CN205919987U - Reation kettle presses sampling system and reation kettle in area - Google Patents
Reation kettle presses sampling system and reation kettle in area Download PDFInfo
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- CN205919987U CN205919987U CN201620743322.XU CN201620743322U CN205919987U CN 205919987 U CN205919987 U CN 205919987U CN 201620743322 U CN201620743322 U CN 201620743322U CN 205919987 U CN205919987 U CN 205919987U
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- valve
- collecting tank
- blow
- reactor
- pressure
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Abstract
The utility model discloses a reaction kettle the area is pressed sampling system and is provided with this sampling system's reation kettle, and this system includes liquid -collecting tank, blow -down pipe, casting tube and take out material evacuation pipe, liquid -collecting tank passes through casting tube and high -pressure batch autoclave intercommunication, the blow -down pipe with the liquid -collecting tank intercommunication, take out material evacuation pipe and casting tube intercommunication, casting tube has set gradually first valve, second valve and third valve from high -pressure batch autoclave to liquid -collecting tank, still set up the cross sight glass between second valve and the third valve, is provided with the sample valve on the cross sight glass, be provided with four valves on the blow -down pipe, it is provided with the 5th valve on the material evacuation pipe to take out, the blow -down pipe with still be provided with the 6th valve between the casting tube. This system can solve reation kettle and in having the normal working process of pressure, take out cauldron internal reaction liquid at any time, carries out analytical test's problem, has effectively reduced the influence to the reaction to can steady in a long -termly use.
Description
Technical field
This utility model belongs to chemical industry, medical consersion unit field, in particular it relates to the industry such as a kind of chemical industry, medicine is anti-
Answer the sampler with pressure of kettle kind equipment, more particularly, to a kind of high, middle pressure reactor multiple sampler in the course of the work.
Background technology
In chemical industry, medical devices, reactor is as Chief equipment, particularly high, middle pressure reactor, reaction with pressure
Up to more than ten hour time, how not stop kettle in a certain stage, in the case of pressure release of not reducing pressure, taking out reactant liquor, divide folding it is anti-
The result answered, thus accurately judging that reactive state, the always insurmountable difficult problem in this area.
Currently for the sampling of reactor reactant liquor with pressure, conventional way can only be stopped kettle, after pressure release, take in kettle
Go out reactant liquor, be analyzed chemically examining.And stop kettle, pressure release means that and stopped reaction.If the result of analysis is undesirable, it is then turned on
Stirring, heats up, boosting continues reaction.Energy consumption, material consumption, the delay of time etc., cause certain loss.
Content of the invention
This utility model purpose is to solve reactor in the course of normal operation having pressure, takes out reaction in kettle at any time
Liquid, the problem being analyzed chemically examining, a kind of new sampler with pressure is provided, solves reactor with pressure in course of normal operation
The problem of sampling, reduces the impact to reaction.
To achieve these goals, this utility model provides a kind of reactor sampler with pressure, and this sampler includes
Liquid collecting tank, blow-down pipe, liquid discharging tube and take out material evacuated tube, described liquid collecting tank is connected with autoclave by described liquid discharging tube, institute
State blow-down pipe to connect with described liquid collecting tank, described material evacuated tube of taking out is connected with liquid discharging tube；Described liquid discharging tube from autoclave to
Liquid collecting tank is disposed with the first valve, the second valve and the 3rd valve, also sets up four between the second valve and the 3rd valve
Way view mirror, four way view mirrors are provided with sampling valve；4th valve is provided with blow-down pipe；Take out and be provided with the 5th valve in material evacuated tube
Door；It is additionally provided with the 6th valve between described blow-down pipe and described liquid discharging tube.
Preferably, described sampling valve is connected with four way view mirrors by mounting seat, and the sample tap of described sampling valve is provided with silicon
Rubber cushion and the gland of compression silicagel pad.The size of described four way view mirrors can determine as needed, for example with dn25 model.
The thickness of described silicagel pad can be 3mm.
Preferably, described first valve, the second valve, the 3rd valve, the 4th valve, the 5th valve and the 6th valve difference
It independently is needle valve or ball valve.
It is further preferred that described first valve, the second valve and the 3rd valve are ball valve；Described 4th valve,
Five valves and the 6th valve are needle valve.
