CN205893456U - Single crystal growing furnace silicon solution liquid surface position detecting device and adjustment system - Google Patents

Single crystal growing furnace silicon solution liquid surface position detecting device and adjustment system Download PDF

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Publication number
CN205893456U
CN205893456U CN201620441734.8U CN201620441734U CN205893456U CN 205893456 U CN205893456 U CN 205893456U CN 201620441734 U CN201620441734 U CN 201620441734U CN 205893456 U CN205893456 U CN 205893456U
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China
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measurement end
liquid level
solution
silicon liquid
input part
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CN201620441734.8U
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Chinese (zh)
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时刚
武海军
张灵鸽
赵辉
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XI'AN CHUANGLIAN NEW ENERGY EQUIPMENT CO Ltd
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XI'AN CHUANGLIAN NEW ENERGY EQUIPMENT CO Ltd
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Abstract

The utility model provides a single crystal growing furnace silicon solution liquid surface position detecting device and the adjustment system who corresponds wherein should the device includes: signal input part, first measuring junction, second measuring junction and control system, wherein control system is used for to signal input part apply signal voltage to through the voltage signal who detects first measuring junction and second measuring junction, the voltage signal who acquires first measuring junction and second measuring junction detects the state, according to the voltage signal detection state, the formation is used for instructing silicon solution liquid surface whether to be in the testing result of reasonable position. The utility model discloses utilize the electric conductivity of silicon solution, after to signal input part apply signal voltage, through the voltage signal detection state that acquires first measuring junction and second measuring junction, automatic and accuracy detects silicon solution liquid surface position to accurate judge whether silicon solution liquid surface is in equitable position, and further carry out corresponding adjustment to the crucible position, make silicon solution liquid surface remain throughout in equitable position.

