CN205873939U - Device that contains heavy metal ion waste water is handled to microwave fluidized bed - Google Patents

Device that contains heavy metal ion waste water is handled to microwave fluidized bed Download PDF

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CN205873939U
CN205873939U CN201620382235.6U CN201620382235U CN205873939U CN 205873939 U CN205873939 U CN 205873939U CN 201620382235 U CN201620382235 U CN 201620382235U CN 205873939 U CN205873939 U CN 205873939U
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fluidized bed
heat exchanger
raw material
distribution plate
hot air
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孙玉红
高向琪
高涵
王宁
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Jining University
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A20/00Water conservation; Efficient water supply; Efficient water use
    • Y02A20/124Water desalination
    • Y02A20/138Water desalination using renewable energy
    • Y02A20/141Wind power

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Abstract

本实用新型涉及一种微波流化床处理含重金属离子废水的装置,属于废水处理技术领域,包括原料罐和流化床,原料罐出口处连接进料泵,进料泵通过管道连接流化床,流化床顶部设置有蒸汽出口,原料罐上方设置有通过管道与进料泵连接的原料分布盘,原料分布盘下方的流化床的壳体上设置有热电偶和微波源,液体分布板下方设置有热风分布盘,热风分布盘下方通过管道连接热风加热器,蒸汽出口通过管道连接换热器,换热器与热风加热器、冷凝器和风机连接,冷凝器另一端连接蒸馏水收集罐。本实用新型结构简单,利用微波流化床,加热速度快,并且在流化床底部通入热风,使得蒸发效果更好,无残留,且通过换热器做到了热能回收再利用,节约了能源。

The utility model relates to a device for treating waste water containing heavy metal ions by a microwave fluidized bed, which belongs to the technical field of waste water treatment and comprises a raw material tank and a fluidized bed. The outlet of the raw material tank is connected to a feed pump, and the feed pump is connected to the fluidized bed through a pipeline , there is a steam outlet on the top of the fluidized bed, a raw material distribution plate connected to the feed pump through pipelines is set above the raw material tank, a thermocouple and a microwave source are set on the shell of the fluidized bed below the raw material distribution plate, and the liquid distribution plate There is a hot air distribution plate below, the hot air distribution plate is connected to the hot air heater through the pipe, the steam outlet is connected to the heat exchanger through the pipe, the heat exchanger is connected to the hot air heater, the condenser and the fan, and the other end of the condenser is connected to the distilled water collection tank. The utility model has a simple structure, uses a microwave fluidized bed, and has a fast heating speed, and hot air is introduced at the bottom of the fluidized bed, so that the evaporation effect is better and there is no residue, and the heat energy is recycled and reused through the heat exchanger, saving energy .

Description

微波流化床处理含重金属离子废水的装置Microwave fluidized bed treatment device for wastewater containing heavy metal ions

技术领域technical field

本实用新型属于废水处理技术领域,具体涉及一种微波流化床处理含重金属离子废水的装置。The utility model belongs to the technical field of waste water treatment, in particular to a device for treating waste water containing heavy metal ions by a microwave fluidized bed.

背景技术Background technique

随着我国工业的迅猛发展,重金属废水产出量越来越大。这些废水主要来自矿山排水、废石场淋滤水、选矿场尾矿排水、有色金属冶炼厂排水、有色金属加工厂酸洗废水、电镀厂镀件洗涤水、钢铁厂酸洗排水及电解、农药、医药、油漆和染料等各种工业废水。如何高效处理这些重金属废水,并使之资源化,已成为人们共同关注的问题。蒸发是处理含重金属离子废水的有效途径之一。作为重要的化工单元操作之一,蒸发是用加热的方法,使溶液在沸腾状态下将其中的水分或具有挥发性的溶剂部分汽化后在冷凝器内实现冷凝、浓缩的技术。因此,蒸发过程是一个热量传递过程,传热效率和速率是蒸发过程的控制环节。对于冶金、化工领域来说,蒸发也是能量消耗量最大的操作单元之一。With the rapid development of my country's industry, the output of heavy metal wastewater is increasing. These wastewaters mainly come from mine drainage, waste rock leaching water, mine tailings drainage, non-ferrous metal smelting plant drainage, non-ferrous metal processing plant pickling wastewater, electroplating factory plating washing water, iron and steel plant pickling drainage and electrolysis, pesticides , pharmaceuticals, paints and dyes and other industrial wastewater. How to efficiently treat these heavy metal wastewater and make it a resource has become a common concern of people. Evaporation is one of the effective ways to treat wastewater containing heavy metal ions. As one of the important chemical unit operations, evaporation is a technology that uses heating to partially vaporize the water or volatile solvent in the solution in the boiling state, and then realize condensation and concentration in the condenser. Therefore, the evaporation process is a heat transfer process, and the heat transfer efficiency and rate are the control links of the evaporation process. For metallurgy and chemical industry, evaporation is also one of the operating units with the largest energy consumption.

