CN205667836U - Integrated form polycarboxylic acids synthesis device - Google Patents

Abstract

The utility model discloses integrated form polycarboxylic acids synthesis device, including offering the container of feed inlet and outlet, and reactor, agitating device, additive dropping system, raw materials system, LOAD CELLS and electricity cabinet；Additive dropping system is connected with reactor top, for being added to reactor by additive in the way of dropping；Raw materials system is connected with reactor side, is used for adding raw materials into and mixes with additive to reactor；Agitating device is arranged on reactor, for being stirred by the material of mixing, makes raw material react to each other with additive；LOAD CELLS is arranged on bottom reactor, for weighing the material in reactor in real time；Reactor is connected with discharging opening by pipeline, for outwards being supplied by reacted material；Electricity cabinet is connected with agitating device, additive dropping system, raw materials system and LOAD CELLS simultaneously.This utility model is reasonable in design, simple operation, significantly facilitates on-the-spot processing, improves production efficiency.

Description

Integrated form polycarboxylic acids synthesis device

Technical field

This utility model relates to a kind of synthesis device, particularly relates to a kind of integrated form polycarboxylic acids synthesis device.

Background technology

At present, factory in carrying out polycarboxylic acids building-up process, be all required equipment is arranged on fixing place or In Factory Building (8 meters of high workshops of the most platform-type needs, ground pit type needs 6 meters of high workshops), it is relatively decentralized that each equipment installs ratio, operates pole Inconvenience, and be all the material carrying out synthetic reaction will to be needed to weigh the most in advance in synthetic reaction process, then By manually or mechanically load weighted material being joined in reactor, not only waste time and energy, and during adding materials Because of each material, to be produced different and additive the rate of addition of loss sometimes fast and sometimes slow, thus easily makes synthetic reaction insufficient, no Stable.Furthermore, present building site major part poor transport, buy finished product compound from fixing producer and not only increase the cost of transportation (only only having 40% content, remaining water of 60%, the packing material produced when also having round transport, loading-unloading vehicle is lost, covers not The finished product leakage that jail, pail pack crack are caused), and it is also easy to the supply of material phenomenon such as not in time occurs, for work when vile weather Cheng Jinzhan brings great inconvenience.Therefore, design one can carry out polycarboxylic acids synthesis, to site requirements not at building-site Height, and material added to reaction can be precisely weighed, the container-type polycarboxylic acids synthetic reaction equipment that precisely drips becomes as institute State technical field technical staff's urgent problem.

Utility model content

The technical problems to be solved in the utility model is: provide one can carry out synthetic reaction at building-site, to field The integrated form polycarboxylic acids synthesis that ground is less demanding, easily operated and material added to reaction can be precisely weighed, precisely drip sets Standby.

For achieving the above object, the technical solution adopted in the utility model is as follows:

Integrated form polycarboxylic acids synthesis device, including offering the container of feed inlet and outlet, and is arranged at this container Interior reactor, agitating device, additive dropping system, raw materials system, LOAD CELLS and electricity cabinet；Described additive drips Adding system is connected with reactor top, for being added to reactor by additive in the way of dropping；Described raw materials system System is connected with reactor side, is used for adding raw materials into and mixes with additive to reactor；Described agitating device is arranged on instead Answer on still, for being stirred by the material of mixing, make raw material react to each other with additive；Described LOAD CELLS is arranged on instead Answer bottom portion, for the material in reactor is weighed in real time；Described reactor is connected with discharging opening by pipeline, for by anti- Material after should is outwards supplied；Described electricity cabinet drips system, raw materials system and biography of weighing with agitating device, additive simultaneously Sensor connects, and is used for providing working power.

Further, it is additionally provided with workbox in described container.

As preferably, described agitating device is horizontal mixer.

Further, described additive dropping system is provided with two, and each additive dropping system all includes storing adding Add the holding vessel of agent, be connected with the top of reactor, for the dropping pump that additive is pumped in reactor, Yi Jiyu simultaneously The circulating line being arranged on holding vessel connects, for circulating pump additive homogenizing being recycled in holding vessel.

Specifically, described raw materials system includes the feed pot storing raw material, and simultaneously with reactor side Connect with feed pot, for the pipeline pump added raw materials into reactor.

Yet further, it is additionally provided with in described reactor and adds heat pipe for what the material of mixing was heated.

Further, described reactor side is provided with observation port.

Further, described container top further respectively has steam vent and manhole.

Further, it is provided with ventilation fan in described steam vent.

Further, described container is further opened with window.

Compared with prior art, this utility model has the advantages that

(1) this utility model is by each synthetic reaction equipment needed thereby secure placement in moveable container, and each equipment is pacified Fill reasonable, compact, be not only easy to operation, and container can move directly to produce building site, the most only need to connect water power Carry out synthetic reaction, complete the synthetic work of product, and outwards output products.Therefore, this utility model have easy to use, right The advantage that site requirements is the highest.