In this utility model, for the first valve, the second valve, the 3rd valve, the 4th valve, the 5th valve and the 6th
The size of valve is not special to be required, and can sample demand according to real reaction and determine, the such as first valve, the second valve
Door, the 3rd valve can adopt dn25 model.4th valve, the 5th valve and the 6th valve can adopt dn15 model.
Preferably, liquid collecting pot bottom is inserted in described liquid discharging tube and the connection end of liquid collecting tank.
This utility model also provides a kind of reactor, and this reactor is provided with above-mentioned reactor sampler with pressure.
Compared with prior art, the reactor sampler with pressure that this utility model provides, can solve the problem that reactor is having
In the course of normal operation of pressure (such as middle high-pressure), take out reactant liquor in kettle at any time, be analyzed the problem of chemical examination, effectively
Decrease the impact to reaction；Reactor of the present utility model sampler with pressure can use steadily in the long term, such as maximal pressure
In the case of reaching 1.2mpa, still normally used using more than 8 years.
Other features and advantages of the utility model will be described in detail in subsequent specific embodiment part.
Brief description
Accompanying drawing is used to provide and further understands to of the present utility model, and constitutes a part for description, and following
Specific embodiment be used for together explaining this utility model, but do not constitute to restriction of the present utility model.In the accompanying drawings:
Fig. 1 is reactor sampler with pressure system schematic；
Fig. 2 is the structural representation of sampling valve；
Description of reference numerals
1st, liquid collecting tank, the 2, the 4th valve, the 3, the 3rd valve, 4, sampling valve, the 5, the 6th valve, the 6, the 5th valve, 7, four-way
Visor, the 8, second valve, 9, take out material blow-down pipe, 10, liquid discharging tube, 11, blow-down pipe, 12, mounting seat, 13, silicagel pad, 14, gland,
15th, the first valve.
Specific embodiment
Hereinafter specific embodiment of the present utility model is described in detail.It should be appreciated that it is described herein
Specific embodiment is merely to illustrate and explains this utility model, is not limited to this utility model.
With reference to Fig. 1 and Fig. 2, a kind of reactor sampler with pressure, this sampler includes liquid collecting tank 1, blow-down pipe 11, puts
Liquid pipe 10 is connected with autoclave by described liquid discharging tube 11 with taking out material evacuated tube 9, described liquid collecting tank 1, described blow-down pipe 10
Connect with described liquid collecting tank 1, described material evacuated tube 9 of taking out is connected with liquid discharging tube 10；Described liquid discharging tube 10 is from autoclave to collection
Flow container 1 is disposed with the first valve 15, the second valve 8 and the 3rd valve 3, also sets between the second valve 8 and the 3rd valve 3
Put four way view mirrors 7, four way view mirrors 7 are provided with sampling valve 4；4th valve 2 is provided with blow-down pipe 11；Take out in material evacuated tube 8
It is provided with the 5th valve 6；It is additionally provided with the 6th valve 5 between described blow-down pipe 11 and described liquid discharging tube 10.
Mounting seat 12 is directly welded on four way view mirrors 7, and described sampling valve 4 is arranged in mounting seat 12, described sampling valve 4
Sample tap is provided with silicagel pad 13 and the gland 14 of compression silicagel pad 13.During sampling, after opening sampling valve 4, long needle-penetration silicon
Rubber cushion 13, extracts the reactant liquor in four way view mirrors 7.
Described first valve 15, the second valve 8 and the 3rd valve 3 are ball valve；Described 4th valve 2, the 5th valve 6 and
6th valve 5 is needle valve.
The bottom of liquid collecting tank 1 is inserted in the connection end of described liquid discharging tube 10 and liquid collecting tank 1.
The operation principle of reactor system with pressure and operating process are as described below: open the 4th valve 2, by blow-down pipe
11, it is vented to liquid collecting tank 1, opens the 3rd valve 3 and the second valve 8, the stagnant liquid in liquid discharging tube 10 is flowed into liquid collecting tank 1, close
Close the 3rd valve 3 and the second valve 8, open the 6th valve 5, be vented to four way view mirrors 7 and pipeline, slowly crack second valve 8,
Observe when having material in four way view mirrors 7, close the second valve 8, open sampling valve 4, with the reactant liquor in minute hand extraction conduit, that is, complete
Become this sub-sampling.As needed, repeatedly sample.After the completion of sampling, open the 3rd valve 3 and the 5th valve 6, by liquid collecting
Material in tank 1 passes through to take out expects that blow-down pipe 9 is drained only.