目前,蒸发设备可分为单效、多效、二次蒸汽压缩式、多级闪发式、多效多级闪发式等。单效蒸发效率低,为了提高蒸发效率,蒸发设备逐渐向多效蒸发发展。多效蒸发系统较复杂,三效蒸发需要三台泵,三个蒸发罐,三套换热系统,而且这些设备都需要耐高温和耐压,生产制造成本较高。At present, evaporation equipment can be divided into single-effect, multi-effect, secondary vapor compression, multi-stage flash, multi-effect multi-stage flash, etc. The efficiency of single-effect evaporation is low. In order to improve the evaporation efficiency, evaporation equipment is gradually developing into multi-effect evaporation. The multi-effect evaporation system is more complicated. The three-effect evaporation requires three pumps, three evaporation tanks, and three sets of heat exchange systems. Moreover, these devices need to withstand high temperature and pressure, and the manufacturing cost is relatively high.

无论是多效蒸发、闪蒸还是两种方式的结合,都还存在一些核心难题需要解决。首先,蒸发所需要的热量主要来源于热交换,通常采用的热源为蒸汽换热方式;不论采用那种换热装置,都存在较大的热损失量。其次,换热器需要承受热蒸汽的高温高压冲击和物料的腐蚀,对设备的稳定运行造成严重影响。第三,溶液中的杂质组分易在换热器壁面上产生结垢,使换热效率急剧下降,能耗水平急剧上升。Whether it is multi-effect evaporation, flash evaporation or a combination of the two methods, there are still some core problems that need to be solved. First of all, the heat required for evaporation mainly comes from heat exchange, and the heat source usually used is steam heat exchange; no matter what kind of heat exchange device is used, there is a large amount of heat loss. Secondly, the heat exchanger needs to withstand the high temperature and high pressure impact of hot steam and the corrosion of materials, which seriously affects the stable operation of the equipment. Third, the impurity components in the solution are prone to fouling on the wall of the heat exchanger, causing a sharp drop in heat transfer efficiency and a sharp increase in energy consumption.

因此现在常用微波流化床来处理重金属废水,但是微波处理电磁场分布不均匀,导致局部温度较高,波动较大,因此影响了蒸发效果,且对于处理后的热量不能回收利用,造成能源浪费。Therefore, microwave fluidized bed is commonly used to treat heavy metal wastewater, but the electromagnetic field distribution of microwave treatment is uneven, resulting in high local temperature and large fluctuations, which affects the evaporation effect, and the heat after treatment cannot be recycled, resulting in energy waste.

实用新型内容Utility model content

本实用新型的目的在于提供一种微波流化床处理含重金属离子废水的装置,来解决上述问题。The purpose of the utility model is to provide a microwave fluidized bed treatment device for wastewater containing heavy metal ions to solve the above problems.

本实用新型微波流化床处理含重金属离子废水的装置,包括原料罐和流化床,原料罐出口处连接进料泵,进料泵通过管道连接流化床,原料罐内部下方设置有净化器,流化床顶部设置有蒸汽出口,原料罐上方设置有通过管道与进料泵连接的原料分布盘,原料分布盘下方均匀分布有原料喷嘴,原料分布盘上方设置有除沫器,原料分布盘下方的流化床的壳体上设置有热电偶和微波源,流化床内部下方设置有若干个液体分布板,液体分布板下方设置有热风分布盘,热风分布盘上方设置有热风分布喷嘴,热风分布盘下方通过管道连接热风加热器,蒸汽出口通过管道连接换热器,换热器与热风加热器、冷凝器和风机连接,冷凝器另一端连接蒸馏水收集罐。The utility model microwave fluidized bed treatment device for waste water containing heavy metal ions comprises a raw material tank and a fluidized bed, the outlet of the raw material tank is connected to a feed pump, the feed pump is connected to the fluidized bed through a pipeline, and a purifier is arranged inside the raw material tank , there is a steam outlet on the top of the fluidized bed, a raw material distribution plate connected to the feed pump through a pipeline is set above the raw material tank, raw material nozzles are evenly distributed under the raw material distribution plate, a demister is set above the raw material distribution plate, and the raw material distribution plate The shell of the fluidized bed below is provided with a thermocouple and a microwave source, a number of liquid distribution plates are provided under the fluidized bed, a hot air distribution plate is provided under the liquid distribution plate, and a hot air distribution nozzle is provided above the hot air distribution plate. The bottom of the hot air distribution plate is connected to the hot air heater through pipes, the steam outlet is connected to the heat exchanger through pipes, the heat exchanger is connected to the hot air heater, the condenser and the fan, and the other end of the condenser is connected to the distilled water collection tank.

