CN205886913U - Novel connect liquid device - Google Patents
Novel connect liquid device Download PDFInfo
- Publication number
- CN205886913U CN205886913U CN201620627107.3U CN201620627107U CN205886913U CN 205886913 U CN205886913 U CN 205886913U CN 201620627107 U CN201620627107 U CN 201620627107U CN 205886913 U CN205886913 U CN 205886913U
- Authority
- CN
- China
- Prior art keywords
- liquid
- bottle
- connects
- connect
- liquid bottle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model provides a novel connect liquid device, including meeting liquid tail pipe, a liquid collection bottle, the 2nd liquid collection bottle, the 3rd liquid collection bottle and fourth liquid collection bottle, connect the liquid tail pipe to have a gas outlet and a branch liquid piston. There are piston, first passageway and second channel on the branch liquid piston. The utility model provides a novel connect liquid device, whole connect liquid device installation with dismantle simple and convenient, can effectual receipts multicomponent result, can solve the problem of distilling change liquid collection bottle.
Description
Technical field
This utility model belongs to experimental biotechnology field and in particular to a kind of Novel connecting liquid device.
Background technology
Whether in biotic experiment, or in chemical experiment, decompression or air-distillation carry out isolated or purified to material
One of conventional meanses.Distilling apparatus generally comprise heater, reaction vessel, condensing units and connect liquid device, vacuum distillation
Also has a decompressor.The material generating during chemical or biological reactionss, different through its respective boiling point, from reaction
Be changed into liquid through condensing units in a gaseous form in container, finally via connect liquid device collect entrance connect in liquid bottle.In distillation
During, due to temperature from low to high, the material of different boiling points was distilled out of in the different time, and particularly some are lower boiling
Solvent or by-product, therefore in fluid collection procedure, need first by lower boiling collecting material, just can collect product.?
In experimentation, need to change and different connect liquid bottle, by the material under different temperatures separately, so that quickly complete reception purification
Different material, it is to avoid secondary pollution.In addition, in still-process, the volume easily occurring connecing within liquid bottle is not enough, needs to change
Connect the situation of liquid bottle, for vacuum distillation, be easily caused the phenomenon that reaction unit leaks air；Anhydrous and oxygen-free is subtracted
Pressure distillation is it is easier to make byproduct of reaction increase or product purity occur the problems such as impacted.
Cn 201520564011.2 discloses a kind of different boiling multicomponent distillation segregation apparatuss, and described different boiling is multigroup
Point separated device includes reaction unit, the first condensing units and the second condensing units；Described reaction unit includes electric jacket
And it is inserted with the there-necked flask of thermometer and spherical condensating tube；Described first condensing units include from the top down the band piston of grafting successively
Thermometer, still head, drum glass change mouth and receiving bottle；Described drum glass changes one end that mouth is connected with receiving bottle and is wrapped with
Electric blanket high temperature cloth, its other end is connected with there-necked flask；Described second condensing units include the straight condensation of mitered downwards successively
Pipe, adapter tube and receiving bottle；Straight cold finger connects still head.
Utility model content
For the deficiencies in the prior art, this utility model provide a kind of new connect liquid device, this appliance arrangement is simple, behaviour
Facilitate, can effectively receive multicomponent, the product of large volume can be received, solve the problems, such as still-process more changing-over liquid bottle.
For reaching above-mentioned purpose, this utility model provides a kind of following technical scheme: Novel connecting liquid device, including connecing liquid tail
Pipe, first connect liquid bottle, second connect liquid bottle, the 3rd connect liquid bottle and the 4th and connect liquid bottle, described second connects liquid bottle and the 3rd, and to connect liquid bottle logical
Cross communicating pipe connection, the 4th connects liquid bottle and the 3rd is connect liquid bottle and connected by communicating pipe.
The described liquid tail pipe that connects directly is connected with the condensing tube of distillation reaction device.
The described liquid tail pipe that connects has a gas outlet and a separatory stopcock.
Piston, first passage and second channel are had on described separatory stopcock, controls reaction drop to pass through by rotating piston
First passage or second channel；One end of described first passage is communicated with first liquid delivery line, and the other end is filled with distillation reaction
Put and communicate；Described second channel one end is communicated with second liquid delivery line, and the other end is communicated with distillation reaction device.
It is provided with two ports in left and right and intermediate piston described communicating pipe.
