CN205517719U - Reation kettle dewatering device with sample function - Google Patents
Reation kettle dewatering device with sample function Download PDFInfo
- Publication number
- CN205517719U CN205517719U CN201620129437.XU CN201620129437U CN205517719U CN 205517719 U CN205517719 U CN 205517719U CN 201620129437 U CN201620129437 U CN 201620129437U CN 205517719 U CN205517719 U CN 205517719U
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- kettle
- shaft
- platen
- probe tube
- pumping rod
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Abstract
The utility model discloses a reation kettle dewatering device with sample function, the reactor comprises a kettle, feed inlet and support, be fixed with the motor on the support, the (mixing) shaft is installed in the internal rotation of cauldron, the agitator is installed to the (mixing) shaft lower extreme, it is provided with the depression bar to slide in the (mixing) shaft, the depression bar top is connected with the cylinder, internal still slip of cauldron is provided with the pressure disk, the pressure disk outer fringe contacts with the internal wall of cauldron, be provided with the spout on the (mixing) shaft, middle part at the cauldron body is provided with the sampling tube, the other one end of sampling tube sets up sealed head, set up a pull pole in the sampling tube, at the sample connection setting valve of department, the one end of the inside pull pole of sampling tube be provided with with the anastomotic clamping block of the internal diameter of sampling tube. The utility model discloses avoid waste, sample accuracy, after the reaction finishes, motor stall, cylinder drive pressure lever driven pressure disk moves down along stirring epaxial spout, compresses tightly the compaction with the epoxy raw materials, and the back is opened to automatically controlled valve, and it includes the moisture that have and discharges from the outlet.
Description
Technical field
This utility model relates to a kind of chemical industry equipment, a kind of reactor dehydration device with sampled functions.
Background technology
Reactor is widely used in type of production user and the researchs of various scientific experiment project such as oil, chemical industry, rubber, pesticide, dyestuff, medicine, food, according to reaction condition to reactor structure function and the design of configuration adnexa.All can complete pre-set reactions steps with higher automaticity from the charging-reaction-discharging started, the important parameters such as the temperature in course of reaction, pressure, mechanics control, reactant or production concentration are carried out strict regulation and control.
At present, response situation at the material in reactor to Chemical Manufacture is monitored, it is to be sampled by arranging a probe tube on reactor, need to release sampling liquid sampling when, so there is techniques below problem: one is to ensure that sampling is accurately as far as possible, to release Subsampling liquid every time, therefore release sampling liquid every time and can cause the waste of material；Two is to release sampling thing when not exclusively cause lower sub-sampling every time, and the sampling liquid before being mixed into causes sampling inaccurate.And in present reactor, it is not dehydrated device, carry out dewatering efficiency again after the principle of synthesis being discharged low.
Utility model content
The purpose of this utility model is to provide a kind of reactor dehydration device with sampled functions, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the following technical scheme of this utility model offer:
nullA kind of reactor dehydration device with sampled functions，Including kettle，Kettle upper end is provided with charging aperture and support，Motor it is fixed with on support，Shaft it is rotatablely equipped with in kettle，Shaft lower end is provided with agitator，Cylinder it is also equipped with on support，Slide in shaft and be provided with depression bar，Depression bar top is connected with cylinder，Also slide in kettle and be provided with platen，Autoclave body bottom is provided with discharging opening and discharge outlet，Electrically-controlled valve it is provided with in discharge outlet，Platen outer rim contacts with inner wall of kettle，Chute it is provided with on shaft，Chute slides and is provided with pull bar，Pull bar one end connects depression bar，The other end connects platen，Second belt pulley is installed on motor，Shaft upper end is provided with the first belt pulley，Belt is connected on the first belt pulley and the second belt pulley，On platen and be positioned at immediately below charging aperture and be provided with charging hole，Platen is provided with sealing device for closing or turn on the connection of charging hole and lower section kettle；The middle part of kettle is provided with probe tube, the other end of probe tube arranges seal head, a piece pumping rod is set in probe tube, the length of pumping rod is more than the length of probe tube, arranging valve at sample tap, be provided with the clamping block that the internal diameter with probe tube coincide in one end of the pumping rod within probe tube, the other end of pumping rod arranges sprue through seal head, connect sample pipe at sample tap, going out, on sample pipe, valve is set
As further program of the utility model: described locking device includes sealing the rotating disk that rotation is installed in platen, center of turntable is provided with spline, spline it is provided with on shaft, rotating disk is slidably mounted on shaft by spline, rotating disk side is provided with circular hole, and when rotating disk turns to relevant position, described circular hole is conducted with charging hole.