(2) this utility model uses pipeline pump and dropping pump to add synthetic reaction needed raw material and additive in reactor Mode, for using the artificial mode added compared to existing technology, more time saving and energy saving, the production effect at scene is greatly improved Rate.

(3) this utility model arranges LOAD CELLS below reactor, can monitor institute in reactor the most exactly Add the weight of material, thus ensure that the principle in reactor can strictly be added according to formula proportion with additive, enter And enable the synthetic reaction of each material fully, intactly carry out.

(4) this utility model is provided with agitating device on reactor top, can be to reactant when synthetic reaction is carried out Material is stirred, and makes the reaction of material more uniformly, completely.

(5) this utility model is also provided with adding heat pipe in reactor, by the way of using and not using and adding heat pipe, and can To meet the temperature environment requirement when synthetic reaction of the dissimilar polycarboxylic acids raw material.

Accompanying drawing explanation

Fig. 1 is inside elevation view of the present utility model.

Fig. 2 is inside top figure of the present utility model.

Fig. 3 is external plan view of the present utility model.

Fig. 4 is external front face figure of the present utility model.

Wherein, corresponding entitled of reference:

1-container, 2-reactor, 3-holding vessel, 4-drips pump, 5-LOAD CELLS, 6-pipeline pump, 7-feed pot, 8- Circulating pump, 9-electricity cabinet, 10-manhole, 11-steam vent, 12-ventilation fan, 13-window, 14-discharging opening, 15-power line storehouse, 16- Agitating device, 17-observation port, 18-adds heat pipe, 19-workbox, 20-lifting eye, 21-forklift hole, 22-dog-house, 23-diminishing Agent is imported and exported, and 24-protects agent of collapsing and imports and exports, the import of 25-water source, 26-acrylic acid import.

Detailed description of the invention

The utility model is described in further detail with embodiment in explanation below in conjunction with the accompanying drawings, and mode of the present utility model includes But it is not limited only to following example.

As shown in figures 1-4, this utility model is mainly used in the synthesis of polycarboxylic acids, and it includes open sided 1, and is all provided with Put the reactor 2 in this container, agitating device 16, additive dropping system, raw materials system, LOAD CELLS 5 and Electricity cabinet 9.

Described container 1 surrounding is equipped with lifting eye 20 and forklift hole 21, has been carried out by whole container 1 for convenient Hang or be transported on fork truck transport；Meanwhile, this container 1 further respectively has water reducer to import and export 23, protect agent turnover of collapsing Mouthfuls 24, water source import 25, acrylic acid import 26 etc. some facilitate material and water to add to the material mouth in reactor.

Described additive dropping system is for adding additive to reactor 2 in the way of dropping.In the present embodiment, Additive dropping system is provided with two, and each additive dropping system all includes the holding vessel 3 that stores additive, simultaneously with instead The top answering still 2 connects, for the dropping pump 4 that additive is pumped in reactor, and the circulation connecting tube of holding vessel 3 Road, for circulating pump 8 that additive homogenizing is recycled in holding vessel.

Described raw materials system is used for adding raw materials into and mixes with additive to reactor 2, and it includes storing former The feed pot 7 of material, and be connected with reactor 2 side and feed pot 7, for the pipeline that raw material is pumped in reactor simultaneously Pump 6.

Described agitating device 16 then for being stirred by the material of mixing, makes raw material react to each other with additive.This reality Executing in example, this agitating device 16 preferably employs horizontal mixer, and (and reductor in blender selects helical gear Hardened gear face spiral shell Rotation cone reductor).And described reactor 2 is connected with the discharging opening 14 being arranged on container 1 by pipeline, for reacting After material outwards supply.

Described LOAD CELLS 5 is arranged on bottom reactor 2, for weighing the material in reactor in real time.Described electricity Cabinet 9 is connected with the said equipment simultaneously, is used for providing working power.

It is additionally provided with workbox 19 in described container 1, is used for depositing various service kit, conveniently at any time each equipment is entered Row maintenance, meanwhile, it also can be provided with plug-type scoring table, conveniently various dosages and operational circumstances be carried out record.

It is additionally provided with in described reactor 2 and adds heat pipe 18, when use adds heat pipe, the temperature in reactor can be realized and raise, from And meet needs higher temperature environment and just can carry out the raw material of synthetic reaction.

It addition, described reactor 2 side is provided with observation port 17, facilitate the material reaction situation in observing response still.Simultaneously Described container 1 top is additionally provided with in further respectively having steam vent 11, manhole 10 and window 13, and steam vent 11 and changes Gas fan 12.

Below a brief description does with regard to utility model works flow process:

First, by pipeline pump 6, the raw material in feed pot 7 is added to reactor 2, then want according to formula proportion Ask, while adding raw material or afterwards by dripping pump 4 by the additive in holding vessel 3 to add to instead by the way of dripping In answering still 2.

