CN206008061U - A kind of new sulfur trioxide autoclave vaporizer - Google Patents

A kind of new sulfur trioxide autoclave vaporizer Download PDF

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Publication number
CN206008061U
CN206008061U CN201621026166.1U CN201621026166U CN206008061U CN 206008061 U CN206008061 U CN 206008061U CN 201621026166 U CN201621026166 U CN 201621026166U CN 206008061 U CN206008061 U CN 206008061U
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CN
China
Prior art keywords
tube sheet
autoclave
pipe box
sulfur trioxide
housing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621026166.1U
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Chinese (zh)
Inventor
安中良
刘兴荣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yangzhou Rong Hui Chemical Equipment Co Ltd
Original Assignee
Yangzhou Rong Hui Chemical Equipment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yangzhou Rong Hui Chemical Equipment Co Ltd filed Critical Yangzhou Rong Hui Chemical Equipment Co Ltd
Priority to CN201621026166.1U priority Critical patent/CN206008061U/en
Application granted granted Critical
Publication of CN206008061U publication Critical patent/CN206008061U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

A kind of new sulfur trioxide autoclave vaporizer, is related to field of heat exchange equipment.Including horizontally disposed autoclave housing;Some U-tubes are provided with autoclave housing, and the left end of autoclave housing is connected with front-end pipe box, is provided with demarcation strip in front-end pipe box;Inner side tube sheet and outside tube sheet is provided between front-end pipe box and autoclave housing, inner side tube sheet is connected with autoclave housing seal, it is tightly connected between outside tube sheet and front-end pipe box, gap is left between inner side tube sheet and outside tube sheet, and between close cavity is connected as by spacer pipe, the bottom of seal cavity is connected with sulfur trioxide leakage alarm;Seal cavity is connected as by spacer pipe between inner side tube sheet and outside tube sheet, the bottom of seal cavity is connected with sulfur trioxide leakage alarm, outside tube sheet, the leakage situation between inner side tube sheet and U-tube is found in time, be easy to keep in repair.