As this utility model further scheme: be provided with heat exchange box outside kettle, heat exchanger tube it is provided with in heat exchange box, blower fan is installed in heat exchange box, heat exchange box is provided with the steam inlet and steam (vapor) outlet being connected respectively with heat exchanger tube two ends, heat exchange box side is additionally provided with exhaust outlet, being provided with air vent on platen, air vent upper end is connected to exhaust outlet by corrugated tube, and air vent lower end is inlayed and is provided with cordierite block.
As this utility model further scheme: the half of a diameter of probe tube diameter of described pumping rod.
As this utility model further scheme: it is at 1/3rd of probe tube total length that described sample tap is arranged on the distance of distance reactor on probe tube.
Compared with prior art, the beneficial effects of the utility model are: this utility model electric machine rotation is rotated by belt drives shaft, thus realize driving agitator to rotate and provide stirring.When after completion of the reaction, motor stalling, air cylinder driven depression bar drives platen to move down along the chute on shaft, carries out epoxy source material compressing compacting, and after electrically-controlled valve is opened, its moisture being contained within is discharged from discharge outlet.During initial charge, the raw material added at charging aperture charging hole from rotating disk drops in the kettle of lower section.After charging, charging hole is closed by sealing device, and when preventing binder to be dehydrated, epoxy resin is upwards scurried out from charging hole.Sampler it is additionally provided with on kettle, when needs sample when, by controlling pumping rod, pull-out pumping rod, liquid to be sampled can enter in probe tube under force, sample at sample tap, after sampling, sampling liquid in pumping rod is pushed in reactor, until the clamping block of pumping rod is resisted against on reactor, when again needing sampling when, repeat aforesaid operations, the reactor sampler using technical solutions of the utility model overcomes the existing situation released in the art every time and sample the waste that thing causes material, do not have the sampling liquid before being mixed into cause sampling inaccurate situation simultaneously yet.
Accompanying drawing explanation
Fig. 1 is the structural representation of the reactor dehydration device with sampled functions；
Fig. 2 is to have the cross-sectional view at platen position in the reactor dehydration device of sampled functions；
Fig. 3 is the plan structure schematic diagram of the reactor dehydration device turntable with sampled functions；
In figure: 1-kettle, 2-support, 3-cylinder, 4-motor, 5-belt, 6-the first belt pulley, 7-the second belt pulley, 8-charging aperture, 9-shaft, 10-platen, 11-agitator, 12-discharge outlet, 13-electrically-controlled valve, 14-heat exchange box, 15-blower fan, 16-steam inlet, 17-steam (vapor) outlet, 18-heat exchanger tube, 19-exhaust outlet, 20-depression bar, 21-chute, 22-rotating disk, 23-charging hole, 24-circular hole, 25-air vent, 26-cordierite block, 27-corrugated tube, 28-pull bar, 29-spline, 30-discharging opening, 31-sample tap, 32-clamping block, 33-pumping rod, 34-sprue, 35-probe tube, 36-valve, 37-goes out sample pipe.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the technical scheme of this patent is described in more detail.
