CN206002350U - A kind of reactor on-line sampler - Google Patents
A kind of reactor on-line sampler Download PDFInfo
- Publication number
- CN206002350U CN206002350U CN201621041271.2U CN201621041271U CN206002350U CN 206002350 U CN206002350 U CN 206002350U CN 201621041271 U CN201621041271 U CN 201621041271U CN 206002350 U CN206002350 U CN 206002350U
- Authority
- CN
- China
- Prior art keywords
- reactor
- valve
- control valve
- sampler
- probe tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Sampling And Sample Adjustment (AREA)
Abstract
The utility model discloses a kind of reactor on-line sampler, it includes reactor body, also include at least three probe tubes that lower end is inserted in differing heights in reactor, probe tube upper end is converged, and each probe tube upper end is corresponding respectively before not converging installs sub-control valve, upper end is connected to transparent sampling room after converging；Set master control valve between meet and transparent sampling room, above master control valve, set sample tap；Transparent sampling room is provided with a connecting tube upwards, and this connecting tube has two branch roads, connects vacuum valve and charge valve respectively.The sample of different parts in reactor can be got by controlling sampling valve, sampler is provided with charge valve simultaneously, the sample remaining in sampler can be blown in reactor, so that sampling is more representative, this sampler is simple to operation, on-line period at any time can be accomplished, enabling tracking reaction process more accurately and timely.
Description
Technical field
This utility model is related to a kind of sampler, more particularly, to a kind of reactor on-line sampler.
Background technology
When carrying out chemical industry synthesis using reactor, in order to adjust the parameter controlling material in reactor in time, it is right to need
Response situation in reactor carries out real-time tracking, thus needing sampling in reactor to be analyzed testing.
The sampling method commonly used at present is to utilize manual sampling, by opening reactor kettle cover, then by probe tube deeply
It is sampled under liquid level in reactor, in order to ensure the uniformity sampling, need the different parts of reactor are taken
Sample, but reactor is deep, more difficult when bottom is sampled；Reaction in simultaneous reactions kettle generally has toxic gas release
Or the corrosivity of liquid are larger, larger to harm using this sampling mode, also surrounding can be polluted.Separately
Outer also have part to be sampled using the sampler of evacuation principle, and shortcoming is that the position of probe tube sampling is fixed it is impossible to represent
Reaction process in whole reactor；Pipeline inside have residual sample after sampling simultaneously, the accuracy of next sub-sampling is made
Become impact.
Utility model content
In order to solve the problems of background technology, the technical solution of the utility model is：
A kind of reactor on-line sampler, including reactor body it is characterised in that：Also include lower end and be inserted in reactor
At least three probe tubes of interior differing heights, probe tube upper end is converged, and each probe tube upper end corresponded to before not converging respectively
Sub-control valve is installed, upper end is connected to transparent sampling room after converging；Master control valve is set, always between meet and transparent sampling room
Sample tap is set above control valve；Transparent sampling room is provided with a connecting tube upwards, and this connecting tube has two branch roads, connects vacuum respectively
Valve and charge valve.
Preferably, setting 3 probe tubes in this utility model reactor, the length of described 3 probe tubes is different, inserts respectively
Enter at reactor 1/4,2/4,3/4 height, adjacent samples pipe is spaced 120 degree of angles, is evenly distributed in reactor inner periphery.Described 3
3 sub-control valves have been filled respectively above root probe tube.
Preferably, described sample tap is located between master control valve and transparent sampling room.
Preferably, reactor is originally additionally provided with agitator in vivo.
This utility model is had an advantageous effect in that：(1) bottom of sampler is provided with 3 probe tubes, described 3 samplings
The length of pipe is different, and is uniformly distributed in reactor inner periphery, can get the sample of different depth in reactor, samples energy
Enough true reflection reaction kettle for reaction situations, more representative.(2) charge valve is connected with sampler, after sampling finishes, can
It is filled with nitrogen or other noble gases into intubation, by the whole blow pressure of residual reactants material in intubation in reactor, thus
Eliminate the impact that in pipe, residual reactants material produces to analytical reactions material.(3) transparent sampling room is further connected with sampler, permissible
Real-time monitored reactant state, sampler is simple to operate simultaneously, is easily controlled, pollution-free, can be analyzed surveying with real time sample
Examination, follows the tracks of extent of reaction.
Brief description
Fig. 1 is a kind of structural representation of this utility model reactor on-line sampler.