Start agitating device 16 material is stirred simultaneously, to realize the synthetic reaction of material, make the reaction of material more Add the most completely；If synthetic reaction needs higher temperature environment, then when carrying out synthetic reaction by controlling in reactor 2 The heat pipe 18 that adds reaction mass is heated.After reaction terminates, by the discharging opening being connected with reactor 2, product is outside Output.Meanwhile, during above-mentioned charging, weighed in real time by LOAD CELLS 5, in order in strict accordance with formula proportion control Each material and the amount of additive.

The power line of this utility model all devices is all externally connected, in making container by electricity cabinet 9 and power line storehouse 15 The each circuit in portion is in good order.Additionally, be provided with unified dog-house 22 or concealed dog-house, all fortune at container front side The material sending reaction to be synthesized all can enter in container by dog-house, makes each pipeline of internal container in good order, as This is available space in can being greatly saved container.Reactor upper side is provided with several observation ports, can be with observing response The synthetic reaction situation of material in still, the wall thickness of reactor is arranged to 20 millimeters, it is ensured that the solid safety of reactor, adds in reactor The power of heat pipe is 45KW, it is ensured that synthetic reaction can be carried out at sufficiently high temperature, is provided with some at container top Manhole, can carry out safety inspection by each manhole to corresponding equipment, arranges and change in the steam vent on container top Gas is fanned, it is ensured that air flowing in container, and this external container is additionally provided with door and window, and in facilitating container, daylighting is with each Equipment carries out overhauling and the work such as cleaning.This utility model design is ingenious rationally, possesses higher using value, possesses substance Feature and progress.

Above-described embodiment is only one of preferred implementation of the present utility model, should not be taken to limit of the present utility model Protection domain, all in body design thought of the present utility model and the change having no essential meaning made mentally or polishing, It is solved the technical problem that still consistent with this utility model, all should be included in protection domain of the present utility model it In.

Claims (10)

1. integrated form polycarboxylic acids synthesis device, it is characterised in that: include the container (1) offering discharging opening, and be respectively provided with Reactor (2) in this container, agitating device (16), additive dropping system, raw materials system, LOAD CELLS (5) and electricity cabinet (9)；Described additive dropping system is connected with reactor (2) top, for being added by additive in the way of dropping Enter to reactor (2)；Described raw materials system is connected with reactor (2) side, is used for adding raw materials into reactor (2) In mix with additive；Described agitating device (16) is arranged on reactor (2), for being stirred by the material of mixing, makes Raw material reacts to each other with additive；Described LOAD CELLS (5) is arranged on reactor (2) bottom, for the thing in reactor Material is weighed in real time；Described reactor (2) is connected with discharging opening by pipeline, for outwards being supplied by reacted material；Described Electricity cabinet (9) is connected with agitating device (16), additive dropping system, raw materials system and LOAD CELLS (5) simultaneously, is used for Working power is provided.

Integrated form polycarboxylic acids synthesis device the most according to claim 1, it is characterised in that: described container also sets in (1) There is workbox (19).

Integrated form polycarboxylic acids synthesis device the most according to claim 1, it is characterised in that: described agitating device (16) is sleeping Formula blender.

4. according to the integrated form polycarboxylic acids synthesis device described in any one of claims 1 to 3, it is characterised in that: described additive Dropping system is provided with two, and each additive dropping system all includes the holding vessel (3) that stores additive, simultaneously and reactor (2) top connects, for the dropping pump (4) that additive is pumped in reactor, and be arranged on holding vessel (3) Circulating line connects, for the circulating pump (8) additive homogenizing being recycled in holding vessel.

Integrated form polycarboxylic acids synthesis device the most according to claim 4, it is characterised in that: described raw materials system includes Store the feed pot (7) of raw material, and be connected with reactor (2) side and feed pot (7) simultaneously, be used for adding raw materials into Pipeline pump (6) in reactor.

6. according to the integrated form polycarboxylic acids synthesis device described in claim 1,2,3 or 5, it is characterised in that: described reactor (2) Inside it is additionally provided with and adds heat pipe (18) for what the material of mixing was heated.

Integrated form polycarboxylic acids synthesis device the most according to claim 1, it is characterised in that: described reactor (2) side sets There is observation port (17).

Integrated form polycarboxylic acids synthesis device the most according to claim 1, it is characterised in that: described container (1) top is also It is respectively equipped with steam vent (11) and manhole (10).

Integrated form polycarboxylic acids synthesis device the most according to claim 8, it is characterised in that: arrange in described steam vent (11) There is ventilation fan (12).

Integrated form polycarboxylic acids synthesis device the most according to claim 1, it is characterised in that: described container is also opened on (1) It is provided with window (13).