CN206008061U - A kind of new sulfur trioxide autoclave vaporizer - Google Patents
A kind of new sulfur trioxide autoclave vaporizer Download PDFInfo
- Publication number
- CN206008061U CN206008061U CN201621026166.1U CN201621026166U CN206008061U CN 206008061 U CN206008061 U CN 206008061U CN 201621026166 U CN201621026166 U CN 201621026166U CN 206008061 U CN206008061 U CN 206008061U
- Authority
- CN
- China
- Prior art keywords
- tube sheet
- autoclave
- pipe box
- sulfur trioxide
- housing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
A kind of new sulfur trioxide autoclave vaporizer, is related to field of heat exchange equipment.Including horizontally disposed autoclave housing;Some U-tubes are provided with autoclave housing, and the left end of autoclave housing is connected with front-end pipe box, is provided with demarcation strip in front-end pipe box;Inner side tube sheet and outside tube sheet is provided between front-end pipe box and autoclave housing, inner side tube sheet is connected with autoclave housing seal, it is tightly connected between outside tube sheet and front-end pipe box, gap is left between inner side tube sheet and outside tube sheet, and between close cavity is connected as by spacer pipe, the bottom of seal cavity is connected with sulfur trioxide leakage alarm;Seal cavity is connected as by spacer pipe between inner side tube sheet and outside tube sheet, the bottom of seal cavity is connected with sulfur trioxide leakage alarm, outside tube sheet, the leakage situation between inner side tube sheet and U-tube is found in time, be easy to keep in repair.
Description
Technical field
This utility model is related to field of heat exchange equipment, specially a kind of new sulfur trioxide autoclave vaporizer.
Background technology
Sulfan production is to heat 32% oleum in heat exchanger, the sulfur trioxide that evaporation wherein dissociates
Gas, sulfur trioxide gas are condensed again to generate sulfan product.
Current sulfur trioxide evaporator, generally vertical tube-type heater, on the heaters portion's design certain space make
For sulfur trioxide evaporating space;Heating medium typically from sulfate system itself pyrolytic conversion gas come heat oleum evaporation
Sulfur trioxide gas.
Some enterprises do not possess and are used as heating medium using pyrolytic conversion gas, but using water vapour as evaporating three oxygen
Change the thermal source of sulfur, the pattern of employing is generally vertical common tubular heat exchanger structure, and the tube sheet at tubulation two ends is single tube plate,
At the numerous tube sheet of solder joint, manufacture or during production run at which, cold fluid and hot fluid can occur unavoidably phase occurs at tube sheet
Mutually leakage problem, once steam occurs at tube sheet leaking in oleum, can cause serious accident, because water vapour with
Oleum can occur vigorous reaction, generate the very strong dilute sulfuric acid of corrosivity, and release substantial amounts of heat, such as process too late
When, the lighter causes equipment to damage, and severe one can cause an explosion accident.
Utility model content
The purpose of this utility model is the risk that accident occurs to reduce sulfur trioxide evaporator, there is provided a kind of safety can
The sulfur trioxide autoclave vaporizer for leaning on.
The technical scheme for realizing above-mentioned purpose is:A kind of new sulfur trioxide autoclave vaporizer, including horizontally disposed kettle
Sandwich type element, the upper center of autoclave housing are provided with sulfur trioxide gas outlet, and the upper end of autoclave housing is provided with oleum and enters
Mouthful, the lower end of autoclave housing is provided with oleum outlet;
Some U-tubes are provided with autoclave housing, the left end of autoclave housing is connected with front-end pipe box, arrange in front-end pipe box
There is demarcation strip, demarcation strip is by front-end pipe box even partition into two not connected first chambers and second chamber, first chamber
On be connected with steam inlet, be connected with steam (vapor) outlet in second chamber;
It is characterized in that:Be provided with inner side tube sheet and outside tube sheet between front-end pipe box and autoclave housing, inner side tube sheet with
Autoclave housing seal connects, and is tightly connected, between leaving between inner side tube sheet and outside tube sheet between outside tube sheet and front-end pipe box
Gap, and close cavity is connected as by spacer pipe directly, the bottom of seal cavity is connected with sulfur trioxide leakage alarm;
The two ends of the U-tube in autoclave housing pass through inner side tube sheet, spacer pipe, outside tube sheet, and connect front-end pipe box, U
It is tightly connected between the two ends of shape pipe and inner side tube sheet, outside tube sheet, the two ends of every U-tube are located at dividing for front-end pipe box respectively
Dividing plate both sides.
Further, manhole is offered on the demarcation strip, be sealedly connected with dismountable cover plate on manhole.
Further, absorbent cotton is coated with the U-tube between the inner side tube sheet and outside tube sheet.
The beneficial effects of the utility model:
1st, this utility model structure is novel, reasonable in design, safe and reliable to operation, and vaporizer front end tube sheet is using two-tube hardened
Structure, it is to avoid leak at the very many tube sheets of solder joint, it is ensured that sulfur trioxide evaporator safe and reliable operation.
2nd, seal cavity is connected as by spacer pipe between inner side tube sheet and outside tube sheet, the bottom of seal cavity is connected with
Sulfur trioxide leakage alarm, enables outside tube sheet, the leakage situation between inner side tube sheet and U-tube to be found in time, just
In maintenance.
3rd, manhole is offered on demarcation strip, be sealedly connected with dismountable cover plate on manhole, thus can be in front-end pipe box
Pressure testing detection is carried out after installation to U-tube, and is easy to the within the chamber to front-end pipe box to carry out daily maintenance and cleaning
Work.
4th, be coated with absorbent cotton on the U-tube between inner side tube sheet and outside tube sheet, occur leakage when, water vapour with send out
The dilute sulfuric acid that cigarette sulfuric acid reaction is produced is attracted on absorbent cotton, reduces the damage to equipment.