Description

Single crystal growing furnace silicon liquid level of solution position detecting device and adjustment system
Technical field
The utility model is related to monocrystalline silicon preparing technical field, more particularly, to a kind of single crystal growing furnace silicon liquid level of solution position detection Device and adjustment system.
Background technology
Czochralski method mono-crystal furnace, during production monocrystalline silicon, will experience evacuation leak detection, heating material, seeding, amplification turn Multiple stages such as shoulder, isometrical, ending.Wherein, it is accomplished by controlling silicon liquid level of solution position after seeding process starts, thus being crystalline substance Bulk-growth creates a suitable temperature field.
In this process, with the continuous growth of silicon single crystal bar, silicon liquid level of solution position can decrease, and is at this moment accomplished by It is adjusted by crucible lifting system, to keep the constant of liquid level position.In existing control system, using crucible lifting When being adjusted, it is a theoretical change according to obtained from multiple variable such as crucible shape, charge, speed of growth is through conversion Change value.So in actual production process, after being adjusted using this theoretical changing value, often occur liquid level position with Gradually step-down, until the situation of relatively large deviation, is at this moment accomplished by operator in real time to equipment state for the growth of silicon single crystal bar Modify, thus ensureing being smoothed out of production process.Therefore, automatic simultaneously accurate detection silicon liquid level of solution position, and in inspection After measuring silicon liquid level of solution position, silicon liquid level of solution position is accurately adjusted to rational position, for prevent above-mentioned the occurrence of It is of great significance with the automatization level tool improving equipment.
Utility model content
The utility model provides a kind of single crystal growing furnace silicon liquid level of solution position detecting device, to solve to cannot oneself in prior art The problem of dynamic simultaneously accurate detection silicon liquid level of solution position.
The utility model also provides a kind of single crystal growing furnace silicon liquid level of solution position adjustment, so that solve cannot in prior art Silicon liquid level of solution is accurately adjusted to the problem of rational position.
In a first aspect, the utility model provides a kind of single crystal growing furnace silicon liquid level of solution position detecting device, described device includes:
Signal input part, the lower surface of wherein said signal input part is always positioned at the lower section of described silicon liquid level of solution;
First measurement end and the second measurement end, the lower surface of wherein said first measurement end and described second measurement end is respectively Flush with the extreme higher position of the rational position of described silicon liquid level of solution and extreme lower position;
Control system, for described signal input part input voltage signal, and by detect described first measurement end and The voltage signal of described second measurement end, obtains the voltage signal detection shape of described first measurement end and described second measurement end State;State is detected according to described voltage signal, generates for indicating whether described silicon liquid level of solution is in the detection of rational position Result.
As the preferred embodiment of the utility model second aspect, described device also includes:
Machinery adjustment unit, for adjusting described signal input part, described first measurement end and described second measurement end Position, makes the lower surface of described signal input part be always positioned at the lower section of described silicon liquid level of solution, makes described first measurement simultaneously End and lower surface extreme higher position and the extreme lower position with the rational position of described silicon liquid level of solution respectively of described second measurement end Flush.
As the preferred embodiment of the utility model second aspect, described signal input part, described first measurement end and described Second measurement end is made by rhenium metal material.
As the preferred embodiment of the utility model second aspect, described control system includes plc and industrial computer, described plc Be connected with described industrial computer, described plc also respectively with described signal input part, described first measurement end and described second measurement end Connect.
Second aspect, the utility model provides a kind of single crystal growing furnace silicon liquid level of solution position adjustment, and described system includes:
Crucible adjustment unit, for being adjusted to the position of crucible according to the silicon liquid level of solution position detecting, makes institute State silicon liquid level of solution and be in rational position;
And, single crystal growing furnace silicon liquid level of solution position detecting device as described in relation to the first aspect.
Single crystal growing furnace silicon liquid level of solution method for detecting position and device that the utility model provides, using the conduction of silicon solution Property, to after signal input part input voltage signal, detected by obtaining the voltage signal of the first measurement end and the second measurement end State, automatic and accurate detection silicon liquid level of solution position, thus accurately judge whether silicon liquid level of solution is in reasonable position further Put.In addition, the single crystal growing furnace silicon liquid level of solution position adjustment that the utility model provides, it is being accurately detected silicon liquid level of solution position Postpone, by adjusting accordingly to the bushing position in single crystal growing furnace, make silicon liquid level of solution remain at rational position, thus Crystal remains at the growth of the most preferable, most suitable position in growth course, makes whole growth course smooth.
Brief description
In order to be illustrated more clearly that the technical scheme in the utility model embodiment, below will be to required in embodiment description Accompanying drawing to be used be briefly described it should be apparent that, drawings in the following description are only that of the present utility model some are real Apply example, for those of ordinary skill in the art, on the premise of not paying creative work, can also be according to these accompanying drawings Obtain other accompanying drawings.
A kind of flow chart of single crystal growing furnace silicon liquid level of solution method for detecting position that Fig. 1 provides for the utility model embodiment;
A kind of structural representation of single crystal growing furnace silicon liquid level of solution position detecting device that Fig. 2 provides for the utility model embodiment Figure;
Signal input in a kind of single crystal growing furnace silicon liquid level of solution position detecting device that Fig. 3 provides for the utility model embodiment The position view of end, the first measurement end and the second measurement end;
A kind of structural representation of single crystal growing furnace silicon liquid level of solution position adjustment that Fig. 4 provides for the utility model embodiment Figure.
Specific embodiment
For making the purpose of this utility model, technical scheme and advantage clearer, new to this practicality below in conjunction with accompanying drawing Type embodiment is described in further detail.
The utility model utilizes the electric conductivity of silicon solution, to after signal input part input voltage signal, single by obtaining The voltage signal detection state of the first measurement end of various location and the second measurement end in brilliant stove, thus judge this two surveys Amount end contact with silicon liquid level of solution situation, can determine whether out whether silicon liquid level of solution is in the conjunction needing during crystal growth further In reason position, generally this rational position is an altitude range, and that is, silicon liquid level of solution is in the altitude range of this rational position Shi Jingti all can be with normal growth, and therefore this rational position includes an extreme higher position and an extreme lower position.
The utility model embodiment discloses a kind of single crystal growing furnace silicon liquid level of solution method for detecting position, with reference to shown in Fig. 1, is somebody's turn to do Method includes:
S1, to signal input part input voltage signal, the lower surface of wherein signal input part is always positioned at silicon liquid level of solution Lower section;
S2, the voltage signal by detecting the first measurement end and the second measurement end, obtain the first measurement end and the second measurement The voltage signal detection state at end, the lower surface of the wherein first measurement end and the second measurement end is reasonable with silicon liquid level of solution respectively The extreme higher position of position and extreme lower position flush;
S3, according to voltage signal detect state, generate for indicating whether silicon liquid level of solution is in the detection of rational position Result.
Specifically, in step s3, if the first measurement end and the second measurement end all voltage signal is detected it is determined that silicon solution Liquid level is in the top of rational position;
