CN205731185U - A kind of chlorination reactor - Google Patents

A kind of chlorination reactor Download PDF

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Publication number
CN205731185U
CN205731185U CN201620095355.8U CN201620095355U CN205731185U CN 205731185 U CN205731185 U CN 205731185U CN 201620095355 U CN201620095355 U CN 201620095355U CN 205731185 U CN205731185 U CN 205731185U
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CN
China
Prior art keywords
secondary response
response device
order reaction
placing
chlorine
Prior art date
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Expired - Fee Related
Application number
CN201620095355.8U
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Chinese (zh)
Inventor
沈建钢
叶敏
叶方国
郑金锋
冯顶文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Shengfu Chemical Co Ltd
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Jiangxi Shengfu Chemical Co Ltd
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Priority to CN201620095355.8U priority Critical patent/CN205731185U/en
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Publication of CN205731185U publication Critical patent/CN205731185U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a kind of chlorination reactor, including first order reaction device, secondary response device, connecting tube, cooling layer and heating and heat-insulating device, the chlorine input channel being distributed in the shape of a spiral it is provided with in secondary response device, chlorine input channel is provided with venthole, the mode that the bottom of secondary response device and the bottom of first order reaction device are all threaded connection connects catalyst apparatus for placing, and is provided with placing trough on catalyst apparatus for placing;It is provided with exhaust gas processing device at the gas outlet of secondary response device, and the other end of exhaust gas processing device is connected with first order reaction device.The beneficial effects of the utility model: add chlorine and the contact area of reactant in the unit interval, thus add the speed of reaction, decrease the response time, improve work efficiency, facilitate later stage more catalyst changeout, this utility model also has reaction heat and easily discharges simultaneously, easy temperature control system, the advantage that chlorine utilization is high, reaction impurities is few.