nullRefer to Fig. 1-3，A kind of reactor dehydration device with sampled functions，Including kettle 1，Kettle 1 upper end is provided with charging aperture 8，Kettle 1 upper end is additionally provided with support 2，Motor 4 it is fixed with on support 2，Shaft 9 it is rotatablely equipped with in kettle 1，Shaft 9 lower end is provided with agitator 10，Cylinder 3 it is also equipped with on support 2，Slide in shaft 9 and be provided with depression bar 20，Depression bar 20 top is connected with cylinder 3，Also slide in kettle 1 and be provided with platen 10，Discharging opening 30 and discharge outlet 12 it is provided with bottom kettle 1，Electrically-controlled valve 13 it is provided with in discharge outlet 12，Platen 10 outer rim contacts with kettle 1 inwall，Chute 21 it is provided with on shaft 9，Chute 21 slides and is provided with pull bar 28，Pull bar 28 one end is connected to depression bar 20，The other end is connected to platen 10，Second belt pulley 7 is installed on motor 4，Shaft 9 upper end is provided with the first belt pulley 6，Belt 5 is connected on the first belt pulley 6 and the second belt pulley 7，On platen 10 and be positioned at immediately below charging aperture 8 and be provided with charging hole 23，Platen 10 is provided with sealing device for closing or turn on the connection of charging hole 23 and lower section kettle 1；The middle part of kettle 1 is provided with probe tube 35, the other end of probe tube 35 arranges seal head, a piece pumping rod 33 is set in probe tube 35, the length of pumping rod 33 is more than the length of probe tube 35, valve 36 is set at sample tap 31, the clamping block 32 that the internal diameter with probe tube 35 coincide it is provided with in one end of the pumping rod 33 within probe tube 35, the other end of pumping rod 33 arranges sprue 34 through seal head, connect sample pipe 37 at sample tap 31, going out, valve 36 is set on sample pipe 37, the half of a diameter of probe tube 35 diameter of pumping rod 33, sample tap 31 is arranged at the distance of distance kettle 11 on probe tube 35 is probe tube 35 total length 1/3rd.Motor 4 rotates through belt 5 and drives shaft 9 to rotate, thus realizes driving agitator 11 to rotate and provide stirring.When after completion of the reaction, motor 4 stall, cylinder 3 drives depression bar 20 to drive platen 10 to move down along the chute 21 on shaft 9, carries out epoxy source material compressing compacting, and after electrically-controlled valve 31 is opened, its moisture being contained within is discharged from discharge outlet 12.During initial charge, the raw material added at charging aperture 8 charging hole 23 from rotating disk 22 drops in the kettle 1 of lower section.After charging, charging hole 23 is closed by sealing device, and when preventing binder to be dehydrated, epoxy resin is upwards scurried out from charging hole 23；When needs sample from reactor when, close discharging opening 30, by controlling pumping rod 33, pull-out pumping rod 33, liquid to be sampled can enter in probe tube 35 under force, samples at sample tap 31, after sampling, sampling liquid in pumping rod 33 is pushed in kettle 1, until the clamping block 32 of pumping rod 33 is resisted against on kettle 1.
Locking device is following structure, it includes sealing the rotating disk 22 that rotation is installed in platen 10, rotating disk 22 is provided centrally with spline 29, it is provided with spline on shaft 9, rotating disk 22 is slidably mounted on shaft 9 by spline 29, rotating disk 22 side is provided with circular hole 24, and when rotating disk 22 turns to relevant position, circular hole 24 is conducted with charging hole 23.Rotating disk 22 can be followed platen about 10 by spline 29 and be moved relative to shaft 9.When starting reaction and adding raw material, the raw material added at charging aperture 8 drops in charging hole 23 circular hole 24 from rotating disk 22 in the kettle 1 of lower section.Rotating disk 22 rotates up to circular hole 24 and charging hole 23 mutual dislocation afterwards, it is achieved closed by charging hole 23, and now platen 10 pressure can carry out dewatering work.