If the first measurement end and the second measurement end are all not detected by voltage signal it is determined that silicon liquid level of solution is in reasonable position The lower section put;
If the first measurement end is not detected by voltage signal, the second measurement end voltage signal is detected it is determined that silicon solution liquid Face is in rational position.
Usually, the extreme higher position of this rational position and extreme lower position are both preferably 2mm, that is, with the distance of this rational position This rational position all can ensure that crystal normal growth in the range of lower deviation 2mm.Specifically, this rational position is according to existing The practical condition of field determines, specific determination process method known to those skilled in the art will not be described here.
The single crystal growing furnace silicon liquid level of solution method for detecting position that the utility model provides, using the electric conductivity of silicon solution, to After signal input part input voltage signal, detect state by obtaining the voltage signal of the first measurement end and the second measurement end, from Dynamic simultaneously accurate detection silicon liquid level of solution position, thus accurately judge whether silicon liquid level of solution is in rational position further.
The utility model embodiment also discloses a kind of single crystal growing furnace silicon liquid level of solution position detecting device, shown in reference Fig. 2, This device 20 includes:
The lower surface of signal input part 21, wherein signal input part is always positioned at the lower section of silicon liquid level of solution;
First measurement end 22 and the second measurement end 23, the lower surface of the wherein first measurement end 22 and the second measurement end 23 is respectively Flush with the extreme higher position of the rational position of silicon liquid level of solution and extreme lower position;
Machinery adjustment unit 24, for adjusting the position of signal input part 21, the first measurement end 22 and the second measurement end 23, Make the lower surface of signal input part 21 be always positioned at the lower section of silicon liquid level of solution, making the first measurement end 22 and the second measurement end simultaneously 23 lower surface is flushed with the extreme higher position of the rational position of silicon liquid level of solution and extreme lower position respectively;
Control system 25, for signal input part 21 input voltage signal, and by detecting the first measurement end 22 and the The voltage signal of two measurement ends 23, obtains the voltage signal detection state of the first measurement end 22 and the second measurement end 23;According to electricity Pressure signal detection state, generates for indicating whether silicon liquid level of solution is in the testing result of rational position.
In original state, silicon liquid level of solution is in the rational position needing during crystal growth, by machinery adjustment list The position of unit 24 pre-adjusting signal input part 21 is it is ensured that the lower surface of signal input part 21 is always positioned under silicon liquid level of solution Side, then adjusts the first measurement end 22 and the position of the second measurement end 23 again, makes the first measurement end 22 and the second measurement end 23 Lower surface is flushed with the extreme higher position of this rational position and extreme lower position respectively, now the first measurement end 22 and the second measurement end 23 Lower surface respectively be located at this silicon liquid level of solution above and below, referring in particular to shown in Fig. 3.Usually, this rational position Extreme higher position and extreme lower position are both preferably 2mm with the distance of this rational position.
Specifically, control system 25 includes plc and industrial computer, is generally arranged at the outside away from single crystal growing furnace.Signal input End the 21, first measurement end 22 and the second measurement end 23 cause outside single crystal growing furnace by high temperature resistant wire, further with plc respectively Connect.To after signal input part 21 input voltage signal, within certain interval time, plc passes through to detect the first measurement end 22 and second measurement end 23 voltage signal, to judge silicon liquid level of solution position.
Plc is also connected with industrial computer, can realize interacting between operating personnel and control system 25 using this industrial computer.
Further, since silicon solution temperature is higher, and electric conductivity is poor, therefore signal input part 21, the first measurement end 22 Made by by rhenium metal material with the second measurement end 23, there is preferably high temperature resistant and electric conductivity.
The single crystal growing furnace silicon liquid level of solution position detecting device that the utility model provides, using the electric conductivity of silicon solution, to After signal input part input voltage signal, detect state by obtaining the voltage signal of the first measurement end and the second measurement end, from Dynamic simultaneously accurate detection silicon liquid level of solution position, thus accurately judge whether silicon liquid level of solution is in rational position further.
The utility model embodiment also provides a kind of single crystal growing furnace silicon liquid level of solution position adjustment, with reference to shown in Fig. 4, is somebody's turn to do System includes:
Crucible adjustment unit 41, for being adjusted to the position of crucible according to the silicon liquid level of solution position detecting, makes Silicon liquid level of solution is in rational position;
And, the single crystal growing furnace silicon liquid level of solution position detecting device 42 as described in above-described embodiment.
Wherein, crucible adjustment unit 41 and control system in described single crystal growing furnace silicon liquid level of solution position detecting device 42 Plc connects, thus realizing the position of crucible is adjusted under the control of plc.
Before whole adjustment system operation, first in plc, default single adjusts adjustment stroke during crucible up or down And the speed of service.To after signal input part input voltage signal, within certain interval time, plc passes through to detect the first survey Amount end and the voltage signal of the second measurement end, to judge silicon liquid level of solution position.After plc judges silicon liquid level of solution position, Determine whether out the state of needs adjustment, and export corresponding signal to control crucible adjustment unit 41 that the position of crucible is carried out Adjustment.Now by detecting the voltage signal of the first measurement end and the second measurement end, plc still can judge that silicon liquid level of solution is real-time Position after adjustment, once silicon liquid level of solution is detected and be in rational position, stops adjusting.
Crucible adjustment unit 41 is adjusted to crucible according to default adjustment stroke and the speed of service, default reaching After single adjustment stroke up or down, when silicon liquid level of solution is still detected and being not in rational position, plc stops to crucible Adjustment, and remind operating personnel to carry out manual confirmation to silicon liquid level of solution position by industrial computer, then further according to manual confirmation Actual conditions afterwards carry out corresponding operating, thus operating accident can effectively anti-locking system because of misjudgment.Specifically, need The situation of manual confirmation to be carried out has following two, and one kind is when the first measurement end and the second measurement end are all not detected by voltage letter Number, after reaching default single adjustment stroke upwards, when the second measurement end is still not detected by voltage signal, this kind of detection knot Fruit shows the lower section still in rational position for the silicon liquid level of solution;Another kind is when the first measurement end and the second measurement end all detect Voltage signal, after reaching the downward adjustment stroke of default single, when the first measurement end still detects voltage signal, Ci Zhongjian Survey result and show the top still in rational position for the silicon liquid level of solution.
Additionally, plc can be entered with variables such as the binding crystal speed of growth, crystal diameter, single crystal growing furnace in-furnace temperature, brilliant lifting speeds Row self-adaptative adjustment, thus improve the whole automatization level adjusting system.
The single crystal growing furnace silicon liquid level of solution position adjustment that the utility model provides, is being accurately detected silicon liquid level of solution position Postpone, by adjusting accordingly to the bushing position in single crystal growing furnace, make silicon liquid level of solution remain at rational position, thus Crystal remains at the growth of the most preferable, most suitable position in growth course, makes whole growth course smooth.
The foregoing is only preferred embodiment of the present utility model, not in order to limit the utility model, all in this practicality Within new spirit and principle, any modification, equivalent substitution and improvement made etc., should be included in guarantor of the present utility model Within the scope of shield.