There are the second opening and the 3rd opening in the described 3rd bottle both sides connecing liquid bottle, the position of two of which opening can more than
Under somewhat stagger or parallel.
Described second connects liquid bottle and there is the first opening the 4th bottle side connecing liquid bottle.
Described liquid delivery line is connect liquid bottle with first and is connected by ground, and described second connects liquid bottle is passed through with liquid delivery line
Ground connects, and the described 3rd connects liquid bottle and the 4th connects liquid bottle bottleneck bottle stopper.
The Novel connecting liquid device that this utility model provides, the described volume connecing liquid bottle is 10ml, 25ml, 50ml,
100ml, 150ml, 200ml etc., the amount of the height with specific reference to distillation reaction device and experiment is selected, in addition can basis
Particular situation decides whether to connect liquid bottle using two or connects liquid bottle using five or even more.
In still-process, the amount of product and by-product number, determine to connect the number of liquid bottle.When distillation starts, will live
Plug rotation, to connecting liquid delivery line, receives lower boiling liquid；When temperature is increased to product boiling point, rotary-piston, by liquid
Body delivery line connects, and opens the piston on communicating pipe；Treat that second connects that liquid bottle is full, the 3rd connects liquid bottle the liquid close to half
During body, according to the situation of the liquid in reaction bulb, decide whether that connecting the 4th connects liquid bottle.In still-process, if there is anti-
Answer liquid in bottle more than the 4th situation connecing liquid bottle, before the 4th connects the connection of liquid bottle, the 4th connect liquid bottle in the middle of insertion the
Five connect liquid bottle, are carried out with the safety controlling reaction.
The beneficial effects of the utility model:
This utility model provides a kind of Novel connecting liquid device, rational in infrastructure, simple structure, improves the efficiency connecing liquid, subtracts
Few due to operating process accidentally lead to connect the situation of liquid bottle spilling, can effectively reduce secondary pollution, separation that can be effectively complete
Product, reduces laboratory operating procedures, the effectively cost-effective and time, can quickly reach detached effect.In addition, connecing liquid bottle
Switching simple, reduce the problem brought due to careless manipulation.Entirely connect liquid device, carry out in the environment of sealing, can control
The flow of liquid and avoid liquid overflow spill leakage, reduce potential safety hazard, ensure experimenter safety；Particularly some carry spinosity
Sharp property abnormal smells from the patient or the serious product still-process of corrosivity, improve the safety of changing-over liquid bottle；For vacuum distillation, energy
Ensure the sealing of whole reaction unit；Distillation procedure to anhydrous and oxygen-free, more effectively ensures the anhydrous of whole experiment process
Oxygen-free environment, improves the yield of product in terms of certain.Entirely connect liquid device installation and removal simple and convenient, and cost of manufacture
Low.
Brief description
Fig. 1 is the overall structure diagram of Novel connecting liquid device described in the utility model；
Fig. 2 is the structural representation of communicating pipe described in the utility model；
Fig. 3 is the structural representation connecing liquid bottle of both ends open described in the utility model；
Fig. 4 is the structural representation connecing liquid bottle of one end open described in the utility model.
In figure:
First passage 1, first liquid delivery line 2, first connect liquid bottle 3, second liquid delivery line 4, second connect liquid bottle 5,
Two passages 6, piston 7, bottle stopper 8, communicating pipe 9, intermediate piston the 10, the 3rd connect liquid bottle 11, the first opening 12, port 13, second open
Mouth the 14, the 3rd opening the 15, the 4th connects liquid bottle 16, connects liquid tail pipe 17, gas outlet 18, separatory stopcock 19.
Specific embodiment
With specific embodiment, this utility model is further described below, but this utility model is not subject to following embodiments
Restriction.