Heat exchange box 14 it is provided with outside kettle 1, heat exchanger tube 18 it is provided with in heat exchange box 14, blower fan 15 is installed in heat exchange box 14, heat exchange box 14 is provided with and the steam inlet 16 that is connected with heat exchanger tube 18 two ends respectively and steam (vapor) outlet 17, heat exchange box 14 side is additionally provided with exhaust outlet 19, air vent 25 it is provided with on platen 10, air vent 25 upper end is connected to exhaust outlet 19 by corrugated tube 27, air vent 25 lower end is inlayed and is provided with cordierite block 26, and when rotating disk 22 turns to relevant position, circular hole 24 is conducted with air vent 25.Vapours flows out after entering heat exchanger tube 18 heat exchange from steam inlet 16 from steam (vapor) outlet 17, hot-air in heat exchange box 14 is flowed at platen 10 through corrugated tube 27 from exhaust outlet 19 by heat exchange rear fan 15, corrugated tube 27 may insure that when platen 10 moves up and down follow flexible.When after platen 10 hold-down ring epoxy resins, shaft 9 drives rotating disk 22 to rotate, make circular hole 24 turn to air vent 25 to be conducted, now hot-air heats epoxy source material from air vent 25 in cordierite block 26 is flowed into bottom kettle 1, make the moisture rapid evaporation that it contains, improve rate of water loss.Cordierite block 26 may insure that epoxy source material does not penetrates into and gas can flow downward.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art is possessed, it is also possible to make a variety of changes on the premise of without departing from this patent objective.
Claims (5)
- null1. a reactor dehydration device with sampled functions，Including kettle，It is characterized in that，Kettle upper end is provided with charging aperture and support，Motor it is fixed with on support，Shaft it is rotatablely equipped with in kettle，Shaft lower end is provided with agitator，Cylinder it is also equipped with on support，Slide in shaft and be provided with depression bar，Depression bar top is connected with cylinder，Also slide in kettle and be provided with platen，Autoclave body bottom is provided with discharging opening and discharge outlet，Electrically-controlled valve it is provided with in discharge outlet，Platen outer rim contacts with inner wall of kettle，Chute it is provided with on shaft，Chute slides and is provided with pull bar，Pull bar one end connects depression bar，The other end connects platen，Second belt pulley is installed on motor，Shaft upper end is provided with the first belt pulley，Belt is connected on the first belt pulley and the second belt pulley，On platen and be positioned at immediately below charging aperture and be provided with charging hole，Platen is provided with sealing device for closing or turn on the connection of charging hole and lower section kettle；The middle part of kettle is provided with probe tube, the other end of probe tube arranges seal head, a piece pumping rod is set in probe tube, the length of pumping rod is more than the length of probe tube, arranging valve at sample tap, be provided with the clamping block that the internal diameter with probe tube coincide in one end of the pumping rod within probe tube, the other end of pumping rod arranges sprue through seal head, connect sample pipe at sample tap, going out, on sample pipe, valve is set.
- The reactor dehydration device with sampled functions the most according to claim 1, it is characterized in that, described locking device includes sealing the rotating disk that rotation is installed in platen, center of turntable is provided with spline, spline it is provided with on shaft, rotating disk is slidably mounted on shaft by spline, and rotating disk side is provided with circular hole, and when rotating disk turns to relevant position, described circular hole is conducted with charging hole.
- The reactor dehydration device with sampled functions the most according to claim 1, it is characterized in that, heat exchange box it is provided with outside kettle, being provided with heat exchanger tube in heat exchange box, be provided with blower fan in heat exchange box, heat exchange box is provided with the steam inlet and steam (vapor) outlet being connected respectively with heat exchanger tube two ends, heat exchange box side is additionally provided with exhaust outlet, being provided with air vent on platen, air vent upper end is connected to exhaust outlet by corrugated tube, and air vent lower end is inlayed and is provided with cordierite block.
- The reactor dehydration device with sampled functions the most according to claim 1, it is characterised in that the half of a diameter of probe tube diameter of described pumping rod.