Description

A kind of new sulfur trioxide autoclave vaporizer
Technical field
This utility model is related to field of heat exchange equipment, specially a kind of new sulfur trioxide autoclave vaporizer.
Background technology
Sulfan production is to heat 32% oleum in heat exchanger, the sulfur trioxide that evaporation wherein dissociates Gas, sulfur trioxide gas are condensed again to generate sulfan product.
Current sulfur trioxide evaporator, generally vertical tube-type heater, on the heaters portion's design certain space make For sulfur trioxide evaporating space;Heating medium typically from sulfate system itself pyrolytic conversion gas come heat oleum evaporation Sulfur trioxide gas.
Some enterprises do not possess and are used as heating medium using pyrolytic conversion gas, but using water vapour as evaporating three oxygen Change the thermal source of sulfur, the pattern of employing is generally vertical common tubular heat exchanger structure, and the tube sheet at tubulation two ends is single tube plate, At the numerous tube sheet of solder joint, manufacture or during production run at which, cold fluid and hot fluid can occur unavoidably phase occurs at tube sheet Mutually leakage problem, once steam occurs at tube sheet leaking in oleum, can cause serious accident, because water vapour with Oleum can occur vigorous reaction, generate the very strong dilute sulfuric acid of corrosivity, and release substantial amounts of heat, such as process too late When, the lighter causes equipment to damage, and severe one can cause an explosion accident.
Utility model content
The purpose of this utility model is the risk that accident occurs to reduce sulfur trioxide evaporator, there is provided a kind of safety can The sulfur trioxide autoclave vaporizer for leaning on.
The technical scheme for realizing above-mentioned purpose is:A kind of new sulfur trioxide autoclave vaporizer, including horizontally disposed kettle Sandwich type element, the upper center of autoclave housing are provided with sulfur trioxide gas outlet, and the upper end of autoclave housing is provided with oleum and enters Mouthful, the lower end of autoclave housing is provided with oleum outlet;
Some U-tubes are provided with autoclave housing, the left end of autoclave housing is connected with front-end pipe box, arrange in front-end pipe box There is demarcation strip, demarcation strip is by front-end pipe box even partition into two not connected first chambers and second chamber, first chamber On be connected with steam inlet, be connected with steam (vapor) outlet in second chamber;
It is characterized in that:Be provided with inner side tube sheet and outside tube sheet between front-end pipe box and autoclave housing, inner side tube sheet with Autoclave housing seal connects, and is tightly connected, between leaving between inner side tube sheet and outside tube sheet between outside tube sheet and front-end pipe box Gap, and close cavity is connected as by spacer pipe directly, the bottom of seal cavity is connected with sulfur trioxide leakage alarm;
The two ends of the U-tube in autoclave housing pass through inner side tube sheet, spacer pipe, outside tube sheet, and connect front-end pipe box, U It is tightly connected between the two ends of shape pipe and inner side tube sheet, outside tube sheet, the two ends of every U-tube are located at dividing for front-end pipe box respectively Dividing plate both sides.
Further, manhole is offered on the demarcation strip, be sealedly connected with dismountable cover plate on manhole.
Further, absorbent cotton is coated with the U-tube between the inner side tube sheet and outside tube sheet.
The beneficial effects of the utility model:
1st, this utility model structure is novel, reasonable in design, safe and reliable to operation, and vaporizer front end tube sheet is using two-tube hardened Structure, it is to avoid leak at the very many tube sheets of solder joint, it is ensured that sulfur trioxide evaporator safe and reliable operation.
2nd, seal cavity is connected as by spacer pipe between inner side tube sheet and outside tube sheet, the bottom of seal cavity is connected with Sulfur trioxide leakage alarm, enables outside tube sheet, the leakage situation between inner side tube sheet and U-tube to be found in time, just In maintenance.
3rd, manhole is offered on demarcation strip, be sealedly connected with dismountable cover plate on manhole, thus can be in front-end pipe box Pressure testing detection is carried out after installation to U-tube, and is easy to the within the chamber to front-end pipe box to carry out daily maintenance and cleaning Work.
4th, be coated with absorbent cotton on the U-tube between inner side tube sheet and outside tube sheet, occur leakage when, water vapour with send out The dilute sulfuric acid that cigarette sulfuric acid reaction is produced is attracted on absorbent cotton, reduces the damage to equipment.
Description of the drawings
Fig. 1 is structural representation of the present utility model;
Structural representations of the Fig. 2 for demarcation strip.
Specific embodiment
As shown in figure 1, this utility model includes that horizontally disposed autoclave housing 1, the upper center of autoclave housing 1 are provided with Sulfur trioxide gas outlet 2, the upper end of autoclave housing 1 are provided with oleum entrance 3, and the lower end of autoclave housing 1 is provided with smoke Sulphuric acid outlet 4, the bottom of autoclave housing 1 is additionally provided with supporting leg 5.
Some U-tubes 6 are provided with autoclave housing 1, the left end of autoclave housing 1 is connected with front-end pipe box 7, front-end pipe box 7 In be provided with demarcation strip 8, demarcation strip 8 by 7 even partition of front-end pipe box into two not connected first chambers and second chamber, Steam inlet 9 is connected with first chamber, is connected with steam (vapor) outlet 10 in second chamber.
Inner side tube sheet 11 and outside tube sheet 12, inner side tube sheet 11 and autoclave is provided between front-end pipe box 7 and autoclave housing 1 Housing 1 is tightly connected, and is tightly connected between outside tube sheet 12 and front-end pipe box 7, stays between inner side tube sheet 11 and outside tube sheet 12 Have a gap, and between close cavity is connected as by spacer pipe 13, the bottom of seal cavity is connected with sulfur trioxide reveals and reports to the police Device 14.
The two ends of the U-tube 6 in autoclave housing 1 pass through inner side tube sheet 11, spacer pipe 13, outside tube sheet 12, and before connecting End pipe case 7, is tightly connected between the two ends of U-tube 6 and inner side tube sheet 11, outside tube sheet 13, the two ends difference of every U-tube 6 It is located at 8 both sides of demarcation strip of front-end pipe box 7.
Absorbent cotton 15 is coated with U-tube 6 between inner side tube sheet 11 and outside tube sheet 13.
As shown in Fig. 2 manhole 16 is offered on demarcation strip 8, cover plate 17 is connected with by bolt seal on manhole 16.

