CN208187760U - A kind of convenient sampler of closed reactor - Google Patents
A kind of convenient sampler of closed reactor Download PDFInfo
- Publication number
- CN208187760U CN208187760U CN201820385871.3U CN201820385871U CN208187760U CN 208187760 U CN208187760 U CN 208187760U CN 201820385871 U CN201820385871 U CN 201820385871U CN 208187760 U CN208187760 U CN 208187760U
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- China
- Prior art keywords
- reaction kettle
- conduit
- module
- sampling bottle
- control valve
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- 238000005070 sampling Methods 0.000 claims abstract description 31
- 238000006243 chemical reaction Methods 0.000 claims abstract description 28
- 238000003780 insertion Methods 0.000 claims abstract description 15
- 230000037431 insertion Effects 0.000 claims abstract description 15
- 239000000376 reactant Substances 0.000 claims abstract description 10
- 238000012545 processing Methods 0.000 claims description 23
- 238000000605 extraction Methods 0.000 claims description 3
- 239000000284 extract Substances 0.000 abstract description 4
- 239000012495 reaction gas Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 5
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007805 chemical reaction reactant Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Sampling And Sample Adjustment (AREA)
Abstract
The utility model innovation discloses a kind of convenient sampler of closed reactor, including reaction kettle and sampling bottle, further include for by reaction kettle reactant extract out vacuum withdraw device, across reaction kettle shell and can extend into as needed the insertion tube and insertion tube of reaction kettle different height position outside reaction kettle one end connection control valve, the opposite other end that the control valve is connect with insertion tube pass through a conduit three-way device connect respectively with vacuum withdraw device and sampling bottle.Vacuum withdraw device is set in the utility model and control valve extracts the reactant inside closed reactor by conduit, can effectively simplify operation, prevents reaction gas reactor from coming out pollution site environment.To achieve the effect that protect environment.
Description
Technical field
The utility model belongs to the convenient sampler of reaction kettle monitoring field more particularly to a kind of closed reactor.
Background technique
In Chemical Manufacture, the response situation needs of reaction mass are monitored sampling in closed reactor.Existing
In technology, sampling process is to open closed feeding port to carry out sample acquisition, but often carry out feeding port in reaction process
Opening and closing is not conducive to closing and the opening and " locked in " operation of feeding port are relatively complicated, often time-consuming and laborious, meanwhile, in reaction process
Being opened to feeding port can also allow reaction gas reactor to come out pollution site environment.
Utility model content
The purpose of the utility model is to overcome the deficiencies in the prior art, provide a kind of convenient sampling dress of closed reactor
It sets, can effectively simplify operation, protect environment.
To realize the purpose, the utility model provides a kind of convenient sampler of closed reactor, including reaction kettle
And sampling bottle, further include for by reaction kettle reactant extract out vacuum withdraw device, across the shell and energy of reaction kettle
It reaches and extend into the insertion tube of reaction kettle different height position as needed, connect with one end outside reaction kettle of insertion tube
Control valve, the opposite other end that the control valve is connect with insertion tube by a conduit three-way device respectively with vacuum withdraw device
It is connected with sampling bottle.
Preferably, one end that the conduit three-way device is connect with sampling bottle is inserted into inside sampling bottle and and sampling bottle
It is detachably connected.
Preferably, the conduit three-way device is conduit tee tube.
Preferably, this sampler is additionally provided with controller, and the controller includes processing module and processing module signal
It connects the switch module for being used to respectively control the work of control valve and vacuum withdraw device, connect with processing module signal
For sampling the button module of control, the processing module is connect with vacuum withdraw device signal.
Preferably, the controller is additionally provided with for extracting indicative indicating lamp module, the finger to reactant
Show that lamp module is connect with processing module signal.