Claims (5)

1. a kind of single crystal growing furnace silicon liquid level of solution position detecting device is it is characterised in that described device includes:
Signal input part, the lower surface of wherein said signal input part is always positioned at the lower section of described silicon liquid level of solution;
First measurement end and the second measurement end, the lower surface of wherein said first measurement end and described second measurement end respectively with institute State the extreme higher position of the rational position of silicon liquid level of solution and extreme lower position flushes;
Control system, for described signal input part input voltage signal, and by detecting described first measurement end and described The voltage signal of the second measurement end, obtains the voltage signal detection state of described first measurement end and described second measurement end;Root Detect state according to described voltage signal, generate for indicating whether described silicon liquid level of solution is in the testing result of rational position.
2. device according to claim 1 is it is characterised in that described device also includes:
Machinery adjustment unit, for adjusting the position of described signal input part, described first measurement end and described second measurement end, Make the lower surface of described signal input part be always positioned at the lower section of described silicon liquid level of solution, making described first measurement end and institute simultaneously The lower surface stating the second measurement end is flushed with the extreme higher position of the rational position of described silicon liquid level of solution and extreme lower position respectively.
3. device according to claim 1 is it is characterised in that described signal input part, described first measurement end and described Second measurement end is made by rhenium metal material.
4. device according to claim 1 is it is characterised in that described control system includes plc and industrial computer, described plc Be connected with described industrial computer, described plc also respectively with described signal input part, described first measurement end and described second measurement end Connect.
5. a kind of single crystal growing furnace silicon liquid level of solution position adjustment is it is characterised in that described system includes:
Crucible adjustment unit, for being adjusted to the position of crucible according to the silicon liquid level of solution position detecting, makes described silicon Liquid level of solution is in rational position;
And, the single crystal growing furnace silicon liquid level of solution position detecting device as any one of Claims 1-4.
CN201620441734.8U 2016-05-16 2016-05-16 Single crystal growing furnace silicon solution liquid surface position detecting device and adjustment system Expired - Fee Related CN205893456U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105821469A (en) * 2016-05-16 2016-08-03 西安创联新能源设备有限公司 Single crystal furnace silicon solution liquid level position detection method and device and adjusting system
WO2020134555A1 (en) * 2018-12-28 2020-07-02 宁夏隆基硅材料有限公司 Seed crystal fusion method and device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105821469A (en) * 2016-05-16 2016-08-03 西安创联新能源设备有限公司 Single crystal furnace silicon solution liquid level position detection method and device and adjusting system
WO2020134555A1 (en) * 2018-12-28 2020-07-02 宁夏隆基硅材料有限公司 Seed crystal fusion method and device

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