CN204973885U - Can stir horizontal tubular atmosphere reactor of microwave - Google Patents
Can stir horizontal tubular atmosphere reactor of microwave Download PDFInfo
- Publication number
- CN204973885U CN204973885U CN201520611926.4U CN201520611926U CN204973885U CN 204973885 U CN204973885 U CN 204973885U CN 201520611926 U CN201520611926 U CN 201520611926U CN 204973885 U CN204973885 U CN 204973885U
- Authority
- CN
- China
- Prior art keywords
- pipe
- crucible
- quartz
- reactor
- quartz ampoule
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000003756 stirring Methods 0.000 title claims abstract description 17
- 239000010453 quartz Substances 0.000 claims abstract description 46
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 46
- 229920000742 Cotton Polymers 0.000 claims abstract description 8
- 239000005030 aluminium foil Substances 0.000 claims abstract description 8
- 238000004321 preservation Methods 0.000 claims abstract description 8
- 239000003708 ampul Substances 0.000 claims description 26
- 238000005245 sintering Methods 0.000 abstract description 4
- 238000003746 solid phase reaction Methods 0.000 abstract description 3
- 239000002775 capsule Substances 0.000 abstract 6
- 230000002093 peripheral effect Effects 0.000 abstract 1
- 239000000376 reactant Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 3
- 239000007790 solid phase Substances 0.000 description 3
- 230000002159 abnormal effect Effects 0.000 description 2
- 238000004320 controlled atmosphere Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
Abstract
The utility model relates to a can stir horizontal tubular atmosphere reactor of microwave belongs to metallurgical equipment technical field. These reactor quartz capsule both sides are equipped with quartzy furnace gate through the screw, quartzy furnace gate one side is equipped with the intake pipe, the opposite side is equipped with the outlet duct, be equipped with the waveguide entry on the furnace chamber outer wall of quartz capsule, the inside crucible that is equipped with of quartz capsule, the body keeps warm in the peripheral parcel of crucible, the crucible top is equipped with the three -way pipe, middle pipe is followed the quartz capsule top through the plug and is inserted the agitator, one of them lateral duct is crossed plug follow quartz capsule top and is inserted the thermocouple, remaining pipe is the intake pipe, the quartz capsule is followed interiorly to wrapping up the aluminium foil outward with the pipeline that quartzy furnace gate is connected, heat preservation cotton and woven wire. This reactor can prevent the sintering phenomenon among the metallurgical solid phase reaction through the stirring.
Description
Technical field
The one that relates to the utility model can stir microwave horizontal pipe atmosphere reactor, belongs to technical field of metallurgical equipment.
Background technology
In microwave metallurgical, some solid phase reactions need to react under different atmospheric conditions, and existing microwave batch-type furnace is too large and air-tightness reason because of cavity, uncontrollable reaction atmosphere; And microwave horizontal pipe stove can meet this requirement, but cannot prevent solid-phase reactant from abnormal sintering phenomenon occurring by stirring material, this abnormal sintering causes material to sinter block into, has a strong impact on the carrying out of reaction, sinters simultaneously and also can damage thermocouple.The utility model improves on original microwave horizontal pipe furnace foundation, adds portable agitato, effectively solves while controlled atmospher because stirring the problem causing solid reactant to sinter; , fully contacted by reactant by stirring power meanwhile, add fast response and carry out, strengthening response intensity.
Summary of the invention
For above-mentioned prior art Problems existing and deficiency, the utility model provides one can stir microwave horizontal pipe atmosphere reactor.This reactor is by stirring the sintering phenomenon prevented in metallurgical solid phase reaction, and the utility model is achieved through the following technical solutions.
One can stir microwave horizontal pipe atmosphere reactor, this reactor comprises air inlet pipe 1, agitator 2, plug 3, thermocouple 4, crucible 5, inside holding body 6, woven wire 7, escape pipe 8, heat-preservation cotton 9, aluminium foil 10, screw 11, Quartz furnace door 12, quartz ampoule 13 and waveguide entrance 14, described quartz ampoule 13 both sides are provided with Quartz furnace door 12 by screw 11, Quartz furnace door 12 side is provided with air inlet pipe 1, opposite side is provided with escape pipe 8, the furnace chamber outer wall 15 of quartz ampoule 13 is provided with waveguide entrance 14, quartz ampoule 13 inside is provided with crucible 5, crucible 5 periphery parcel inside holding body 6, three-way pipe is provided with above crucible 5, middle pipe inserts agitator 2 by plug 3 from quartz ampoule 13 top, wherein an arm inserts thermocouple 4 by plug 3 from quartz ampoule 13 top, remaining pipe is air inlet pipe 1, the pipeline that quartz ampoule 13 is connected with Quartz furnace door 12 is wrapped in aluminium foil 10 from the inside to the outside, heat-preservation cotton 9 and woven wire 7.
