CN205182704U - Sulfur dichloride prepares reactor - Google Patents
Sulfur dichloride prepares reactor Download PDFInfo
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- CN205182704U CN205182704U CN201520934748.9U CN201520934748U CN205182704U CN 205182704 U CN205182704 U CN 205182704U CN 201520934748 U CN201520934748 U CN 201520934748U CN 205182704 U CN205182704 U CN 205182704U
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- tank body
- sulfur dichloride
- reactor
- refrigerant
- jar body
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Abstract
The utility model discloses a sulfur dichloride prepares reactor, press from both sides the jacketed jar of body including having, the top of jar body is equipped with dismantled and assembled head, and the top of head is equipped with solid feeding hole, gaseous feed inlet and tail gas export, and the middle part of jar body is equipped with a plurality of sight glasss, and the well lower part of jar body is equipped with discharge gate and sample connection, and the bottom of jar body is equipped with cooling water inlet and emptying mouth, and a jar internal portion is equipped with a straight tube, and the one end of straight tube is equipped with the flange with gaseous feed inlet extension union coupling, the other end extend jar body bottom and with a plurality of gas distribution union couplings formation T fonts, the efficiency of gas -liquid looks contact time and area, gaseous dispersion effect, the withstand voltage security of reactor, the reaction is visual, the reaction is improved.
Description
Technical field
The utility model relates to a kind of Reactive Synthesis device, is that a kind of sulfur dichloride produces reactor specifically.
Background technology
Sulfur dichloride and sulfur monochloride use mainly as the intermediate in sulfur-bearing analog assistant production process, sulfur dichloride and sulfur monochloride poisonous, easily decompose, it produces extremely difficult control.At present, its Reactive Synthesis device mainly adopts withstand voltage glass jar or enamel tank reactor, and withstand voltage glass jar is low due to safety coefficient, is only limitted to small lot and produces, although and tank reactor improves security, also there is shortcoming.One is cannot effective monitoring for course of reaction, and two is that its sealing is strong, easily causes leak source, etching apparatus, three be gas with liquid comes into contact not evenly, production efficiency and of low quality.
Utility model content
The utility model object is to overcome the low and tank reactor poor visibility of glass reactor safety coefficient, and sealing is not high, the shortcoming that reaction efficiency is low.
The utility model solves the technical scheme that its technical problem adopts: a kind of sulfur dichloride produces reactor, comprise the tank body with chuck layer, the top of described tank body is provided with removable end socket, the top of end socket is provided with feeding-in solid body mouth, gas feed mouth and offgas outlet, the middle part of tank body is provided with some visors, the middle and lower part of tank body is provided with discharging opening and sample tap, the bottom of tank body is provided with cooling water inlet and discharging hole, tank interior is provided with a straight tube, one end of straight tube is provided with the flange be connected with gas feed mouth extension tube, the other end extends tank base and is connected to form T-shaped with some gas distribution tubes.
As preferably, the ratio of described tank body length and width is 6-7:1.
Preferably, described each visor is arranged in different angles in the middle part of tank body and differing heights.
Preferably, the material of described tank body is stainless steel.
Preferably, described gas distribution tube is evenly distributed with some abscesses.
Preferably, the bottom of described tank body chuck layer is provided with refrigerant inlet and refrigerant discharging hole, and the upper end of tank body chuck layer is provided with refrigerant exit and refrigerant temperature-measuring port.
The beneficial effects of the utility model are: increase the main length of tank of reactor, shorten tank body width, and gas up springs up distance along inner straight tube by tank base to be increased because length of tank increases, and extends path.Simultaneously because air inlet straight tube tail end vertical direction connects several band abscess straight tube, favourable gas is uniformly distributed in tank body; Both combine, and increase gas and liquid comes into contact, improve reaction efficiency; Increase several visor, be conducive to the observation of course of reaction and the judgement of reaction end; In the discharging of tank body middle and lower part, can prevent impurities at bottom from flowing out.
Accompanying drawing explanation
Fig. 1 is the structural representation that sulfur dichloride produces reactor.
1-chlorine inlet, 2-sulphur charging aperture, 3-offgas outlet, 4-end socket, 5-screw rod, 6-tank body, 7-refrigerant exit, 8-refrigerant temperature-measuring port, 9-chuck layer, 10-air inlet pipe, 11-visor, 12-material temperature-measuring port, 13-sample tap, 14-discharging opening, 15-refrigerant inlet, 16-discharging hole, 17-gas distribution tube, 18-refrigerant discharging hole in figure.
Detailed description of the invention
The technical problem solved to make the utility model, technical scheme and beneficial effect are clearly understood, below in conjunction with accompanying drawing and embodiment, are further described the utility model.Should be appreciated that embodiment described herein only for explaining the utility model, and be not used in restriction the utility model.