In figure, 1 is reactor body, and 2 is stirring paddle, and 3 is sampling master control valve, and 3-1 is the first sub-control valve, and 3-2 is
Second sub-control valve, 3-3 is the 3rd sub-control valve, and 4 is transparent sampling room, and 5 is vacuum valve, and 6 is charge valve, and 7 is the first sampling
Pipe, 8 is the second probe tube, and 9 is the 3rd probe tube, and 10 is sample tap.
Specific embodiment
In order that those skilled in the art more fully understand the technical solution of the utility model, below in conjunction with the accompanying drawings
The utility model is described in further detail with most preferred embodiment.
A kind of this utility model reactor on-line sampler, as shown in figure 1, including reactor body 1, stirring paddle 2, sampling
Master control valve 3, the first sub-control valve 3-1, the second sub-control valve 3-2, the 3rd sub-control valve 3-3, transparent sampling room 4, vacuum valve
5, charge valve 6, the first probe tube 7, the second probe tube 8, probe tube 9, sample tap 10.
Wherein, probe tube 7, probe tube 8, the length of this three probe tubes of probe tube 9 is different, upper end converge be connected to transparent
Sampling room 4；Lower end is respectively at insertion reaction kettle 1/4,2/4,3/4 height, and adjacent samples pipe is spaced 120 degree of angles, is evenly distributed
In reactor inner periphery.This three probe tube upper ends are corresponding respectively before not converging to install three sub-control valves, is respectively, the
The first sub-control valve 3-1 is installed in one probe tube 7 upper end.The second sub-control valve 3-2, the 3rd sampling are installed in second probe tube 8 upper end
The 3rd sub-control valve 3-3 is installed in pipe 9 upper end.Be connected to transparent sampling room 4 after converging, and meet and transparent sampling room 4 it
Between set master control valve 3, be provided with opening sample tap 10 diagonally downward between master control valve 3 and transparent sampling room 4.Transparent sampling room
4 are provided with a connecting tube upwards, and this connecting tube has two branch roads, connect vacuum valve 5 and charge valve 6 respectively.
In a further embodiment, transparent sampling room 4 is one section of transparent connecting tube.
A kind of simple operationss of this utility model reactor on-line sampler are as follows, open master control valve 3 successively, the
One sub-control valve 3-1, vacuum valve 5, is extracted material at the first probe tube 7, reacts when being observed that by transparent sampling room 4
During material, close the first sub-control valve 3-1, master control valve 3 and vacuum valve 5 successively, open sample tap 10, reaction mass is from sampling
Mouth flows out；After sampling terminates at probe tube 7, close sample tap 10, open master control valve 3, the second sub-control valve 3- successively
2, vacuum valve 5, extracts material, when being observed that reaction mass by transparent sampling room 4, successively at the second probe tube 8
Close the second sub-control valve 3-2, master control valve 3 and vacuum valve 5, open sample tap 10, reaction mass flows out from sample tap；Second
After sampling terminates at probe tube 8, close sample tap 10, open master control valve 3, the 3rd sub-control valve 3-3, vacuum valve successively
5, extract material at the 3rd probe tube 9, when reaction mass is observed that by transparent connection 4, close the 3rd successively secondary
Control valve 3-3, master control valve 3 and vacuum valve 5, open sample tap 10, and reaction mass flows out from sample tap；At 3rd probe tube 9
After sampling terminates, close and remove sample sample tap 10, open the secondary control of the first sub-control valve 3-1, the second sub-control valve 3-2, the 3rd successively
Valve 3-3 processed, opens ventilating control valve 6, into transparent sampling room 4, the first probe tube 7, the second probe tube 8 and the 3rd probe tube 9
Blow pressure nitrogen for several times, is replaced the reaction mass of intubation bottom, is then shut off ventilating control valve 6, master control valve 3, the first sub-control
Valve 3-1, the second sub-control valve 3-2, the 3rd sub-control valve 3-3；To carry out after the material mix homogeneously of these three different parts point
Analysis test.Repeat above just operating procedure when needing to sample again.
Claims (4)
1. a kind of reactor on-line sampler, including reactor body it is characterised in that：Also include lower end to be inserted in reactor
At least three probe tubes of differing heights, probe tube upper end is converged, and each probe tube upper end corresponded to peace before not converging respectively
Dress sub-control valve, upper end is connected to transparent sampling room after converging；Master control valve, master control is set between meet and transparent sampling room
Sample tap is set above valve processed；Transparent sampling room is provided with a connecting tube upwards, and this connecting tube has two branch roads, connects vacuum valve respectively
And charge valve.