- The reactor dehydration device with sampled functions the most according to claim 1, it is characterised in that it is at 1/3rd of probe tube total length that described sample tap is arranged on the distance of distance reactor on probe tube.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620129437.XU CN205517719U (en) | 2016-02-20 | 2016-02-20 | Reation kettle dewatering device with sample function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620129437.XU CN205517719U (en) | 2016-02-20 | 2016-02-20 | Reation kettle dewatering device with sample function |
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| Publication Number | Publication Date |
|---|---|
| CN205517719U true CN205517719U (en) | 2016-08-31 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620129437.XU Expired - Fee Related CN205517719U (en) | 2016-02-20 | 2016-02-20 | Reation kettle dewatering device with sample function |
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| CN (1) | CN205517719U (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107715819A (en) * | 2017-10-25 | 2018-02-23 | 张子和 | The quick reaction device that a kind of laboratory uses |
| CN108786583A (en) * | 2018-07-12 | 2018-11-13 | 芜湖鑫霖森椽环保科技有限公司 | A kind of sewage disposal chemicals dosing plant |
| CN109130065A (en) * | 2018-08-28 | 2019-01-04 | 宁夏龙江化工科技有限公司 | A kind of quantitative glue injection device of high-temperature resin transfer modling |
| CN112128485A (en) * | 2020-09-28 | 2020-12-25 | 湛江市长合环保科技有限公司 | Butt joint pipeline convenient to overhaul, disassemble and assemble for water treatment |
| CN112747259A (en) * | 2021-01-21 | 2021-05-04 | 碎得机械(北京)有限公司 | Sealed treatment bin and dangerous waste treatment system |
| CN112774610A (en) * | 2021-01-07 | 2021-05-11 | 南阳理工学院 | Chemical dyeing raw material rapid reaction device and working method |
| CN112871119A (en) * | 2021-02-02 | 2021-06-01 | 北京图腾猎技科技有限公司 | Antibiotic composition biosynthesis equipment |
| CN113213503A (en) * | 2021-06-23 | 2021-08-06 | 南京永成分子筛有限公司 | Sodium-based oxygen generation molecular sieve and preparation process thereof |
-
2016
- 2016-02-20 CN CN201620129437.XU patent/CN205517719U/en not_active Expired - Fee Related
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107715819A (en) * | 2017-10-25 | 2018-02-23 | 张子和 | The quick reaction device that a kind of laboratory uses |
| CN108786583A (en) * | 2018-07-12 | 2018-11-13 | 芜湖鑫霖森椽环保科技有限公司 | A kind of sewage disposal chemicals dosing plant |
| CN109130065A (en) * | 2018-08-28 | 2019-01-04 | 宁夏龙江化工科技有限公司 | A kind of quantitative glue injection device of high-temperature resin transfer modling |
| CN112128485A (en) * | 2020-09-28 | 2020-12-25 | 湛江市长合环保科技有限公司 | Butt joint pipeline convenient to overhaul, disassemble and assemble for water treatment |
| CN112128485B (en) * | 2020-09-28 | 2022-02-22 | 湛江市长合环保科技有限公司 | Butt joint pipeline convenient to overhaul, disassemble and assemble for water treatment |
| CN112774610A (en) * | 2021-01-07 | 2021-05-11 | 南阳理工学院 | Chemical dyeing raw material rapid reaction device and working method |
| CN112774610B (en) * | 2021-01-07 | 2023-01-06 | 南阳理工学院 | Chemical dyeing raw material rapid reaction device and working method |
| CN112747259A (en) * | 2021-01-21 | 2021-05-04 | 碎得机械(北京)有限公司 | Sealed treatment bin and dangerous waste treatment system |
| CN112871119A (en) * | 2021-02-02 | 2021-06-01 | 北京图腾猎技科技有限公司 | Antibiotic composition biosynthesis equipment |
| CN113213503A (en) * | 2021-06-23 | 2021-08-06 | 南京永成分子筛有限公司 | Sodium-based oxygen generation molecular sieve and preparation process thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160831 Termination date: 20190220 |