CN205662622U - Single crystal cultivation device of controllable condition - Google Patents
Single crystal cultivation device of controllable condition Download PDFInfo
- Publication number
- CN205662622U CN205662622U CN201620576464.1U CN201620576464U CN205662622U CN 205662622 U CN205662622 U CN 205662622U CN 201620576464 U CN201620576464 U CN 201620576464U CN 205662622 U CN205662622 U CN 205662622U
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- single crystal
- crystal cultivation
- cultivation device
- device box
- pressure
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Abstract
The utility model provides a single crystal cultivation device of controllable condition, single crystal cultivation device box front mounted has the chamber door, pressure boost mouth and decompression mouth are installed to single crystal cultivation device box top, single crystal cultivation device box internally mounted has temperature sensor, pressure sensor, the infrared lamp strip, camera and single crystal cultivation bottle tray, the single crystal cultivation bottle has been placed on the single crystal cultivation bottle tray, the refrigerator is installed to the bottom of single crystal cultivation device box, single crystal cultivation device box side -mounting has microprocessor, touch display screen and wireless transceiver module, microprocessor respectively with temperature sensor, pressure sensor, the infrared lamp strip, the refrigerator, the camera, touch display screen, wireless transceiver module connects. The utility model provides a can control the device of single crystal cultivation environment, single crystal cultivation temperature, pressure condition can be controlled to this single crystal cultivation device, and the user can the remote monitoring growth of single crystal condition, and it is very convenient to use.
Description
Technical field
This utility model relates to experimental apparatus technical field, particularly relates to the single crystal cultivation device of a kind of controlled condition.
Background technology
Monocrystalline has widely in the structure elucidation in the fields such as Coordinative Chemistry, inorganic material chemistry, Organometallic Chemistry
Application, uses single crystal diffractometer to resolve crystal structure, it is necessary to turning out good monocrystalline, therefore single crystal cultivation is tied for compound
Structure resolves and has great importance.
Monocrystal cultivation method conventional in the lab has cooling method, biphase diffusion method, volatilization crystallization process, sol-gal process
Deng, crystal growth is affected by multiple extraneous factor, and the air pressure of temperature, solvent volatilization, the factor such as temperature changing speed are to crystalline substance
Bulk-growth all has a major impact.But generally laboratory cultures monocrystalline external condition is difficult to accurately control, and cultivates the success rate of monocrystalline
Relatively low, the monocrystalline of cultivation is usually present crystal defect, affects mono-crystalline structures and resolves, and experiment repeatability is poor.
Summary of the invention
This utility model is for the problems referred to above, it is provided that one can control single crystal cultivation temperature, pressure condition, convenient monitoring
The single crystal cultivation device of crystal growth situation.
The technical scheme that the above-mentioned technical problem of this utility model solution is used is as follows:
The single crystal cultivation device of a kind of controlled condition, including single crystal cultivation device box, chamber door, boost port, pressure-reduction outlet, temperature
Degree sensor, pressure transducer, infrared lamp bar, refrigerator, photographic head, microprocessor, touch display screen, radio receiving transmitting module,
Single crystal cultivation bottle holder dish, single crystal cultivation bottle, be provided with chamber door, single crystal cultivation device case before described single crystal cultivation device box
Body top is provided with boost port and pressure-reduction outlet, and single crystal cultivation device box is internally installed temperature sensor, pressure transducer, red
Outer lamp bar, photographic head and single crystal cultivation bottle holder dish, single crystal cultivation bottle holder dish is placed with single crystal cultivation bottle, single crystal cultivation device case
The bottom of body is provided with refrigerator, and single crystal cultivation device box side is provided with microprocessor, touches display screen and wireless receiving and dispatching
Module, microprocessor respectively with temperature sensor, pressure transducer, infrared lamp bar, refrigerator, photographic head, touch display screen, nothing
Line transceiver module connects.
Preferably, A/D change-over circuit it is provided with between described microprocessor and temperature sensor, pressure transducer.
Preferably, it is provided with control circuit between described microprocessor and infrared lamp bar, refrigerator.
Preferably, described boost port is internally installed drainage screen, and boost port is provided with valve I.
Preferably, described pressure-reduction outlet is provided with valve II.
This utility model has the advantages that the single crystal cultivation device of a kind of controlled condition, by infrared lamp bar and
Refrigerator can lift by program precise control of temperature, accesses high pressure air bottle by boost port, increases in single crystal cultivation device
Air pressure, slow down solution evaporation speed；Or access vacuum pump by pressure-reduction outlet, reduce the air pressure in single crystal cultivation device, accelerate molten
Liquid evaporation rate；Reaching to cultivate the optimum condition that different monocrystalline needs by controlling corresponding conditions, photographic head can gather simultaneously
The image of the growth of crystal, the operating state data of crystal growth situation and single crystal cultivation device is real by radio receiving transmitting module
Time be transferred to user, save human resources, simple to operate, improve single crystal cultivation efficiency and quality.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Fig. 2 is control structure schematic diagram of the present utility model.