所述流化床与微波源间设有保温层。An insulating layer is provided between the fluidized bed and the microwave source.

所述换热器包括盘管,盘管一端通过管道连接蒸汽出口、另一端伸出换热器内部与冷凝器连接,盘管的内部套接有换热管,换热管一端连接风机、另一端伸出换热器与热风加热器相连,可以充分进行热交换,减少能源浪费。The heat exchanger includes a coil, one end of the coil is connected to the steam outlet through a pipe, and the other end extends out of the heat exchanger to connect with the condenser. One end protrudes from the heat exchanger and is connected with the hot air heater, which can fully perform heat exchange and reduce energy waste.

本实用新型与现有技术相比,具有以下有益效果:Compared with the prior art, the utility model has the following beneficial effects:

结构简单,利用微波流化床,加热速度快,并且在流化床底部通入热风,使得蒸发效果更好,无残留,且通过换热器做到了热能回收再利用,节约了能源。The structure is simple, the microwave fluidized bed is used, the heating speed is fast, and the hot air is introduced at the bottom of the fluidized bed, so that the evaporation effect is better and there is no residue, and the heat energy is recovered and reused through the heat exchanger, which saves energy.

附图说明Description of drawings

图1为本实用新型结构示意图;Fig. 1 is the structural representation of the utility model;

图中:1、原料罐,2、净化器,3、进料泵,4、热风分布盘,5、热风分布喷嘴,6、液体分布板,7、热电偶,8、微波源,9、原料喷嘴,10、原料分布盘,11、流化床,12、除沫器,13、蒸汽出口,14、风机,15、换热器,16、换热管,17、盘管,18、冷凝器,19、蒸馏水收集罐,20、热风加热器。In the figure: 1. Raw material tank, 2. Purifier, 3. Feed pump, 4. Hot air distribution plate, 5. Hot air distribution nozzle, 6. Liquid distribution plate, 7. Thermocouple, 8. Microwave source, 9. Raw material Nozzle, 10. Raw material distribution plate, 11. Fluidized bed, 12. Demister, 13. Steam outlet, 14. Fan, 15. Heat exchanger, 16. Heat exchange tube, 17. Coil, 18. Condenser , 19, distilled water collection tank, 20, hot air heater.

具体实施方式detailed description

下面结合实施例对本实用新型作进一步的说明。Below in conjunction with embodiment the utility model is further described.

如图1所示的微波流化床处理含重金属离子废水的装置,包括原料罐1和流化床11,原料罐1出口处连接进料泵3,进料泵3通过管道连接流化床11,原料罐1内部下方设置有净化器2,流化床11顶部设置有蒸汽出口13,原料罐1上方设置有通过管道与进料泵3连接的原料分布盘10,原料分布盘10下方均匀分布有原料喷嘴9,原料分布盘10上方设置有除沫器12,原料分布盘10下方的流化床11的壳体上设置有热电偶7和微波源8,流化床11内部下方设置有若干个液体分布板6,液体分布板6下方设置有热风分布盘4,热风分布盘4上方设置有热风分布喷嘴5,热风分布盘4下方通过管道连接热风加热器20,蒸汽出口13通过管道连接换热器15,换热器15与热风加热器20、冷凝器18和风机14连接,冷凝器18另一端连接蒸馏水收集罐19。The device for treating waste water containing heavy metal ions by a microwave fluidized bed as shown in Figure 1 includes a raw material tank 1 and a fluidized bed 11, the outlet of the raw material tank 1 is connected to a feed pump 3, and the feed pump 3 is connected to the fluidized bed 11 through a pipeline A purifier 2 is arranged under the inside of the raw material tank 1, a steam outlet 13 is arranged on the top of the fluidized bed 11, a raw material distribution plate 10 connected to the feed pump 3 through a pipeline is arranged above the raw material tank 1, and the raw material distribution plate 10 is evenly distributed There are raw material nozzles 9, a demister 12 is arranged above the raw material distribution plate 10, a thermocouple 7 and a microwave source 8 are arranged on the housing of the fluidized bed 11 below the raw material distribution plate 10, and several A liquid distribution plate 6, a hot-air distribution plate 4 is arranged below the liquid distribution plate 6, a hot-air distribution nozzle 5 is arranged above the hot-air distribution plate 4, a hot-air heater 20 is connected to the bottom of the hot-air distribution plate 4, and a steam outlet 13 is connected to a heat exchanger through a pipeline. Heater 15, heat exchanger 15 are connected with hot air heater 20, condenser 18 and fan 14, and the other end of condenser 18 is connected with distilled water collection tank 19.

流化床11与微波源8间设有保温层。An insulating layer is provided between the fluidized bed 11 and the microwave source 8 .

