CN205323273U - High -efficient antiseized crystallization reaction unit who attaches - Google Patents
High -efficient antiseized crystallization reaction unit who attaches Download PDFInfo
- Publication number
- CN205323273U CN205323273U CN201620073743.6U CN201620073743U CN205323273U CN 205323273 U CN205323273 U CN 205323273U CN 201620073743 U CN201620073743 U CN 201620073743U CN 205323273 U CN205323273 U CN 205323273U
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- reaction vessel
- rotating seat
- cooling
- end cap
- middle cylinder
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a high -efficient antiseized crystallization reaction unit who attaches, including the inner tank with outer jar, jar inside inner tank that sets up wherein sets up the clearance in order to constitute reaction vessel between outer jar and the inner tank outward, bearing swing joint roating seat is passed through at reaction vessel's top, reaction vessel's inside sets up cooling coil, and the one end of the recess and the middle barrel at roating seat top is connected respectively at cooling coil's both ends to realize the inside circulation of coolant liquid, the reaction vessel top sets up the charge door, and reaction vessel's bottom sets up bin outlet and supersonic generator. The utility model discloses a cooling coil that the roating seat drove in the reaction vessel takes place to rotate to make the even cooling of inside solution, make the crystallization efficient and stable, cooperate the supersonic generator spaced to send the ultrasonic wave vibrations simultaneously, make the crystal can not the adhesion at reaction vessel's inner wall, the phenomenon of blockking up can not take place yet.
Description
Technical field
This utility model relates to a kind of crystallization reaction device, the specifically crystallization reaction device of a kind of efficient anti-adhesion。
Background technology
Inside chemistry, after the saturated solution cooling of heat, solute precipitates out with the form of crystal, and this process is crystallization。Adopting crystallization kettle that solution is cooled down in Chemical Manufacture, crystallization kettle is after mixing of materials reaction, the crystallizer that still domestic demand chilled water or chilled water are sharply lowered the temperature。Existing crystallization kettle structure is complex, is substantially use chuck and cools down, and jacket for heat exchange area is little, and fluid-flow rate is little, and heat transfer coefficient is not high, thus causing that material cooling is uneven, thus affecting crystal habit。Meanwhile, there is also discharging opening and easily lump, the defect such as non-separation of solid-liquid after crystallization。The existing type of cooling is all external refrigeration simultaneously so that internal cooling is unstable, and crystal precipitates out instability。
Utility model content
The purpose of this utility model is in that to provide the crystallization reaction device of a kind of efficient anti-adhesion, with the problem solving to propose in above-mentioned background technology。
For achieving the above object, this utility model provides following technical scheme:
A kind of crystallization reaction device of efficient anti-adhesion, including rotating seat, bearing, charge door, end cap, interior cool down out liquid interface, interior cooling feed liquor interface, middle cylinder, cooling coil, inner canister, outer tank, discharge gate and supersonic generator, inner canister is set inside described outer tank to constitute reaction vessel, gap is wherein set between outer tank and inner canister；The top of described reaction vessel is flexibly connected rotating seat by bearing, fixing one end connecting middle cylinder in the groove at rotating seat top, and the groove ends at rotating seat top is flexibly connected end cap by bearing, the top of end cap cools down feed liquor interface in connecting, the other end of middle cylinder cools down out liquid interface in being connected by bearing, the described interior liquid interface that cools down out is connected in the surface of end cap by connector, and interior cools down out liquid interface and interior cooling feed liquor interface connects cooling system respectively；The inside of described reaction vessel arranges cooling coil, the two ends of cooling coil connect the groove at rotating seat top and one end of middle cylinder respectively, thus realizing the circulation within coolant, described reaction vessel top arranges charge door, and the bottom of reaction vessel arranges discharge gate and supersonic generator。
As further program of the utility model: the two ends up and down of described outer tank are respectively mounted and outer cool down out liquid interface and outer cooling feed liquor interface。
As further program of the utility model: arrange sealing ring between described end cap and rotating seat, sealing ring is set between end cap and middle cylinder, and middle cylinder and interior cooling out arrange sealing ring between liquid interface。