Description of the drawings
Fig. 1 is structural representation of the present utility model;
Structural representations of the Fig. 2 for demarcation strip.
Specific embodiment
As shown in figure 1, this utility model includes that horizontally disposed autoclave housing 1, the upper center of autoclave housing 1 are provided with
Sulfur trioxide gas outlet 2, the upper end of autoclave housing 1 are provided with oleum entrance 3, and the lower end of autoclave housing 1 is provided with smoke
Sulphuric acid outlet 4, the bottom of autoclave housing 1 is additionally provided with supporting leg 5.
Some U-tubes 6 are provided with autoclave housing 1, the left end of autoclave housing 1 is connected with front-end pipe box 7, front-end pipe box 7
In be provided with demarcation strip 8, demarcation strip 8 by 7 even partition of front-end pipe box into two not connected first chambers and second chamber,
Steam inlet 9 is connected with first chamber, is connected with steam (vapor) outlet 10 in second chamber.
Inner side tube sheet 11 and outside tube sheet 12, inner side tube sheet 11 and autoclave is provided between front-end pipe box 7 and autoclave housing 1
Housing 1 is tightly connected, and is tightly connected between outside tube sheet 12 and front-end pipe box 7, stays between inner side tube sheet 11 and outside tube sheet 12
Have a gap, and between close cavity is connected as by spacer pipe 13, the bottom of seal cavity is connected with sulfur trioxide reveals and reports to the police
Device 14.
The two ends of the U-tube 6 in autoclave housing 1 pass through inner side tube sheet 11, spacer pipe 13, outside tube sheet 12, and before connecting
End pipe case 7, is tightly connected between the two ends of U-tube 6 and inner side tube sheet 11, outside tube sheet 13, the two ends difference of every U-tube 6
It is located at 8 both sides of demarcation strip of front-end pipe box 7.
Absorbent cotton 15 is coated with U-tube 6 between inner side tube sheet 11 and outside tube sheet 13.
As shown in Fig. 2 manhole 16 is offered on demarcation strip 8, cover plate 17 is connected with by bolt seal on manhole 16.
Claims (3)
1. a kind of new sulfur trioxide autoclave vaporizer, including horizontally disposed autoclave housing, the upper center of autoclave housing sets
Sulfur trioxide gas outlet is equipped with, the upper end of autoclave housing is provided with oleum entrance, and the lower end of autoclave housing is provided with smoke
Sulphuric acid is exported;
Some U-tubes are provided with autoclave housing, the left end of autoclave housing is connected with front-end pipe box, be provided with point in front-end pipe box
Front-end pipe box even partition into two not connected first chambers and second chamber, is connected in first chamber by dividing plate, demarcation strip
Steam inlet is connected to, steam (vapor) outlet in second chamber, is connected with;
It is characterized in that:Inner side tube sheet and outside tube sheet, inner side tube sheet and autoclave is provided between front-end pipe box and autoclave housing
Housing seal connects, and is tightly connected, leaves gap between inner side tube sheet and outside tube sheet between outside tube sheet and front-end pipe box, and
And between close cavity is connected as by spacer pipe, the bottom of seal cavity is connected with sulfur trioxide leakage alarm;
The two ends of the U-tube in autoclave housing pass through inner side tube sheet, spacer pipe, outside tube sheet, and connect front-end pipe box, U-tube
Two ends and inner side tube sheet, outside tube sheet between be tightly connected, the two ends of every U-tube are located at the demarcation strip of front-end pipe box respectively
Both sides.
2. a kind of new sulfur trioxide autoclave vaporizer according to claim 1, it is characterised in that:Offer on demarcation strip
Manhole, is sealedly connected with dismountable cover plate on manhole.
3. a kind of new sulfur trioxide autoclave vaporizer according to claim 1, it is characterised in that:The inner side tube sheet and
Absorbent cotton is coated with U-tube between the tube sheet of outside.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201621026166.1U CN206008061U (en) | 2016-08-31 | 2016-08-31 | A kind of new sulfur trioxide autoclave vaporizer |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201621026166.1U CN206008061U (en) | 2016-08-31 | 2016-08-31 | A kind of new sulfur trioxide autoclave vaporizer |
Publications (1)
Publication Number | Publication Date |
---|---|
CN206008061U true CN206008061U (en) | 2017-03-15 |
Family
ID=58258105
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201621026166.1U Expired - Fee Related CN206008061U (en) | 2016-08-31 | 2016-08-31 | A kind of new sulfur trioxide autoclave vaporizer |
Country Status (1)
Country | Link |
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CN (1) | CN206008061U (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109364503A (en) * | 2018-11-29 | 2019-02-22 | 李晓垚 | A kind of sulfuric acid evaporator |
CN109437122A (en) * | 2018-11-29 | 2019-03-08 | 李晓垚 | A kind of purification acid production process |
-
2016
- 2016-08-31 CN CN201621026166.1U patent/CN206008061U/en not_active Expired - Fee Related
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109364503A (en) * | 2018-11-29 | 2019-02-22 | 李晓垚 | A kind of sulfuric acid evaporator |
CN109437122A (en) * | 2018-11-29 | 2019-03-08 | 李晓垚 | A kind of purification acid production process |
CN109437122B (en) * | 2018-11-29 | 2020-05-22 | 联仕(昆山)化学材料有限公司 | Refined acid production process |
CN109364503B (en) * | 2018-11-29 | 2021-01-05 | 广德县桃州镇明莲蔬果种植家庭农场 | Sulfuric acid evaporator |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170315 Termination date: 20200831 |
|
CF01 | Termination of patent right due to non-payment of annual fee |