In figure: 1-single crystal cultivation device box；2-chamber door；3-boost port；4-pressure-reduction outlet；5-temperature sensor；6-pressure
Sensor；7-infrared lamp bar；8-refrigerator；9-photographic head；10-microprocessor；11-touches display screen；12-wireless receiving and dispatching mould
Block；13-single crystal cultivation bottle holder dish；14-single crystal cultivation bottle；15-drainage screen；16-valve I；17-valve II.
Detailed description of the invention
For making the purpose of this utility model, technical scheme and advantage of greater clarity, come in detail below in conjunction with accompanying drawing
Embodiment of the present utility model is described.However, it should be understood that these describe the most exemplary, and it is not intended to limit this practicality
Novel scope.Additionally, in the following description, the description to known features and technology is eliminated, to avoid unnecessarily obscuring
Concept of the present utility model.
In describing the invention, it should be noted that term " " center ", " longitudinally ", " laterally ", " on ", D score,
Orientation or the position relationship of the instruction such as "front", "rear", "left", "right", " vertically ", " level ", " top ", " end " " interior ", " outward " are
Based on orientation shown in the drawings or position relationship, it is for only for ease of the description present invention and simplifies description rather than instruction or dark
The device or the element that show indication must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that right
The restriction of the present invention.
In describing the invention, it should be noted that unless otherwise clearly defined and limited, term " is installed ", " phase
Even ", " connection " should be interpreted broadly, for example, it may be fixing connection, it is also possible to be to removably connect, or be integrally connected；Can
To be mechanical connection, it is also possible to be electrical connection；Can be to be joined directly together, it is also possible to be indirectly connected to by intermediary, Ke Yishi
The connection of two element internals.For the ordinary skill in the art, can understand that above-mentioned term is at this with concrete condition
Concrete meaning in invention.
As shown in Figure 1 and Figure 2, the single crystal cultivation device of a kind of controlled condition, including single crystal cultivation device box 1, chamber door 2,
Boost port 3, pressure-reduction outlet 4, temperature sensor 5, pressure transducer 6, infrared lamp bar 7, refrigerator 8, photographic head 9, microprocessor 10,
Touch display screen 11, radio receiving transmitting module 12, single crystal cultivation bottle holder dish 13, single crystal cultivation bottle 14, before single crystal cultivation device box 1
Face is provided with chamber door 2, and single crystal cultivation device box 1 top is provided with boost port 3 and pressure-reduction outlet 4, in single crystal cultivation device box 1
Portion is provided with temperature sensor 5, pressure transducer 6, infrared lamp bar 7, photographic head 9 and single crystal cultivation bottle holder dish 13, single crystal cultivation
Being placed with single crystal cultivation bottle 14 on bottle holder dish 13, the bottom of single crystal cultivation device box 1 is provided with refrigerator 8, and single crystal cultivation fills
Put casing 1 side microprocessor 10 to be installed, touches display screen 11 and radio receiving transmitting module 12, microprocessor 10 respectively with temperature
Sensor 5, pressure transducer 6, infrared lamp bar 7, refrigerator 8, photographic head 9, touch display screen 11, radio receiving transmitting module 12 are even
Connect.
Further, A/D conversion electricity it is provided with between described microprocessor 10 and temperature sensor 5, pressure transducer 6
Road.
Further, it is provided with control circuit between described microprocessor 10 and infrared lamp bar 7, refrigerator 8.
Further, described boost port 3 is internally installed drainage screen 15, and boost port is provided with valve I 16.
Further, described pressure-reduction outlet 4 is provided with valve II 17.
The operation principle of detailed description of the invention of the present utility model is: combine Fig. 1, Fig. 2 and work of the present utility model is described
Principle, when using the single crystal cultivation device of controlled condition, the single crystal cultivation bottle 14 that will be equipped with culture solution is placed on single crystal cultivation
On bottle holder dish 13, temperature parameter is set by touching display screen 11, according to the physical property of single crystal cultivation liquid, can be set to constant
A certain temperature, it is also possible to programmed cooling or intensification are set.Arranging temperature parameter according to touching display screen 11, microprocessor 10 passes through
Control circuit controls infrared lamp bar 7 or refrigerator 8 state, and microprocessor 10 accepts temperature sensor 5, pressure transducer 6 detects
Data and photographic head 9 view data, and data are sent as user by radio receiving transmitting module 12, touch display screen 11 permissible
Display pressure, temperature and image information.When needs condition of normal pressure carries out single crystal cultivation, open valve I 16 or valve II 17, make
Single crystal cultivation device box 1 is internal to be in communication with the outside；When the difficult volatile solvent soln of single crystal cultivation liquid, crystal growth is slow, or
When can not grow, pressure-reduction outlet 4 accesses vacuum pump, control valve I 16 or valve II 17, keeps single crystal cultivation device box 1
Interior pressure subatmospheric, accelerates solution evaporation, promotes that crystal generates；When single crystal cultivation liquid is volatile solution, solution
Volatilize too fast, when formation polycrystalline or crystal growth defect are more, use the pressure increased in single crystal cultivation device box 1, slow down
Solution evaporation speed, accesses high pressure air bottle by boost port 3, increases the air pressure in single crystal cultivation device, by control valve I
16 or valve II 17, make single crystal cultivation device box 1 air pressure inside higher than room pressure.