As further program of the utility model: the outer surface of cupular part fixed installation belt pulley of described rotating seat, belt pulley connects the belt pulley on motor output shaft by belt。
As further program of the utility model: described charge door connects feeding tube or vacuum extractor。
As further program of the utility model: described discharge gate arranges valve。
Compared with prior art, the beneficial effects of the utility model are: drive the cooling coil in reaction vessel to rotate by rotating seat, so that internal solution cools down uniformly, make crystal precipitation efficiency high and stable, what coordinate supersonic generator interval sends vibration of ultrasonic wave simultaneously, make crystal will not stick to the inwall of reaction vessel, without the phenomenon that blocking occurs。
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model。
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is clearly and completely described, it is clear that described embodiment is only a part of embodiment of this utility model, rather than whole embodiments。Based on the embodiment in this utility model, the every other embodiment that those of ordinary skill in the art obtain under not making creative work premise, broadly fall into the scope of this utility model protection。
Refer to Fig. 1, in this utility model embodiment, a kind of crystallization reaction device of efficient anti-adhesion, including rotating seat 1, bearing 2, charge door 3, end cap 4, inside cool down out liquid interface 5, interior cooling feed liquor interface 6, belt 7, motor 8, middle cylinder 9, cooling coil 10, inner canister 11, outer tank 12, discharge gate 13, valve 14 and supersonic generator 15, described outer tank 12 is internal arranges inner canister 11 to constitute reaction vessel, wherein between outer tank 12 and inner canister 11, gap is set, and the two ends up and down of outer tank 12 are respectively mounted and outer cool down out liquid interface and outer cooling feed liquor interface, so that flowing in the gap that coolant is between outer tank 12 and inner canister 11, thus the heat taken away in inner canister 11, solution in inner canister 11 is lowered the temperature, crystal is quickly precipitated out；The top of described reaction vessel is flexibly connected rotating seat 1 by bearing, fixing one end connecting middle cylinder 9 in the groove at rotating seat 1 top, and the groove ends at rotating seat 1 top is flexibly connected end cap 4 by bearing, thus ensureing that when rotating seat 1 rotates, end cap 4 can not rotate, the top of end cap 4 cools down feed liquor interface 6 in connecting, the other end of middle cylinder 9 cools down out liquid interface 5 by bearing in being connected, the described interior liquid interface 5 that cools down out is connected in the surface of end cap 4 by connector, and interior cools down out liquid interface 5 and interior cooling feed liquor interface 6 connects cooling system respectively。
The inside of described reaction vessel arranges cooling coil 10, the two ends of cooling coil 10 connect the groove at rotating seat 1 top and one end of middle cylinder 9 respectively, thus realizing the circulation within coolant, cooling coil 10 can occur to rotate slowly along with rotating seat 1 simultaneously, make internal cooling, cooling is uniformly so that crystal quickly precipitates out。
Sealing ring is set between described end cap 4 and rotating seat 1, sealing ring is set between end cap 4 and middle cylinder 9, and middle cylinder 9 and interior cooling out arrange sealing ring between liquid interface 5, it is ensured that overall tightness。
The outer surface of cupular part fixed installation belt pulley of described rotating seat 1, belt pulley connects the belt pulley on motor 8 output shaft by belt 7, seat 1 is rotated by motor 8 and rotates。
Described reaction vessel top arranges charge door 3, is connected feeding tube or vacuum extractor by charge door 3, it is achieved reinforced before work, the function of evacuation in work。
The bottom of described reaction vessel arranges discharge gate 13 and supersonic generator 15, wherein discharge gate 13 arranges valve 14, vibration of ultrasonic wave is sent so that crystal will not stick to the inwall of reaction vessel, without the phenomenon that blocking occurs by supersonic generator 15 interval。
Operation principle of the present utility model is: drive the cooling coil 10 in reaction vessel to rotate by rotating seat 1, so that internal solution cools down uniformly, make crystal precipitation efficiency high and stable, what coordinate supersonic generator 15 interval sends vibration of ultrasonic wave simultaneously, make crystal will not stick to the inwall of reaction vessel, without the phenomenon that blocking occurs。