Embodiment 1
Referring to Fig. 1～4, this utility model provides a kind of Novel connecting liquid device, including connect liquid tail pipe 17, first connect liquid bottle 3,
Second connects liquid bottle the 5, the 3rd connects liquid bottle 11 and the 4th and connects liquid bottle 16, and described second connects liquid bottle 5 connects liquid bottle 11 with the 3rd and pass through to connect
Pipe 9 connects, and the 4th connects liquid bottle 16 connects liquid bottle 11 by connecting communicating pipe 9 with the 3rd.It is described that to connect liquid tail pipe 17 directly anti-with distillation
The condensing tube answering device connects.The described liquid tail pipe 17 that connects has a gas outlet 18 and a separatory stopcock 19.Described separatory stopcock
There are piston 7, passage 1 and passage 6 on 19, control reaction drop to pass through first passage 1 or second channel 6 by rotating piston 7；Institute
State and be provided with two ports 13 in left and right and intermediate piston 10 communicating pipe 9.The described 3rd bottle both sides connecing liquid bottle 11 have second to open
Mouth 14 and the 3rd opening 15, can somewhat stagger up and down in the position of two of which opening.Described second connects liquid bottle 5 and the 4th connects liquid
There is the first opening 12 the bottle side of bottle 16.Described first liquid delivery line 2 is connect liquid bottle 3 with first and is connected by ground, described
Second connects liquid bottle 5 is connected by ground with second liquid delivery line 4, and the described 3rd connects liquid bottle 11 and the 4th connects liquid bottle 16 bottleneck has
Bottle stopper 8.
When distillation starts, piston 7 is rotated to connecting liquid delivery line 2, receives lower boiling liquid；Treat that temperature is increased to
During product boiling point, rotary-piston 7, second liquid delivery line 4 is connected, opens the piston 10 on communicating pipe 9；Treat that second connects liquid bottle
5 is full, the 3rd connect liquid bottle 11 had close to the liquid of half when, according to the situation of the liquid in reaction bulb, decide whether to connect
Logical 4th connects liquid bottle 16.
Embodiment 2
Referring to Fig. 1～4, this utility model provides a kind of Novel connecting liquid device, including connect liquid tail pipe 17, first connect liquid bottle 3,
Second connects liquid bottle the 5, the 3rd connects liquid bottle 11 and the 4th and connects liquid bottle 16, and described second connects liquid bottle 5 connects liquid bottle 11 with the 3rd and pass through to connect
Pipe 9 connects, and the 4th connects liquid bottle 16 connects liquid bottle 11 by connecting communicating pipe 9 with the 3rd.It is described that to connect liquid tail pipe 17 directly anti-with distillation
The condensing tube answering device connects.The described liquid tail pipe 17 that connects has a gas outlet 18 and a separatory stopcock 19.Described separatory stopcock
There are piston 7, first passage 1 and second channel 6 on 19, control reaction drop to pass through first passage 1 or the second by rotating piston 7
Passage 6；It is provided with two ports 13 in left and right and intermediate piston 10 described communicating pipe 9.The described 3rd bottle both sides connecing liquid bottle 11
There are the second opening 14 and the 3rd opening 15, the position of two of which opening is parallel.Described second connects liquid bottle 5 and the 4th connects liquid bottle 16
Bottle side have the first opening 12.
Described first liquid delivery line 2 is connect liquid bottle 3 with first and is connected by ground, and described second connects liquid bottle 5 and the second liquid
Body delivery line 4 is connected by ground, and the described 3rd connects liquid bottle 11 and the 4th connects liquid bottle 16 bottleneck bottle stopper 8.
When distillation starts, piston 7 is rotated to connecting first liquid delivery line 2, receives lower boiling liquid；Treat temperature liter
When height is to product boiling point, rotary-piston 7, second liquid delivery line 4 is connected, opens the piston 10 on communicating pipe 9；Treat that second connects
Liquid bottle 5 is full, the 3rd connect liquid bottle 11 had close to the liquid of half when, according to the situation of the liquid in reaction bulb, decision is
No connection the 4th connects liquid bottle 16.In still-process, liquid in reaction bulb occurs more than the 4th situation connecing liquid bottle 16,
Before four connect liquid bottle 16 connection, connect liquid bottle (concrete bottle kind is as shown in Figure 3) in the 4th middle insertion the 5th connecing liquid bottle 16, to control
The safety of reaction is carried out.
The foregoing is only preferred embodiment of the present utility model, be not limited to this utility model, for this
For the technical staff in field, this utility model can have various modifications and variations.All of the present utility model spirit and principle
Within, any modification, equivalent substitution and improvement made etc., should be included within protection domain of the present utility model.