Claims (3)

1. a kind of new sulfur trioxide autoclave vaporizer, including horizontally disposed autoclave housing, the upper center of autoclave housing sets Sulfur trioxide gas outlet is equipped with, the upper end of autoclave housing is provided with oleum entrance, and the lower end of autoclave housing is provided with smoke Sulphuric acid is exported;
Some U-tubes are provided with autoclave housing, the left end of autoclave housing is connected with front-end pipe box, be provided with point in front-end pipe box Front-end pipe box even partition into two not connected first chambers and second chamber, is connected in first chamber by dividing plate, demarcation strip Steam inlet is connected to, steam (vapor) outlet in second chamber, is connected with;
It is characterized in that:Inner side tube sheet and outside tube sheet, inner side tube sheet and autoclave is provided between front-end pipe box and autoclave housing Housing seal connects, and is tightly connected, leaves gap between inner side tube sheet and outside tube sheet between outside tube sheet and front-end pipe box, and And between close cavity is connected as by spacer pipe, the bottom of seal cavity is connected with sulfur trioxide leakage alarm;
The two ends of the U-tube in autoclave housing pass through inner side tube sheet, spacer pipe, outside tube sheet, and connect front-end pipe box, U-tube Two ends and inner side tube sheet, outside tube sheet between be tightly connected, the two ends of every U-tube are located at the demarcation strip of front-end pipe box respectively Both sides.
2. a kind of new sulfur trioxide autoclave vaporizer according to claim 1, it is characterised in that:Offer on demarcation strip Manhole, is sealedly connected with dismountable cover plate on manhole.
3. a kind of new sulfur trioxide autoclave vaporizer according to claim 1, it is characterised in that:The inner side tube sheet and Absorbent cotton is coated with U-tube between the tube sheet of outside.
CN201621026166.1U 2016-08-31 2016-08-31 A kind of new sulfur trioxide autoclave vaporizer Expired - Fee Related CN206008061U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621026166.1U CN206008061U (en) 2016-08-31 2016-08-31 A kind of new sulfur trioxide autoclave vaporizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621026166.1U CN206008061U (en) 2016-08-31 2016-08-31 A kind of new sulfur trioxide autoclave vaporizer

Publications (1)

Publication Number Publication Date
CN206008061U true CN206008061U (en) 2017-03-15

Family

ID=58258105

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621026166.1U Expired - Fee Related CN206008061U (en) 2016-08-31 2016-08-31 A kind of new sulfur trioxide autoclave vaporizer

Country Status (1)

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CN (1) CN206008061U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109364503A (en) * 2018-11-29 2019-02-22 李晓垚 A kind of sulfuric acid evaporator
CN109437122A (en) * 2018-11-29 2019-03-08 李晓垚 A kind of purification acid production process

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109364503A (en) * 2018-11-29 2019-02-22 李晓垚 A kind of sulfuric acid evaporator
CN109437122A (en) * 2018-11-29 2019-03-08 李晓垚 A kind of purification acid production process
CN109437122B (en) * 2018-11-29 2020-05-22 联仕(昆山)化学材料有限公司 Refined acid production process
CN109364503B (en) * 2018-11-29 2021-01-05 广德县桃州镇明莲蔬果种植家庭农场 Sulfuric acid evaporator

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170315

Termination date: 20200831

CF01 Termination of patent right due to non-payment of annual fee