Using on the alkylation reaction kettle of antioxidant factory, this kettle amasss and is aforesaid reaction vessel sampler with pressure
12m3, maximum working pressure reaches 1.2mpa, normally using always in the time more than 8 years.Solve pressure reaction still very well to exist
Problem of sampling in normal work.
Preferred implementation of the present utility model described in detail above, but, this utility model is not limited to above-mentioned reality
Apply the detail in mode, in range of the technology design of the present utility model, the technical solution of the utility model can be entered
The multiple simple variant of row, these simple variant belong to protection domain of the present utility model.
It is further to note that each particular technique feature described in above-mentioned specific embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, this utility model is to each
Plant possible compound mode no longer separately to illustrate.
Additionally, combination in any can also be carried out, as long as it is not disobeyed between various different embodiment of the present utility model
Carry on the back thought of the present utility model, it equally should be considered as content disclosed in the utility model.
Claims (7)
1. a kind of reactor sampler with pressure, this system includes liquid collecting tank, blow-down pipe, liquid discharging tube and takes out material evacuated tube, described
Liquid collecting tank is connected with autoclave by described liquid discharging tube, and described blow-down pipe is connected with described liquid collecting tank, and described material of taking out empties
Pipe is connected with liquid discharging tube；Described liquid discharging tube be disposed with from autoclave to liquid collecting tank the first valve, the second valve and
3rd valve, also sets up four way view mirrors between the second valve and the 3rd valve, and four way view mirrors are provided with sampling valve；On blow-down pipe
It is provided with the 4th valve；Take out and be provided with the 5th valve in material evacuated tube；It is additionally provided between described blow-down pipe and described liquid discharging tube
6th valve.
2. reactor sampler with pressure according to claim 1 it is characterised in that described sampling valve pass through mounting seat with
Four way view mirrors connect, and the sample tap of described sampling valve is provided with silicagel pad and the gland of compression silicagel pad.
3. reactor sampler with pressure according to claim 1 it is characterised in that described first valve, the second valve,
3rd valve, the 4th valve, the 5th valve and the 6th valve are separately needle valve or ball valve.
4. reactor according to claim 3 sampler with pressure is it is characterised in that described first valve, the second valve
It is ball valve with the 3rd valve；Described 4th valve, the 5th valve and the 6th valve are needle valve.
5. reactor sampler with pressure according to claim 4 it is characterised in that described first valve, the second valve,
3rd valve is the ball valve of dn25 model；4th valve, the 5th valve and the 6th valve are the needle valve of dn15 model.
6. reactor sampler with pressure according to claim 1 is it is characterised in that the company of described liquid discharging tube and liquid collecting tank
Connect end insertion liquid collecting pot bottom.
7. a kind of reactor is it is characterised in that be provided with the reactor described in any one in claim 1-6 on this reactor
Sampler with pressure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620743322.XU CN205919987U (en) | 2016-07-14 | 2016-07-14 | Reation kettle presses sampling system and reation kettle in area |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620743322.XU CN205919987U (en) | 2016-07-14 | 2016-07-14 | Reation kettle presses sampling system and reation kettle in area |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205919987U true CN205919987U (en) | 2017-02-01 |
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ID=57872897
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620743322.XU Active CN205919987U (en) | 2016-07-14 | 2016-07-14 | Reation kettle presses sampling system and reation kettle in area |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205919987U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108318370A (en) * | 2018-01-05 | 2018-07-24 | 西南石油大学 | The device and its assay method with pressure for measuring paraffin remover the speed of paraffin dissolution and recovery ratio |
-
2016
- 2016-07-14 CN CN201620743322.XU patent/CN205919987U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108318370A (en) * | 2018-01-05 | 2018-07-24 | 西南石油大学 | The device and its assay method with pressure for measuring paraffin remover the speed of paraffin dissolution and recovery ratio |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20211210 Address after: 276000 chemical industry park of Lingang Economic Development Zone, Linyi City, Shandong Province (taohuayu village, tuanlin town) Patentee after: SHANDONG SANFENG NEW MATERIAL CO.,LTD. Address before: 276034 No.167 Sanhe East Street, Hedong District, Linyi City, Shandong Province Patentee before: SHANDONG LINYI SUNNY WEALTH CHEMICALS CO.,LTD. |
|
| TR01 | Transfer of patent right |