2. as claimed in claim 1 a kind of reactor on-line sampler it is characterised in that：Probe tube has three, described three
The length of probe tube is different, and respectively at insertion reaction kettle 1/4,2/4,3/4 height, adjacent samples pipe is spaced 120 degree of angles, average mark
It is distributed in reactor inner periphery.
3. as claimed in claim 1 a kind of reactor on-line sampler it is characterised in that：Described sample tap is located at master control
Between valve and transparent sampling room.
4. as claimed in claim 1 a kind of reactor on-line sampler it is characterised in that：Reactor is originally additionally provided with stirring in vivo
Device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621041271.2U CN206002350U (en) | 2016-09-07 | 2016-09-07 | A kind of reactor on-line sampler |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621041271.2U CN206002350U (en) | 2016-09-07 | 2016-09-07 | A kind of reactor on-line sampler |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206002350U true CN206002350U (en) | 2017-03-08 |
Family
ID=58193898
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621041271.2U Expired - Fee Related CN206002350U (en) | 2016-09-07 | 2016-09-07 | A kind of reactor on-line sampler |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206002350U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110220748A (en) * | 2018-03-01 | 2019-09-10 | 山东新泰华高科食品检测有限公司 | Sampler is used in a kind of detection of liquid food |
-
2016
- 2016-09-07 CN CN201621041271.2U patent/CN206002350U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110220748A (en) * | 2018-03-01 | 2019-09-10 | 山东新泰华高科食品检测有限公司 | Sampler is used in a kind of detection of liquid food |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101975865B (en) | Automatic titration system for acid or alkali liquor | |
| CN201444119U (en) | On-line sampling device of reaction kettle | |
| CN107271707A (en) | The sampling device of a kind of sampler and the use device, detecting system | |
| CN206002350U (en) | A kind of reactor on-line sampler | |
| CN208999113U (en) | Reactor process sampler | |
| CN207153733U (en) | Chromatography gas bottle | |
| CN206248393U (en) | A kind of reaction kettle of the esterification multidraw device | |
| CN205333371U (en) | Empty gas analysis of branch that can arrange sweeping gas outward concentrates sample cabinet | |
| CN104764894B (en) | Full-automatic gas sample retention device | |
| CN106769346B (en) | Method for analyzing hydrogen isotopes in water | |
| CN207133265U (en) | It is a kind of to be used for compost or the reactor of sewage inventory of gas emission monitoring | |
| CN211856046U (en) | Device for collecting soil breathing gas | |
| CN107449930A (en) | A kind of liquid keeps sample sampler | |
| CN207456856U (en) | Device is measured by sampling in a kind of material in reactor PH | |
| CN210051719U (en) | Automatic on-line detection device for crude oil hydrogen sulfide | |
| CN111366423A (en) | Device for collecting soil breathing gas and gas collecting method | |
| CN207164077U (en) | A kind of liquid keeps sample sampler | |
| CN107631906A (en) | A kind of sampler | |
| CN209727916U (en) | Water quality on-line analysis system | |
| CN206683989U (en) | Negative reaction device sampler | |
| CN209014301U (en) | A kind of extraction element and automatic extractor for hydrolyzable nitrogen measurement | |
| CN206420895U (en) | It is a kind of to possess the automatic sampler for clearing up function | |
| CN206772945U (en) | It is a kind of can measuring pressure depolymerization experimental provision | |
| CN207336132U (en) | A kind of sampler | |
| CN214277553U (en) | PH value detection device of vacuum sampling |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 361000 Fujian province Xiamen torch hi tech Zone (Xiangan) Industrial Zone neian Road No. 169 Co-patentee after: Kezhijie New Material Group Fujian Co.,Ltd. Patentee after: KZJ NEW MATERIALS GROUP Co.,Ltd. Address before: 361000 Fujian province Xiamen torch hi tech Zone (Xiangan) Industrial Zone neian Road No. 169 Co-patentee before: FUJIAN KZJ NEW MATERIALS Co.,Ltd. Patentee before: KZJ NEW MATERIALS GROUP Co.,Ltd. |
|
| CP01 | Change in the name or title of a patent holder | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170308 Termination date: 20210907 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |