CN205886253U - Portable type rotary evaporato - Google Patents

Portable type rotary evaporato Download PDF

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Publication number
CN205886253U
CN205886253U CN201620895461.4U CN201620895461U CN205886253U CN 205886253 U CN205886253 U CN 205886253U CN 201620895461 U CN201620895461 U CN 201620895461U CN 205886253 U CN205886253 U CN 205886253U
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CN
China
Prior art keywords
condensing tube
support
receiving flask
revolving bottle
water
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Active
Application number
CN201620895461.4U
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Chinese (zh)
Inventor
徐庆
苏献兰
刘薇薇
唐志文
胡浩东
黄磊
周晋生
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HAOLISEN COATING (SHANGHAI) Co Ltd
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HAOLISEN COATING (SHANGHAI) Co Ltd
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Priority to CN201620895461.4U priority Critical patent/CN205886253U/en
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model relates to a chemical experimental instruments technical field is a portable type rotary evaporato particularly, including the revolving bottle, the thermostat water bath, the condenser pipe, the low -temperature cooling water circulating pump, circulation ability of swimming vacuum pump, the receiving flask, support and base, the pulley is equipped with respectively to base four corners lower part, pulley one side is equipped with the fixing device button, the removal of fixing device pushbutton control pulley, a support is arranged on the base, support middle part centre gripping has rotary device, a rotary device side joint has the revolving bottle, rotary device drives the revolving bottle that is located the thermostat water bath and rotates, the rotary device opposite side is equipped with the gas -tight valve, a support side joint has the condenser pipe, the condenser pipe below has connect the receiving flask, condenser pipe upper portion is equipped with the joint of bleeding, bleed and connect through pipe connection to circulating ability of swimming vacuum pump messenger condenser pipe at vacuum environment. The utility model discloses convenient operation is removed, can effectual improvements cooling efficiency, and improvement evaporation efficiency, the receiving flask bottom is equipped with drainage valve.

Description

A kind of movable-type Rotary Evaporators
[technical field]
This utility model is related to chemical experimental instrument technical field, specifically a kind of movable-type Rotary Evaporators.
[background technology]
Rotary Evaporators are commonly used to medicine, food, the concentration of biological industry, and Rotary Evaporators are mainly used in decompression bar Continuous still a large amount of effumability solvent under part.The distillation of the reception liquid when concentration especially to extract and chromatographic isolation, can To separate and purification reaction product, its distillation principle mainly drives distilling flask to rotate continuous by rotator, formation rotation Thin film increases disengagement area, accelerates evaporation rate, and negative pressure reduces the boiling point of solvent simultaneously, reduces heating-up temperature, to concentration The heat-sensitive ingredients of liquid have good protective effect.
There is certain defect in traditional Rotary Evaporators, because Rotary Evaporators are to be combined by multiple equipment and parts Form, not only operate inconvenience, and form complex structure, need the single instrument of line in the Eight Diagrams independently to carry during moving, cause to carry Journey is relatively complicated, the phenomenon such as is also easy to cause instrument fragile during carrying.
[utility model content]
This utility model is that the operation that leads to for above-mentioned traditional Rotary Evaporators structure, the technology of mobile inconvenience are asked A kind of topic, there is provided the novel movable-type Rotary Evaporators of structure.
To achieve these goals, a kind of movable-type Rotary Evaporators are designed, including revolving bottle, thermostat water bath, cold Solidifying pipe, sub-cooled water-circulating pump, circulating water type vacuum pump, receiving flask, support and base, described base corner bottom is respectively Equipped with pulley, pulley side is provided with fixing device button, the movement of described fixing device button control pulley, described base It is provided with support, mid-stent is clamped with rotary apparatuss, rotary apparatuss side is connected to revolving bottle, described rotary apparatuss drive position Revolving bottle in thermostat water bath rotates, and rotary apparatuss opposite side is provided with gas-tight valve, and support side is connected to condensing tube, described Condensing tube below be connected to receiving flask, condensing tube top is provided with air extraction connector, and air extraction connector is connected to circulating water type by conduit Vacuum pump makes condensing tube be in vacuum environment.
Described revolving bottle, thermostat water bath, condensing tube, sub-cooled water-circulating pump, circulating water type vacuum pump, collection Bottle, are placed on base top.
Condensing tube bottom is respectively equipped with condensing tube inlet union and condensing tube outlet connection, described condensing tube inlet union It is connected with the cooling water inlet joint on sub-cooled water-circulating pump, described condensing tube outlet connection connects low-temperature cooling water and follows Coolant outlet joint on ring pump.
Control panel is connected on described support, control panel is according to the temperature in material characteristic regulating thermostatic water-bath simultaneously Keep constant temperature.
Connected by connection valve between described revolving bottle and rotary apparatuss.
Described receiving flask bottom is provided with bleeder valve.
This utility model compared with the existing technology, has an advantage in that: by revolving bottle, thermostat water bath, condensing tube, low temperature cold But the part such as water-circulating pump, circulating water type vacuum pump, receiving flask, support is all placed on the base of installing pulley, being capable of basis Use demand moves to diverse location at any time and uses and be fixed, and convenient operation is moved, and also preferably prevents rotation simultaneously Evaporimeter such as damages at the phenomenon when moving;Sub-cooled water-circulating pump is directly connected with condensing tube, can effectively improve cooling Efficiency, accelerates to prevent volatile matter to be inhaled in vacuum pump while evaporation rate, improves evaporation efficiency;Receiving flask bottom is provided with puts Liquid valve, can directly release liquid in bottle without taking off receiving flask, easy to operate, it is to avoid because collection is broken in experimenter's carelessness into pieces Bottle.
[brief description]
Fig. 1 is structural representation of the present utility model;
In figure: 1. air extraction connector 2. condensing tube 3. condensing tube inlet union 4. condensing tube outlet connection 5. venting valve 6. gas vent 7. receiving flask 8. sub-cooled water-circulating pump 9. control panel 10. support, 11. rotary apparatuss 12. connection valve 13. revolving bottle, 14. thermostat water bath, 15. base, 16. circulating water type vacuum pump 17. vacuum pressure exports 18. cooling waters and enters Mouth joint 19. coolant outlet joint, 20. fixing device button 21. pulley.
[specific embodiment]
The utility model is described in further detail below in conjunction with the accompanying drawings, the structure of this device and the principle people professional to this For be very clearly.It should be appreciated that specific embodiment described herein is only in order to explain this utility model, and without In restriction this utility model.
Embodiment 1
As shown in figure 1, this device include revolving bottle 13, thermostat water bath 14, condensing tube 2, sub-cooled water-circulating pump 8, Circulating water type vacuum pump 16, receiving flask 7, support 10 and base 15,15 4 jiaos of bottoms of base are respectively provided with pulley 21, pulley 21 1 Side is provided with fixing device button 20, and fixing device button 20 controls the movement of pulley 21.Base 15 is provided with support 10, support 10 Middle part is clamped with rotary apparatuss 11, and rotary apparatuss 11 side is connected to revolving bottle 13, passes through between revolving bottle 13 and rotary apparatuss 11 Connection valve 12 connects, and rotary apparatuss 11 drive the revolving bottle 13 being located in thermostat water bath 14 to rotate, rotary apparatuss 11 opposite side It is provided with gas-tight valve 5, support 10 side is connected to condensing tube 2, below condensing tube 2, is connected to receiving flask 7, condensing tube 2 top is provided with takes out Gas joint 1, air extraction connector 1 is connected by conduit makes condensing tube 2 be in vacuum environment to circulating water type vacuum pump 16;Condensing tube 2 Bottom is respectively equipped with condensing tube inlet union 3 and condensing tube outlet connection 4, condensing tube inlet union 3 and sub-cooled water circulation Cooling water inlet joint 18 on pump 8 is connected, and the cooling water that condensing tube outlet connection 4 connects on sub-cooled water-circulating pump 8 goes out Mouth joint 19.Due to revolving bottle 13, thermostat water bath 14, condensing tube 2, sub-cooled water-circulating pump 8, circulating water type vacuum pump 16th, receiving flask 7, support 10 are all placed in base 15 top, fill four removable movable pulleys respectively at mobile base bottom four angle And fixing device for installing, fixing device button and then fixation can be pressed after base being moved to the position wanting movement, prevent bottom Seat slides, and such Rotary Evaporators are more easy and convenient when moving also preferably to prevent Rotary Evaporators when moving simultaneously The phenomenons such as damage.
Control panel 9 is connected on support 10, control panel 9 is according to the temperature in material characteristic regulating thermostatic water-bath 14 simultaneously Thermostat water bath 14 is made to keep constant temperature.
Sub-cooled water-circulating pump 8 is connected with condensing tube 2, can effectively improve cooling effectiveness, accelerates evaporation rate same When prevent volatile matter to be inhaled in vacuum pump.
Receiving flask 7 bottom is provided with bleeder valve 5, can directly release liquid in bottle without taking off receiving flask, easy to operate, keeps away Exempt to break receiving flask into pieces due to experimenter's carelessness.

Claims (6)

1. a kind of movable-type Rotary Evaporators, including revolving bottle, thermostat water bath, condensing tube, sub-cooled water-circulating pump, follow Ring ability of swimming vacuum pump, receiving flask, support and base are it is characterised in that described base corner bottom is respectively provided with pulley, pulley Side is provided with fixing device button, the movement of described fixing device button control pulley, and described base is provided with support, It is clamped with rotary apparatuss, rotary apparatuss side is connected to revolving bottle, described rotary apparatuss drive and are located at thermostat water bath in the middle part of frame Interior revolving bottle rotates, and rotary apparatuss opposite side is provided with gas-tight valve, and support side is connected to condensing tube, below described condensing tube It is connected to receiving flask, condensing tube top is provided with air extraction connector, and air extraction connector is connected by conduit makes condensation to circulating water type vacuum pump Pipe is in vacuum environment.
2. as claimed in claim 1 a kind of movable-type Rotary Evaporators it is characterised in that described revolving bottle, water bath with thermostatic control Pot, condensing tube, sub-cooled water-circulating pump, circulating water type vacuum pump, receiving flask, it is placed on base top.
3. as claimed in claim 1 a kind of movable-type Rotary Evaporators it is characterised in that condensing tube bottom be respectively equipped with cold Solidifying pipe inlet union and condensing tube outlet connection, the cooling water in described condensing tube inlet union and sub-cooled water-circulating pump Inlet union is connected, and described condensing tube outlet connection connects the coolant outlet joint on sub-cooled water-circulating pump.
4. as claimed in claim 1 a kind of movable-type Rotary Evaporators it is characterised in that being connected to control on described support Panel, control panel according to the temperature in material characteristic regulating thermostatic water-bath and keeps constant temperature.
5. as claimed in claim 1 a kind of movable-type Rotary Evaporators it is characterised in that described revolving bottle and rotating dress Connected by connection valve between putting.
6. as claimed in claim 1 a kind of movable-type Rotary Evaporators it is characterised in that described receiving flask bottom is provided with Bleeder valve.
CN201620895461.4U 2016-08-17 2016-08-17 Portable type rotary evaporato Active CN205886253U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620895461.4U CN205886253U (en) 2016-08-17 2016-08-17 Portable type rotary evaporato

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620895461.4U CN205886253U (en) 2016-08-17 2016-08-17 Portable type rotary evaporato

Publications (1)

Publication Number Publication Date
CN205886253U true CN205886253U (en) 2017-01-18

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620895461.4U Active CN205886253U (en) 2016-08-17 2016-08-17 Portable type rotary evaporato

Country Status (1)

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CN (1) CN205886253U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115177966A (en) * 2021-04-07 2022-10-14 济宁明德环保科技有限公司 Easy-to-operate rotary evaporator for chemical laboratory

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115177966A (en) * 2021-04-07 2022-10-14 济宁明德环保科技有限公司 Easy-to-operate rotary evaporator for chemical laboratory

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