Description

A kind of chlorination reactor
Technical field
This utility model relates to technical field of chemical production equipment, it particularly relates to a kind of chlorination reactor.
Background technology
Chlorination reaction refers generally to the reaction introducing in compound by chlorine element, and its reaction has been typically necessary catalytic condition, as heated, illumination or add catalyst etc..Wherein, chlorination reactor is a device for chlorination reaction, and it is a place being easy to chlorination reaction.
The patent disclosure of Application No. 201320655272.6 has gone out a kind of Low Temperature Thermal chlorination reactor, include first order reaction device, secondary response device, connecting tube and circulating device, the first order reaction bucket of first order reaction device is externally provided with heating and heat-insulating device, secondary response device bottom is provided with chlorine feed mouth, the secondary response bucket of secondary response device is externally provided with cooling layer, in the exit of secondary response device equipped with vent gas treatment liberation port, secondary response device is connected with circulating device by circulating line, circulating device is connected with the charging aperture of first order reaction device, the discharging opening of first order reaction device is connected with the charging aperture of secondary response device by connecting tube.After this Low Temperature Thermal chlorination reactor chlorine in use enters into secondary response device, chlorine is short for time of contact with the reactant in secondary response device, and contact area is little, causes response speed slow, when this external interpolation or more catalyst changeout the most inconvenient, tail gas recycling time weak effect.
For the problem in correlation technique, effective solution is the most not yet proposed.
Utility model content
The purpose of this utility model is to provide a kind of chlorination reactor, to overcome currently available technology above shortcomings.
For realizing above-mentioned technical purpose, the technical solution of the utility model is achieved in that
A kind of chlorination reactor, including first order reaction device and secondary response device, it is connected by connecting tube between first order reaction device and secondary response device, cooling layer and heating and heat-insulating device it is respectively equipped with outside described secondary response device and outside first order reaction device, it is provided with chlorine input channel in described secondary response device, described chlorine input channel is distributed in the shape of a spiral at secondary response device inner close fitting secondary response device inwall, described chlorine input channel is distributed in the shape of a spiral on one section and is provided with the venthole towards secondary response device center position, the mode that the bottom of described secondary response device and the bottom of described first order reaction device are all threaded connection connects catalyst apparatus for placing, and it is provided with placing trough on described catalyst apparatus for placing;It is provided with exhaust gas processing device at the gas outlet of described secondary response device, and the other end of this exhaust gas processing device is connected with first order reaction device.
Further, described secondary response device and first order reaction device are equipped with on discharging opening, and discharging opening it are equipped with control valve.
Further, described exhaust gas processing device includes the air shooter being connected with the gas outlet of secondary response device, and the described air shooter other end connects has condenser, the liquid outlet of described condenser to be connected with first order reaction device by liquid return tube.
Further, in described first order reaction device and secondary response device, it is equipped with temperature sensor, and temperature sensor connection has display device.
The beneficial effects of the utility model: use the helical form chlorine input channel of band venthole, substantially increase chlorine and the contact area of reactant in the unit interval, thus add the speed of reaction, decrease the response time, it is effectively increased work efficiency, after placing catalyst in placing trough on catalyst apparatus for placing, the mode being threaded connection is fixed on first order reaction device or secondary response device, facilitate later stage more catalyst changeout, this utility model also has reaction heat and easily discharges simultaneously, easy temperature control system, chlorine utilization is high, the advantage that reaction impurities is few.
Accompanying drawing explanation
In order to be illustrated more clearly that this utility model embodiment or technical scheme of the prior art, the accompanying drawing used required in embodiment will be briefly described below, apparently, accompanying drawing in describing below is only embodiments more of the present utility model, for those of ordinary skill in the art, on the premise of not paying creative work, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
Fig. 1 is the structural representation according to the chlorination reactor described in this utility model embodiment.
In figure:
1, first order reaction device;2, secondary response device;3, connecting tube;4, cooling layer;5, heating and heat-insulating device;6, chlorine input channel;7, catalyst apparatus for placing;8, placing trough;9, exhaust gas processing device;10, air shooter;11, condenser;12, temperature sensor;13, liquid return tube.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is clearly and completely described, it is clear that described embodiment is only a part of embodiment of this utility model rather than whole embodiments.Based on the embodiment in this utility model, all other embodiments that those of ordinary skill in the art are obtained, broadly fall into the scope of this utility model protection.
nullAs shown in Figure 1,According to a kind of chlorination reactor described in embodiment of the present utility model,Including first order reaction device 1 and secondary response device 2,It is connected by connecting tube 3 between first order reaction device 1 and secondary response device 2,It is respectively equipped with cooling layer 4 and heating and heat-insulating device 5 outside described secondary response device 2 and outside first order reaction device 1,It is provided with chlorine input channel 6 in described secondary response device 2,Described chlorine input channel 6 is distributed in the shape of a spiral at secondary response device 2 inner close fitting secondary response device 2 inwall,Described chlorine input channel 6 is provided with the venthole towards secondary response device 2 center position on being distributed one section in the shape of a spiral,The mode that the bottom of described secondary response device 2 and the bottom of described first order reaction device 1 are all threaded connection connects catalyst apparatus for placing 7,And it is provided with placing trough 8 on described catalyst apparatus for placing 7;It is provided with exhaust gas processing device 9 at the gas outlet of described secondary response device 2, and the other end of this exhaust gas processing device 9 is connected with first order reaction device 1.
It is equipped with on discharging opening, and discharging opening on described secondary response device 2 and first order reaction device 1 and is equipped with control valve.
Described exhaust gas processing device 9 includes the air shooter 10 being connected with the gas outlet of secondary response device 2, described air shooter 10 other end connects condenser 11, the liquid outlet of described condenser 11 is connected with first order reaction device 1 by liquid return tube 13, tail gas is condensed, unreacted chlorine is allowed to flow back to after being condensed into liquid in first order reaction device 1, improve chlorine utilization, change traditional by circulating pump when tail gas recycle the defect of recovering effect difference.
It is equipped with temperature sensor 12 in described first order reaction device 1 and secondary response device 2, and temperature sensor 12 connection has display device, the convenient temperature value understood in described first order reaction device 1 and secondary response device 2, consequently facilitating carry out suitable regulation, it is ensured that efficiently carrying out of reaction.
Understand technique scheme of the present utility model for convenience, below by way of in specifically used mode, technique scheme of the present utility model is described in detail.
When specifically used, spiral helicine described chlorine input channel 6 is when carrying chlorine, chlorine and the contact area of reactant in the unit interval can be increased, thus add the speed of reaction, decrease the response time, it is effectively increased work efficiency, the mode that the bottom of this external described first order reaction device 1 and described secondary response device 2 is all threaded connection is fixed with described catalyst apparatus for placing 7, catalyst is placed in described placing trough 8, reaction is catalyzed, and the later stage is when more catalyst changeout, have only to back-out after described catalyst apparatus for placing 7 and be replaced, very convenient.
In sum, by means of technique scheme of the present utility model, use the helical form chlorine input channel 6 of band venthole, substantially increase chlorine and the contact area of reactant in the unit interval, thus add the speed of reaction, decrease the response time, it is effectively increased work efficiency, after placing catalyst in placing trough 8 on catalyst apparatus for placing 7, the mode being threaded connection is fixed on first order reaction device 1 or secondary response device 2, facilitate later stage more catalyst changeout, this utility model also has reaction heat and easily discharges simultaneously, easy temperature control system, chlorine utilization is high, the advantage that reaction impurities is few.
The foregoing is only preferred embodiment of the present utility model; not in order to limit this utility model; all within spirit of the present utility model and principle, any modification, equivalent substitution and improvement etc. made, within should be included in protection domain of the present utility model.