As shown in Figure 1, a kind of sulfur dichloride of the utility model produces reactor, comprise the tank body 6 with chuck layer 9, tank body 6 adopts stainless steel to make, the top of tank body 6 is provided with removable end socket 4, end socket 4 is connected by screw rod 5 with tank body 6, the top of end socket 4 is provided with sulphur charging aperture 2, chlorine inlet 1 and offgas outlet 3, around the middle part of tank body 6, different angles and differing heights distributed six visors 11 respectively, the middle and lower part of tank body 6 is provided with discharging opening 14 and sample tap 13, the bottom of tank body 6 is provided with cooling water inlet and discharging hole 16, tank body 6 inside is provided with an air inlet pipe 10, one end of air inlet pipe 10 is provided with the flange be connected with chlorine inlet 1 extension tube, the other end to extend bottom tank body 6 and is connected to form T-shaped with four gas distribution tubes 17, gas distribution tube 17 is evenly distributed with some abscesses, the bottom of tank body 6 chuck layer 9 is provided with refrigerant inlet 15 and refrigerant discharging hole 18, and upper end is provided with refrigerant exit 7 and refrigerant temperature-measuring port 8.
During work, add quantitative sulphur from sulphur charging aperture 2, pass into constant pressure chlorine from chlorine inlet 1, chlorine to be flowed out by gas distribution tube 17 by air inlet pipe 10 and to contact with bottom sulphur and to react, and unnecessary chlorine is flowed out by offgas outlet 3; Pass into refrigerant by refrigerant inlet 15 to chuck layer 9, refrigerant upwards flows and flows back to refrigeration plant through refrigerant exit 7 in chuck, and recycle, refrigerant temperature-measuring port 8 can measure refrigerant temperature; In course of reaction, observe temperature of charge by material temperature-measuring port 12, regulate reaction temperature by refrigerant pressure; When reaction proceeds to the middle and later periods, observe level condition in tank body 6 by visor 11, regulate chlorine gas pressure in conjunction with level condition and judge reaction end; After reaction terminates, get material sample by sample tap 13 and carry out analysis detection, detect qualified rear material and release use by material outlet 14, under material outlet 14 liquid level, material uses as next reaction mass seed, also can regularly be discharged by discharging hole 16.
Compared with existing withstand voltage glass jar reactor or enamel tank reactor, improve the security performance of equipment, reduce simultaneously and run leakage phenomenon because equipment seals the chlorine that strong band is next, pollute; In course of reaction can fully observing response process and therefore adjustable admission pressure optimize reaction and judge reaction terminal; The gas dispersion apparatus increased, than agitating mode dispersed gas liquid phase better, improves reaction efficiency.
Improve the security performance of equipment, reduce simultaneously and run the phenomenon of leaking and polluting because equipment seals the chlorine that strong band is not next; In course of reaction can fully observing response process and therefore adjustable admission pressure optimize reaction and judge reaction terminal; The gas dispersion apparatus increased, than agitating mode dispersed gas liquid phase better, improves reaction efficiency.
The foregoing is only preferred embodiment of the present utility model, not in order to limit the utility model, all any amendment, on an equal basis replacement and improvement etc. done within spirit of the present utility model and principle, all should drop within protection domain of the present utility model.
Claims (6)
1. a sulfur dichloride produces reactor, it is characterized in that: comprise the tank body with chuck layer, the top of described tank body is provided with removable end socket, the top of end socket is provided with feeding-in solid body mouth, gas feed mouth and offgas outlet, the middle part of tank body is provided with some visors, the middle and lower part of tank body is provided with discharging opening and sample tap, the bottom of tank body is provided with cooling water inlet and discharging hole, tank interior is provided with a straight tube, one end of straight tube is provided with the flange be connected with gas feed mouth extension tube, and the other end extends tank base and is connected to form T-shaped with some gas distribution tubes.
2. a kind of sulfur dichloride according to claim 1 produces reactor, it is characterized in that: the ratio of described tank body length and width is 6-7:1.
3. a kind of sulfur dichloride according to claim 1 produces reactor, it is characterized in that: described each visor is arranged in different angles in the middle part of tank body and differing heights.
4. a kind of sulfur dichloride according to claim 1 produces reactor, it is characterized in that: the material of described tank body is stainless steel.
5. a kind of sulfur dichloride according to claim 1 produces reactor, it is characterized in that: described gas distribution tube is evenly distributed with some abscesses.
6. a kind of sulfur dichloride according to claim 1 produces reactor, it is characterized in that: the bottom of described tank body chuck layer is provided with refrigerant inlet and refrigerant discharging hole, and the upper end of tank body chuck layer is provided with refrigerant exit and refrigerant temperature-measuring port.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520934748.9U CN205182704U (en) | 2015-11-19 | 2015-11-19 | Sulfur dichloride prepares reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520934748.9U CN205182704U (en) | 2015-11-19 | 2015-11-19 | Sulfur dichloride prepares reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205182704U true CN205182704U (en) | 2016-04-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520934748.9U Active CN205182704U (en) | 2015-11-19 | 2015-11-19 | Sulfur dichloride prepares reactor |
Country Status (1)
| Country | Link |
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| CN (1) | CN205182704U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109433113A (en) * | 2018-11-08 | 2019-03-08 | 镇江先锋植保科技有限公司 | Thiodicarb production equipment |
-
2015
- 2015-11-19 CN CN201520934748.9U patent/CN205182704U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109433113A (en) * | 2018-11-08 | 2019-03-08 | 镇江先锋植保科技有限公司 | Thiodicarb production equipment |
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| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |