet connects the water inlet of horizontal condenser by cooling tower, the outlet of horizontal condenser is connected with thinning vessel chuck water inlet by pipeline, the discharging opening of thinning vessel is connected with stirred tank charging aperture, is provided with filter between stirred tank and holding vessel.Whole resin reaction kettle system can make full use of waste water, recycle cooling water, non-wastewater discharge, and feed purity high.

Description

A kind of resin reaction kettle system
Technical field
This utility model belongs to resin technology production field, and in particular to a kind of resin reaction kettle system.
Background technology
Paint is made up of resin, solvent, color stuffing, auxiliary agent etc., and wherein played a crucial role is resin used, It is the basic of paint chemistry classification.The production of resin is:First putting into reactant in reactor carries out polycondensation reaction, big through one After the completion of section time response, then corresponding diluent and thixotropic agent, mix homogeneously will be added to obtain most in product input thinning vessel Whole finished product.
Existing process units structure is relatively simple, reclaims not enough fully, can produce waste liquid, inadequate energy-conserving and environment-protective.In tree The course of reaction of fat can produce a number of solid impurity, as reflux gas are entered in final storage tank, so be unfavorable for clear Reason is also unfavorable for the raising of product quality.Current letdown tank chuck is connected with chilled water tank respectively with condenser chuck, latting drown Tank cooling demand cooling water is less, and condenser chuck demand cooling water is more, is so unfavorable for saving cooling water resources.And point The waste water that separates from device not only increases processing cost, is unfavorable for saving water resource frequently as wastewater treatment.
Adopting at present conventional separator production of resins process more, simple structure, but in high volume production process, equipment body Product is big, and dispersed phase drop settling height is long, and separation efficiency and disposal ability are low, and more or less exist in Paint Production Surfactant, is unfavorable for separating, strong inhibition disperse phase liquid drops in the coarse separation on interface.
Utility model content
This utility model provides a kind of resin reaction kettle system, solves above-mentioned resin and contains impurity effect paint quality Problem, rationally using separator waste water, reduce water resources consumption, improve separation efficiency.
Realize that the technical solution of the utility model is:A kind of resin reaction kettle system, including reactor, horizontal separator, Thinning vessel, holding vessel, the reactor top gas outlet are connected with vertical condenser, and vertical condenser is led to horizontal separator Cross horizontal condenser to be connected;Coalescence filter core is provided with the horizontal separator, and the backflow in horizontal separator passes through desiccant Box is back in reactor, and the wastewater outlet of horizontal separator is connected with thinning vessel chuck water inlet, thinning vessel chuck outlet The water inlet that horizontal condenser is connected by cooling tower, the outlet of horizontal condenser is by pipeline and thinning vessel chuck water inlet It is connected, the discharging opening of thinning vessel is connected with stirred tank charging aperture, is provided with filter between stirred tank and holding vessel.
It is provided with the filter with diatomaceous screen plate.
Desiccant is provided with the desiccant box.
The reactor is provided with chuck, is provided with deep fat passage in chuck.
The horizontal condenser is provided with chuck, and chuck is provided with water inlet and outlet.
The thinning vessel is provided with chuck, and chuck is provided with water inlet and outlet.
The beneficial effects of the utility model are:
(1)Using horizontal separator, the big liquid for needing sharp separation of volume of production is disclosure satisfy that, because horizontal separator Liquid-liquid separation interfacial area is big, and separating rate is fast, and compared with the conventional separator with size, treating capacity may be up to 2-5 times, carry High production efficiency;And it is provided with Coalescence filter core in horizontal separator, the water of part emulsifying breakdown of emulsion, poly- after Coalescence filter core Knot, separates the water of emulsified state, further improves the purity of waste water;
(2)The wastewater outlet of horizontal separator is connected with thinning vessel chuck water inlet, chuck thinning vessel chuck outlet The water of outflow enters horizontal condenser through cooling tower, and the water that horizontal condenser flows out reenters thinning vessel, forms a water Stream circulation, substantially increases the utilization ratio of waste water, reduces the utilization of water resource, reduce production cost, energy-conserving and environment-protective;
(3)Add agitator tank and filter between thinning vessel and holding vessel, entered after the material after dilution is agitated Filter, the impurity that the kieselguhr on screen plate can be in active adsorption material, improves the purity of material and the production matter of product Amount;
(4)The reflux pipeline of horizontal separator is provided with desiccant box, is provided with desiccant, isolates in desiccant box After the drying agent such as backflow such as benzene are dried, the moisture in backflow can be effectively removed, improve the purity level of backflow, enter And improve product quality.
Description of the drawings
In order to be illustrated more clearly that this utility model embodiment or technical scheme of the prior art, below will be to embodiment Or accompanying drawing to be used is briefly described needed for description of the prior art, it should be apparent that, drawings in the following description are only It is some embodiments of the present utility model, for those of ordinary skill in the art, in the premise for not paying creative work Under, can be with according to these other accompanying drawings of accompanying drawings acquisition.
Fig. 1 is structural representation of the present utility model.
Specific embodiment
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of this utility model, rather than whole Embodiment.Embodiment in based on this utility model, those of ordinary skill in the art are not under the premise of creative work is paid The every other embodiment for being obtained, belongs to the scope of this utility model protection.
As shown in figure 1, a kind of resin reaction kettle system, including reactor 1, horizontal separator 5, thinning vessel 7, holding vessel 10, the outlet of 1 top gas of the reactor is connected with vertical condenser 3, and vertical condenser 3 is with horizontal separator 5 by horizontal Condenser 4 is connected;Coalescence filter core 5-1 is provided with the horizontal separator 5, and the backflow in horizontal separator 5 passes through desiccant Box 6 is back in reactor 1, and the wastewater outlet of horizontal separator 5 is connected with 7 chuck water inlet of thinning vessel, and 7 chuck of thinning vessel goes out The mouth of a river connects the water inlet of horizontal condenser 4 by cooling tower 2, and the outlet of horizontal condenser 4 is pressed from both sides with thinning vessel 7 by pipeline Set water inlet is connected, and the discharging opening of thinning vessel 7 is connected with 8 charging aperture of stirred tank, is provided with filtration between stirred tank 8 and holding vessel 10 Machine 9.
During production, material is entered in reactor 1, and heat kerosene enters the heat of the chuck of reactor 1 to be had in passage, to reach thing Temperature needed for material reaction, during reaction, the gas outlet on reacted 1 top of kettle of gas phase gas enters be attached thereto vertical cool solidifying Device 3, enters horizontal condenser 4 afterwards, and vertical condenser 3 is used in combination with horizontal condenser 4, more fully can be taken away in pipe Heat, rapid condensation raw material liq and water prevent opposing steam flow to reactor 1.Raw material liq after condensation and water are entered Horizontal separator 5, carries out the separation of organic faciess and water, in horizontal separator 5 due to the more general gravity of horizontal separator 5 point Big from device separating interface area, the purpose of sharp separation can be reached, while the water of part emulsifying is in horizontal separator 5 Coalescence filter core 5-1, through breakdown of emulsion, coalescence, separates the water of emulsified state.The backflow that isolates contains some water Point, desiccant box 6 is therefore provided with the pipeline outside horizontal separator 5, is provided with desiccant in desiccant box 6, backflow is passed through After desiccant dryness, the moisture in backflow can be effectively removed, improve the purity of backflow.By the material out of reactor 1 to Thinning vessel 7 is reached, and the material after dilution after stirred tank 8 stirs enters filter 9, filtration is provided with filter 9 Plate, screen plate are provided with kieselguhr, and the impurity in kieselguhr energy active adsorption material improves the purity of material, through filtered Material is finally stored in holding vessel 10.
Preferably, the horizontal condenser 4 is provided with chuck, and chuck is provided with water inlet and outlet;Thinning vessel 7 is provided with Chuck, chuck are provided with water inlet and outlet.For effectively improving the utilization ratio of waste water, it is useless that horizontal separator 5 is isolated Water enters the water inlet of 7 chuck of thinning vessel, and the cooling water as thinning vessel 7 is used, the water of the outlet discharge of 7 chuck of thinning vessel Again cool down through cooling tower, enter the water inlet of 4 chuck of horizontal condenser, the cooling water as horizontal condenser 4 is used, made Used waste water is discharged from 4 chuck outlet of horizontal condenser, and the waste water that is discharged with horizontal separator 5 is converged, again as cold But water circulation is used, and in whole cooling procedure, discharge without waste water reduces the consumption of water, makes full use of waste water, reduces whole Individual production cost.
Preferred embodiment of the present utility model is the foregoing is only, not in order to limit this utility model, all at this Within the spirit and principle of utility model, any modification, equivalent substitution and improvements that is made etc. should be included in this utility model Protection domain within.

Claims (6)

1. a kind of resin reaction kettle system, including reactor(1), horizontal separator(5), thinning vessel(7), holding vessel(10), its It is characterised by:The reactor(1)Top gas outlet and vertical condenser(3)It is connected, vertical condenser(3)Separate with horizontal Device(5)By horizontal condenser(4)It is connected;The horizontal separator(5)Coalescence filter core is inside provided with(5-1), horizontal separator(5) In backflow pass through desiccant box(6)It is back to reactor(1)Interior, horizontal separator(5)Wastewater outlet and thinning vessel(7) Chuck water inlet is connected, thinning vessel(7)Chuck outlet passes through cooling tower(2)Connection horizontal condenser(4)Water inlet, horizontal Condenser(4)Outlet by pipeline and thinning vessel(7)Chuck water inlet is connected, thinning vessel(7)Discharging opening and stirred tank (8)Charging aperture connects, stirred tank(8)With holding vessel(10)Between be provided with filter(9).
2. resin reaction kettle system according to claim 1, it is characterised in that:The filter(9)Band diatom is inside provided with The screen plate of soil.
3. resin reaction kettle system according to claim 1, it is characterised in that:The desiccant box(6)Drying is inside provided with Agent.
4. resin reaction kettle system according to claim 1, it is characterised in that:The reactor(1)It is provided with chuck, chuck Deep fat passage is inside provided with.
5. resin reaction kettle system according to claim 1, it is characterised in that:The horizontal condenser(4)It is provided with chuck, Chuck is provided with water inlet and outlet.
6. resin reaction kettle system according to claim 1, it is characterised in that:The thinning vessel(7)Chuck is provided with, is pressed from both sides Put and be provided with water inlet and outlet.
CN201620921830.2U 2016-08-23 2016-08-23 A kind of resin reaction kettle system Active CN206008677U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620921830.2U CN206008677U (en) 2016-08-23 2016-08-23 A kind of resin reaction kettle system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620921830.2U CN206008677U (en) 2016-08-23 2016-08-23 A kind of resin reaction kettle system

Publications (1)

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CN206008677U true CN206008677U (en) 2017-03-15

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CN201620921830.2U Active CN206008677U (en) 2016-08-23 2016-08-23 A kind of resin reaction kettle system

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109395679A (en) * 2018-11-02 2019-03-01 浙江六合工程技术有限公司 Adjustable multipurpose way horizontal separator

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109395679A (en) * 2018-11-02 2019-03-01 浙江六合工程技术有限公司 Adjustable multipurpose way horizontal separator

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