The single crystal cultivation device of controlled condition, can be lifted by program precise control of temperature by infrared lamp bar and refrigerator,
Accessing high pressure air bottle by boost port, increase the air pressure in single crystal cultivation device, slow down solution evaporation speed；Or by decompression
Mouth accesses vacuum pump, reduces the air pressure in single crystal cultivation device, accelerates solution evaporation speed；Training is reached by controlling corresponding conditions
Supporting the optimum condition that different monocrystalline needs, photographic head can gather the image of growth of crystal simultaneously, by crystal growth situation and
The operating state data of single crystal cultivation device to user, saves human resources, operation letter by radio receiving transmitting module real-time Transmission
Single, improve single crystal cultivation efficiency and quality.
The foregoing describe embodiment of the present utility model, but described content only readily appreciates this utility model technology
Scheme and the embodiment that uses, skilled person will appreciate that of the industry, this utility model is not restricted to the described embodiments,
On the premise of without departing from this utility model spirit and scope, this utility model also has various changes and modifications, these changes
In the range of both falling within claimed this utility model with improvement.This utility model claims scope by appended claim
Book and equivalent thereof define.
Claims (5)
1. a single crystal cultivation device for controlled condition, including single crystal cultivation device box (1), chamber door (2), boost port (3), subtracts
Pressure mouth (4), temperature sensor (5), pressure transducer (6), infrared lamp bar (7), refrigerator (8), photographic head (9), microprocessor
(10), display screen (11), radio receiving transmitting module (12), single crystal cultivation bottle holder dish (13), single crystal cultivation bottle (14), its feature are touched
It is: described single crystal cultivation device box (1) is above provided with chamber door (2), and single crystal cultivation device box (1) top is provided with
Boost port (3) and pressure-reduction outlet (4), single crystal cultivation device box (1) is internally installed temperature sensor (5), pressure transducer
(6), infrared lamp bar (7), photographic head (9) and single crystal cultivation bottle holder dish (13), single crystal cultivation bottle holder dish (13) is placed with monocrystalline
Culture bottle (14), the bottom of single crystal cultivation device box (1) is provided with refrigerator (8), and single crystal cultivation device box (1) side is pacified
Equipped with microprocessor (10), touch display screen (11) and radio receiving transmitting module (12), microprocessor (10) respectively with temperature sensing
Device (5), pressure transducer (6), infrared lamp bar (7), refrigerator (8), photographic head (9), touch display screen (11), wireless receiving and dispatching mould
Block (12) connects.
The single crystal cultivation device of a kind of controlled condition the most according to claim 1, it is characterised in that: described microprocessor
And temperature sensor (5), pressure transducer are provided with A/D change-over circuit between (6) (10).
The single crystal cultivation device of a kind of controlled condition the most according to claim 1, it is characterised in that: described microprocessor
And infrared lamp bar (7), refrigerator are provided with control circuit between (8) (10).
The single crystal cultivation device of a kind of controlled condition the most according to claim 1, it is characterised in that: described boost port
(3) internally installed have drainage screen (15), and boost port is provided with valve I (16).
The single crystal cultivation device of a kind of controlled condition the most according to claim 1, it is characterised in that: described pressure-reduction outlet
(4) valve II (17) it is provided with.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620576464.1U CN205662622U (en) | 2016-06-16 | 2016-06-16 | Single crystal cultivation device of controllable condition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620576464.1U CN205662622U (en) | 2016-06-16 | 2016-06-16 | Single crystal cultivation device of controllable condition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205662622U true CN205662622U (en) | 2016-10-26 |
Family
ID=57154492
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620576464.1U Expired - Fee Related CN205662622U (en) | 2016-06-16 | 2016-06-16 | Single crystal cultivation device of controllable condition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205662622U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108103583A (en) * | 2017-12-29 | 2018-06-01 | 四川大学 | Low defect albumen monocrystal culture systems based on single drop microenvironment precision control |
| CN109652854A (en) * | 2018-12-29 | 2019-04-19 | 宁波卢米蓝新材料有限公司 | A kind of single crystal cultivation device and monocrystal cultivation method |
| CN113718341A (en) * | 2021-09-02 | 2021-11-30 | 郑州大学 | Visual single crystal culture apparatus |
-
2016
- 2016-06-16 CN CN201620576464.1U patent/CN205662622U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108103583A (en) * | 2017-12-29 | 2018-06-01 | 四川大学 | Low defect albumen monocrystal culture systems based on single drop microenvironment precision control |
| CN109652854A (en) * | 2018-12-29 | 2019-04-19 | 宁波卢米蓝新材料有限公司 | A kind of single crystal cultivation device and monocrystal cultivation method |
| CN113718341A (en) * | 2021-09-02 | 2021-11-30 | 郑州大学 | Visual single crystal culture apparatus |
| CN113718341B (en) * | 2021-09-02 | 2022-04-22 | 郑州大学 | Visual single crystal culture apparatus |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161026 Termination date: 20170616 |