The utility model compared with prior art, the beneficial effect is that:
Vacuum withdraw device and control valve are set in the present invention by conduit to the reaction inside closed reactor
Object is extracted, and operation can be effectively simplified, and prevents reaction gas reactor from coming out pollution site environment.To reach guarantor
The effect in retaining ring border.After conduit tee tube and sampling bottle are vacuumized by setting vacuum evacuation device in the present invention
Reactant extraction is carried out opening control valve, can effectively control the extraction amount of reactant, so that control is more ingenious and saves
The energy.It is just able to carry out sampling by pressing button module in the present invention, so that integrated operation is simpler.
Detailed description of the invention
FIG. 1 is a schematic structural view of the utility model;
Fig. 2 is that the utility model further deepens structural schematic diagram;
Fig. 3 is the utility model control structure block diagram.
Specific embodiment
The technical solution of the utility model, but the protection scope of the utility model are described in further detail with reference to the accompanying drawing
It is not limited to as described below.
Embodiment one
As shown in Figure 1, a kind of convenient sampler of closed reactor, including reaction kettle 1 and sampling bottle 2, it further include using
In by reaction kettle 1 reactant extract out vacuum withdraw device 3, across reaction kettle 1 shell and can protrude into as needed
Insertion tube 6, the control valve 5 that is connect with one end outside reaction kettle 1 of insertion tube 6 to 1 different location of reaction kettle, control valve
5 opposite other end connecting with insertion tube 6 are connected with vacuum withdraw device 3 and sampling bottle 2 respectively by a conduit three-way device 4
It connects.
One end that conduit three-way device 4 is connect with sampling bottle 2 is inserted into the inside of sampling bottle 2 and detachable with sampling bottle 2
Connection.Conduit three-way device 4 is conduit tee tube.
In the present embodiment, the position that insertion tube 6 passes through 1 shell of reaction kettle is sealed processing, avoids the gas of reaction kettle
Body comes out.Conduit three-way device 4 can be detachably connected with vacuum withdraw device 3 and control valve 5 respectively.
In the present embodiment, when needing to be sampled, vacuum withdraw device 3 first is opened by conduit three-way device 4 and is adopted
Sample bottle 2 carries out vacuumize process, after the completion of vacuumize process, closes vacuum withdraw device 3 and opens control valve 5, so that reaction
Reactant is pushed into sampling bottle 2 through insertion tube 6 and conduit three-way device 4 and under the action of pressure difference in kettle 1, reaches sampling
Purpose.
Embodiment two
As shown in Fig. 2-Fig. 3, the present embodiment is with the difference of embodiment one: this sampler is additionally provided with controller 7, control
Device 7 processed is connect for respectively to the work of control valve 5 and vacuum withdraw device 3 including processing module 71, with 71 signal of processing module
The switch module 72 that is controlled is connect for sample the button module 73 controlled, processing module with 71 signal of processing module
71 connect with 3 signal of vacuum withdraw device.Controller 7 is additionally provided with for extracting indicative indicating lamp module to reactant
74, indicating lamp module 74 is connect with 71 signal of processing module.Switch module 72 is by respectively to control valve 5 and vacuum withdraw device 3
Work controlled relay composition.
In the present embodiment, indicating lamp module 74 is LED light, and during being sampled, the control of processing module 71 refers to
Show that lamp module 74 is flashed, to be sampled prompt.Button module 73 is sampled control for staff, and work people
Member presses button module 73, and then processing module 71 is controlled and is sampled automatically.Vacuum withdraw device 3 connects with conduit three-way device 4
Position is connect to be provided with pressure sensor and connect with 71 signal of processing module.
In the present embodiment, when needing to be sampled, staff presses button module 73, and processing module 71 receives
After signal, control switch module 72 opens vacuum withdraw device 3 and conduit three-way device 4 and sampling bottle 2 is carried out vacuumize process,
Show that pressure decline reaches in conduit three-way device 4 and sampling bottle 2 in the signal that vacuum withdraw device 3 feeds back to processing module 71
After setting value, processing module 71 closes vacuum withdraw device 3 by switch module 72 and opens control valve 5, so that anti-in reaction kettle 1
It answers object to be pushed into sampling bottle 2 by insertion tube 6 and conduit three-way device 4 and under the action of pressure difference, is examined in vacuum withdraw device 3
It measures conduit three-way device 4 and after 2 pressure recovery of sampling bottle reaches setting value, processing module 71 closes control by switch module 72
Valve 5 processed, achievees the purpose that sampling.