换热器15包括盘管17,盘管17一端通过管道连接蒸汽出口13、另一端伸出换热器15内部与冷凝器18连接,盘管17的内部套接有换热管16,换热管16一端连接风机14、另一端伸出换热器15与热风加热器20相连,可以充分进行热交换,减少能源浪费。The heat exchanger 15 includes a coil tube 17, one end of the coil tube 17 is connected to the steam outlet 13 through a pipe, and the other end extends out of the heat exchanger 15 to connect with the condenser 18. The inside of the coil tube 17 is sleeved with a heat exchange tube 16 for heat exchange One end of the pipe 16 is connected to the blower fan 14, and the other end extends out of the heat exchanger 15 and is connected to the hot air heater 20, which can fully perform heat exchange and reduce energy waste.

综上所述,本实用新型结构简单,利用微波流化床,加热速度快,并且在流化床底部通入热风,使得蒸发效果更好,无残留,且通过换热器做到了热能回收再利用,节约了能源。In summary, the utility model has a simple structure, uses a microwave fluidized bed, and has a fast heating speed, and hot air is passed through the bottom of the fluidized bed, so that the evaporation effect is better and there is no residue, and the heat energy is recovered and reused through the heat exchanger. Utilization saves energy.

Claims (2)

1. a device for microwave fluidized bed processing heavy metal ion-containing waste water, including head tank (1) and fluid bed (11), raw material Tank (1) exit connects feed pump (3), and feed pump (3) connects fluid bed (11) by pipeline, and head tank (1) lower inside sets Being equipped with depurator (2), fluid bed (11) top is provided with steam (vapor) outlet (13), it is characterised in that head tank (1) is provided above The feed distribution dish (10) being connected with feed pump (3) by pipeline, feed distribution dish (10) lower section is evenly distributed with raw material nozzles (9), feed distribution dish (10) is provided above demister (12), on the housing of the fluid bed (11) of feed distribution dish (10) lower section Being provided with thermocouple (7) and microwave source (8), fluid bed (11) lower inside is provided with several liquid distributing boards (6), and liquid divides Fabric swatch (6) lower section is provided with hot blast distributing disc (4), and hot blast distributing disc (4) is provided above hot blast distribution nozzles (5), and hot blast divides Cloth dish (4) lower section connects storage heater (20) by pipeline, and steam (vapor) outlet (13) connects heat exchanger (15), heat exchange by pipeline Device (15) is connected with storage heater (20), condenser (18) and blower fan (14), and condenser (18) other end connects distilled water and receives Collection tank (19), described heat exchanger (15) includes coil pipe (17), coil pipe (17) one end by pipeline connect steam (vapor) outlet (13), another End stretches out heat exchanger (15) inside and is connected with condenser (18), and the internal sleeve of coil pipe (17) is connected to heat exchanger tube (16), heat exchanger tube (16) one end connecting fan (14), the other end stretch out heat exchanger (15) and are connected with storage heater (20).
The device of microwave fluidized bed processing heavy metal ion-containing waste water the most according to claim 1, it is characterised in that described It is provided with heat-insulation layer between fluid bed (11) and microwave source (8).
CN201620382235.6U 2016-04-29 2016-04-29 Device that contains heavy metal ion waste water is handled to microwave fluidized bed Expired - Fee Related CN205873939U (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111592169A (en) * 2020-07-08 2020-08-28 上海环境卫生工程设计院有限公司 Horizontal cross heat exchange's hot air drying waste liquid system that circulates
CN111905403A (en) * 2020-08-06 2020-11-10 周丽华 Raw materials boiling device is used in cosmetics production
CN115031494A (en) * 2022-06-21 2022-09-09 哈尔滨工业大学 Microwave drying device for fluidized bed
WO2023063669A1 (en) * 2021-10-14 2023-04-20 (주)맨지온 Seawater desalination equipment

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111592169A (en) * 2020-07-08 2020-08-28 上海环境卫生工程设计院有限公司 Horizontal cross heat exchange's hot air drying waste liquid system that circulates
CN111592169B (en) * 2020-07-08 2024-08-02 上海环境卫生工程设计院有限公司 Circulating hot air drying waste liquid system with transverse cross heat exchange
CN111905403A (en) * 2020-08-06 2020-11-10 周丽华 Raw materials boiling device is used in cosmetics production
CN111905403B (en) * 2020-08-06 2023-01-17 中国检验检疫科学研究院粤港澳大湾区研究院 A raw material cooking device for cosmetic production
WO2023063669A1 (en) * 2021-10-14 2023-04-20 (주)맨지온 Seawater desalination equipment
CN115031494A (en) * 2022-06-21 2022-09-09 哈尔滨工业大学 Microwave drying device for fluidized bed

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