Claims (4)
1. a kind of Novel connecting liquid device is it is characterised in that described Novel connecting liquid device includes connecing liquid tail pipe (17), first connects liquid
Bottle (3), second connect liquid bottle (5), the 3rd connect liquid bottle (11) and the 4th and connect liquid bottle (16), described second connects liquid bottle (5) connects with the 3rd
Liquid bottle (11) passes through to connect communicating pipe (9), and the 4th connects liquid bottle (16) connects liquid bottle (11) by connecting communicating pipe (9) with the 3rd；Institute
State and connect liquid tail pipe (17) and directly connect with the condensing tube of distillation reaction device；The described liquid tail pipe (17) that connects has a gas outlet (18)
With a separatory stopcock (19)；Piston (7), first passage (1) and second channel (6) are had on described separatory stopcock (19)；Described
One end of first passage (1) is communicated with first liquid delivery line (2), and the other end is communicated with distillation reaction device；Described second leads to
Road (6) one end is communicated with second liquid delivery line (4), and the other end is communicated with distillation reaction device；Described first liquid delivery line
(2) connect liquid bottle (3) with first to connect by ground, described second connects liquid bottle (5) passes through ground phase with second liquid delivery line (4)
Connect, the described 3rd connects liquid bottle (11) and the 4th connects liquid bottle (16) bottleneck bottle stopper (8).
2. a kind of Novel connecting liquid device according to claim 1 is it is characterised in that be provided with left and right described communicating pipe (9)
Two ports (13) and intermediate piston (10).
3. a kind of Novel connecting liquid device according to claim 1 is it is characterised in that the described 3rd connects the bottle of liquid bottle (11)
There are the second opening (14) and the 3rd opening (15) in both sides.
4. a kind of Novel connecting liquid device according to claim 1 is it is characterised in that described second meets liquid bottle (5) and the 4th
There is the first opening (12) the bottle side connecing liquid bottle (16).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620627107.3U CN205886913U (en) | 2016-06-23 | 2016-06-23 | Novel connect liquid device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620627107.3U CN205886913U (en) | 2016-06-23 | 2016-06-23 | Novel connect liquid device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205886913U true CN205886913U (en) | 2017-01-18 |
Family
ID=57768823
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620627107.3U Expired - Fee Related CN205886913U (en) | 2016-06-23 | 2016-06-23 | Novel connect liquid device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205886913U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109248464A (en) * | 2018-11-08 | 2019-01-22 | 乐山师范学院 | A kind of full-automatic still head |
-
2016
- 2016-06-23 CN CN201620627107.3U patent/CN205886913U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109248464A (en) * | 2018-11-08 | 2019-01-22 | 乐山师范学院 | A kind of full-automatic still head |
| CN109248464B (en) * | 2018-11-08 | 2023-12-12 | 乐山师范学院 | Full-automatic distillation head |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN205886913U (en) | Novel connect liquid device | |
| CN202315368U (en) | Small negative pressure stripping device | |
| CN201392289Y (en) | Water sample extractive distillation apparatus | |
| CN201417095Y (en) | Double three-way glass condenser | |
| CN207081726U (en) | A kind of Soil Thermal repairs feasibility analogue experiment installation | |
| CN207131389U (en) | Separate type Samper for oil well | |
| CN206161390U (en) | Vacuum transfer device is collected to atmosphere steam | |
| CN205287661U (en) | Trace liquid distillation plant | |
| CN203408724U (en) | Novel distillation device | |
| CN202220163U (en) | Essential oil extraction device | |
| CN203303810U (en) | Device for extracting purified methane and carbon dioxide from marsh gas impurities | |
| CN206566531U (en) | A kind of integrated hydrosol essential oil separator | |
| CN201819579U (en) | Second-generation double-tee glass condenser | |
| CN103331029B (en) | Distiller | |
| CN206252986U (en) | A kind of coal bed gas purifies Vacuum Pressure Swing power transformation Coupling Adsorption experimental provision | |
| CN203459091U (en) | Continuously operated intermittent sampling type decompress evaporation device | |
| CN208003477U (en) | Distilling and extracting device while volatile oil | |
| CN206934800U (en) | A kind of refluxing extraction device | |
| CN202136993U (en) | Self-stirring distillation reactor | |
| CN206168395U (en) | Desorption bottle organic reagent recovery unit | |
| CN208018188U (en) | A kind of efficient distillation condensing unit | |
| CN105289034B (en) | Gas-liquid chromatograph (GLC) separator | |
| CN205391810U (en) | Medical oil -water separator | |
| CN204656062U (en) | A kind of thin layer chromatography column packing apparatus for removing | |
| CN202329269U (en) | Third generation double-tee glass condenser |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170118 Termination date: 20170623 |