Above are merely preferred embodiments of the utility model, it should be understood that the utility model is not limited to be draped over one's shoulders herein
The form of dew, should not be regarded as an exclusion of other examples, and can be used for other combinations, modifications, and environments, and can
In this paper contemplated scope, modifications can be made through the above teachings or related fields of technology or knowledge.And those skilled in the art institute into
Capable modifications and changes do not depart from the spirit and scope of the utility model, then all should be in the guarantor of the appended claims for the utility model
It protects in range.
Claims (4)
1. a kind of convenient sampler of closed reactor, including reaction kettle (1) and sampling bottle (2), which is characterized in that further include
For by the vacuum withdraw device (3) of reaction kettle (1) interior reactant extraction, pass through reaction kettle (1) shell and being capable of basis
Need to extend into the insertion tube (6) of reaction kettle (1) different height position and the one end external in reaction kettle (1) of insertion tube (6)
The control valve (5) of connection, the opposite other end that the control valve (5) connect with insertion tube (6) pass through a conduit three-way device (4)
It is connect respectively with vacuum withdraw device (3) and sampling bottle (2);
This sampler is additionally provided with controller (7), and the controller (7) includes processing module (71) and processing module (71)
The switch module (72) and place that signal connection is used to respectively control the work of control valve (5) and vacuum withdraw device (3)
Reason module (71) signal connection is for sampling the button module (73) of control, the processing module (71) and vacuum withdraw device
(3) signal connects, the vacuum withdraw device (3) and conduit three-way device (4) link position be provided with pressure sensor and
Pressure sensor is connect with processing module (71) signal.
2. a kind of convenient sampler of closed reactor according to claim 1, which is characterized in that the conduit threeway
One end that device (4) is connect with sampling bottle (2) is inserted into sampling bottle (2) inside and is detachably connected with sampling bottle (2).
3. a kind of convenient sampler of closed reactor according to claim 1, which is characterized in that the conduit threeway
Device (4) is conduit tee tube.
4. a kind of convenient sampler of closed reactor according to claim 1, which is characterized in that the controller
(7) it is additionally provided with for extracting indicative indicating lamp module (74), the indicating lamp module (74) and processing to reactant
The connection of module (71) signal.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201820385871.3U CN208187760U (en) | 2018-03-21 | 2018-03-21 | A kind of convenient sampler of closed reactor |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201820385871.3U CN208187760U (en) | 2018-03-21 | 2018-03-21 | A kind of convenient sampler of closed reactor |
Publications (1)
Publication Number | Publication Date |
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CN208187760U true CN208187760U (en) | 2018-12-04 |
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CN201820385871.3U Active CN208187760U (en) | 2018-03-21 | 2018-03-21 | A kind of convenient sampler of closed reactor |
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CN (1) | CN208187760U (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114682204A (en) * | 2022-05-09 | 2022-07-01 | 广东日出化工有限公司 | Non-stop liquid taking mechanism in water-based acrylic emulsion synthesis stage |
-
2018
- 2018-03-21 CN CN201820385871.3U patent/CN208187760U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114682204A (en) * | 2022-05-09 | 2022-07-01 | 广东日出化工有限公司 | Non-stop liquid taking mechanism in water-based acrylic emulsion synthesis stage |
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Legal Events
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GR01 | Patent grant | ||
CP03 | Change of name, title or address |
Address after: 455000 intersection of Jingzhong Road and Xinglong Road in Tangyin County Industrial Park, Anyang City, Henan Province Patentee after: Henan Yongxin Chemical Co.,Ltd. Country or region after: China Address before: Intersection of Jingzhong road and Xinglong Road, industrial park, Tangyin County, Anyang City, Henan Province Patentee before: TANGYIN YONGXIN CHEMICAL Co.,Ltd. Country or region before: China |
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CP03 | Change of name, title or address |