Claims (4)

  1. null1. a chlorination reactor,Including first order reaction device (1) and secondary response device (2),It is connected by connecting tube (3) between first order reaction device (1) and secondary response device (2),Described secondary response device (2) is respectively equipped with cooling layer (4) and heating and heat-insulating device (5) with outside first order reaction device (1) outward,It is characterized in that,It is provided with chlorine input channel (6) in described secondary response device (2),Described chlorine input channel (6) is distributed in the shape of a spiral at secondary response device (2) inner close fitting secondary response device (2) inwall,Described chlorine input channel (6) is provided with the venthole towards secondary response device (2) center position on being distributed one section in the shape of a spiral,The mode that the bottom of described secondary response device (2) and the bottom of described first order reaction device (1) are all threaded connection connects catalyst apparatus for placing (7),And it is provided with placing trough (8) on described catalyst apparatus for placing (7);It is provided with exhaust gas processing device (9) at the gas outlet of described secondary response device (2), and the other end of this exhaust gas processing device (9) is connected with first order reaction device (1).
  2. Chlorination reactor the most according to claim 1, it is characterised in that be equipped with on discharging opening, and discharging opening on described secondary response device (2) and first order reaction device (1) and be equipped with control valve.
  3. Chlorination reactor the most according to claim 1, it is characterized in that, described exhaust gas processing device (9) includes the air shooter (10) being connected with the gas outlet of secondary response device (2), described air shooter (10) other end connects condenser (11), and the liquid outlet of described condenser (11) is connected with first order reaction device (1) by liquid return tube (13).
  4. Chlorination reactor the most according to claim 1, it is characterised in that be equipped with temperature sensor (12) in described first order reaction device (1) and secondary response device (2), and temperature sensor (12) connection has display device.
CN201620095355.8U 2016-01-30 2016-01-30 A kind of chlorination reactor Expired - Fee Related CN205731185U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620095355.8U CN205731185U (en) 2016-01-30 2016-01-30 A kind of chlorination reactor

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Application Number Priority Date Filing Date Title
CN201620095355.8U CN205731185U (en) 2016-01-30 2016-01-30 A kind of chlorination reactor

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CN205731185U true CN205731185U (en) 2016-11-30

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107253578A (en) * 2017-06-19 2017-10-17 派尔实验装备有限公司 A kind of experimental bench liquid waste treating apparatus

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107253578A (en) * 2017-06-19 2017-10-17 派尔实验装备有限公司 A kind of experimental bench liquid waste treating apparatus

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161130

Termination date: 20180130