It is obvious to a person skilled in the art that this utility model is not limited to the details of above-mentioned one exemplary embodiment, and when without departing substantially from spirit of the present utility model or basic feature, it is possible to realize this utility model in other specific forms。Therefore, no matter from which point, embodiment all should be regarded as exemplary, and be nonrestrictive, scope of the present utility model is limited by claims rather than described above, it is intended that all changes in the implication of the equivalency dropping on claim and scope included in this utility model。Any accompanying drawing labelling in claim should be considered as the claim that restriction is involved。
In addition, it is to be understood that, although this specification is been described by according to embodiment, but not each embodiment only comprises an independent technical scheme, this narrating mode of description is only for clarity sake, description should be made as a whole by those skilled in the art, and the technical scheme in each embodiment through appropriately combined, can also form other embodiments that it will be appreciated by those skilled in the art that。
Claims (6)
1. the crystallization reaction device of an efficient anti-adhesion, including rotating seat, bearing, charge door, end cap, interior cool down out liquid interface, interior cooling feed liquor interface, middle cylinder, cooling coil, inner canister, outer tank, discharge gate and supersonic generator, it is characterized in that, inner canister is set inside described outer tank to constitute reaction vessel, gap is wherein set between outer tank and inner canister；The top of described reaction vessel is flexibly connected rotating seat by bearing, fixing one end connecting middle cylinder in the groove at rotating seat top, and the groove ends at rotating seat top is flexibly connected end cap by bearing, the top of end cap cools down feed liquor interface in connecting, the other end of middle cylinder cools down out liquid interface in being connected by bearing, the described interior liquid interface that cools down out is connected in the surface of end cap by connector, and interior cools down out liquid interface and interior cooling feed liquor interface connects cooling system respectively；The inside of described reaction vessel arranges cooling coil, the two ends of cooling coil connect the groove at rotating seat top and one end of middle cylinder respectively, thus realizing the circulation within coolant, described reaction vessel top arranges charge door, and the bottom of reaction vessel arranges discharge gate and supersonic generator。
2.RootCrystallization reaction device according to a kind of efficient anti-adhesion described in claim 1, it is characterised in that the two ends up and down of described outer tank are respectively mounted and outer cool down out liquid interface and outer cooling feed liquor interface。
3. the crystallization reaction device of a kind of efficient anti-adhesion according to claim 1, it is characterized in that, sealing ring is set between described end cap and rotating seat, sealing ring is set between end cap and middle cylinder, and middle cylinder and interior cooling out arrange sealing ring between liquid interface。
4. the crystallization reaction device of a kind of efficient anti-adhesion according to claim 1, it is characterised in that the outer surface of cupular part fixed installation belt pulley of described rotating seat, belt pulley connects the belt pulley on motor output shaft by belt。
5.RootCrystallization reaction device according to a kind of efficient anti-adhesion described in claim 1, it is characterised in that described charge door connects feeding tube or vacuum extractor。
6. the crystallization reaction device of a kind of efficient anti-adhesion according to claim 1, it is characterised in that on described discharge gate, valve is set。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620073743.6U CN205323273U (en) | 2016-01-26 | 2016-01-26 | High -efficient antiseized crystallization reaction unit who attaches |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620073743.6U CN205323273U (en) | 2016-01-26 | 2016-01-26 | High -efficient antiseized crystallization reaction unit who attaches |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205323273U true CN205323273U (en) | 2016-06-22 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620073743.6U Expired - Fee Related CN205323273U (en) | 2016-01-26 | 2016-01-26 | High -efficient antiseized crystallization reaction unit who attaches |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205323273U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109529399A (en) * | 2018-12-11 | 2019-03-29 | 广州风行乳业股份有限公司 | A kind of manifold formula crystallizing tank |
| CN110227280A (en) * | 2019-06-14 | 2019-09-13 | 南京恒桥化学技术材料有限公司 | A kind of photoinitiator crystallizing device of anti-inner wall crystallization |
-
2016
- 2016-01-26 CN CN201620073743.6U patent/CN205323273U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109529399A (en) * | 2018-12-11 | 2019-03-29 | 广州风行乳业股份有限公司 | A kind of manifold formula crystallizing tank |
| CN110227280A (en) * | 2019-06-14 | 2019-09-13 | 南京恒桥化学技术材料有限公司 | A kind of photoinitiator crystallizing device of anti-inner wall crystallization |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160622 Termination date: 20180126 |