This reactor described also comprises the stove hook 16 being provided with LED 17, and LED 17 makes conveniently to observe situation in quartz ampoule when charging and discharging.
This using method that can stir microwave horizontal pipe atmosphere reactor is: first material is placed in crucible 5, then crucible 5 is placed in quartz ampoule 13 by stove hook 16, then Quartz furnace door 12 is fixed on quartz ampoule 13 by screw 11, open waveguide and agitator 2, in air inlet pipe 1, pass into gas, material is reacted at desired temperatures.
The beneficial effects of the utility model are: the utility model solves in microwave metallurgical reaction, the problem causing solid reactant to sinter because stirring while controlled atmospher; , fully contacted by reactant by stirring power meanwhile, add fast response and carry out, strengthening response intensity; The utility model be applicable to all kinds of solid-solid phase, solid-liquid phase, vapor solid be gentle-liquid-solid phase metallurgical reaction system.
Accompanying drawing explanation
Fig. 1 is the utility model structural representation.
In figure: 1-air inlet pipe, 2-agitator, 3-plug, 4-thermocouple, 5-crucible, 6-inside holding body, 7-woven wire, 8-escape pipe, 9-heat-preservation cotton, 10-aluminium foil, 11-screw, 12-Quartz furnace door, 13-quartz ampoule, 14-waveguide entrance, 15-furnace chamber outer wall, 16-stove hook, 17-LED lamp.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the utility model is described in further detail.
Embodiment 1
This can stir microwave horizontal pipe atmosphere reactor, this reactor comprises air inlet pipe 1, agitator 2, plug 3, thermocouple 4, crucible 5, inside holding body 6, woven wire 7, escape pipe 8, heat-preservation cotton 9, aluminium foil 10, screw 11, Quartz furnace door 12, quartz ampoule 13 and waveguide entrance 14, described quartz ampoule 13 both sides are provided with Quartz furnace door 12 by screw 11, Quartz furnace door 12 side is provided with air inlet pipe 1, opposite side is provided with escape pipe 8, the furnace chamber outer wall 15 of quartz ampoule 13 is provided with waveguide entrance 14, quartz ampoule 13 inside is provided with crucible 5, crucible 5 periphery parcel inside holding body 6, three-way pipe is provided with above crucible 5, middle pipe inserts agitator 2 by plug 3 from quartz ampoule 13 top, wherein an arm inserts thermocouple 4 by plug 3 from quartz ampoule 13 top, remaining pipe is air inlet pipe 1, the pipeline that quartz ampoule 13 is connected with Quartz furnace door 12 is wrapped in aluminium foil 10 from the inside to the outside, heat-preservation cotton 9 and woven wire 7.
Wherein this reactor also comprises the stove hook 16 being provided with LED 17, and LED 17 makes conveniently to observe situation in quartz ampoule when charging and discharging.
Below by reference to the accompanying drawings detailed description of the invention of the present utility model is explained in detail, but the utility model is not limited to above-mentioned embodiment, in the ken that those of ordinary skill in the art possess, various change can also be made under the prerequisite not departing from the utility model aim.
Claims (2)
1. can stir a microwave horizontal pipe atmosphere reactor, it is characterized in that: this reactor comprises air inlet pipe (1), agitator (2), plug (3), thermocouple (4), crucible (5), inside holding body (6), woven wire (7), escape pipe (8), heat-preservation cotton (9), aluminium foil (10), screw (11), Quartz furnace door (12), quartz ampoule (13) and waveguide entrance (14), described quartz ampoule (13) both sides are provided with Quartz furnace door (12) by screw (11), Quartz furnace door (12) side is provided with air inlet pipe (1), opposite side is provided with escape pipe (8), the furnace chamber outer wall (15) of quartz ampoule (13) is provided with waveguide entrance (14), quartz ampoule (13) inside is provided with crucible (5), crucible (5) periphery parcel inside holding body (6), crucible (5) top is provided with three-way pipe, middle pipe inserts agitator (2) by plug (3) from quartz ampoule (13) top, wherein an arm inserts thermocouple (4) by plug (3) from quartz ampoule (13) top, remaining pipe is air inlet pipe (1), and the pipeline that quartz ampoule (13) is connected with Quartz furnace door (12) is wrapped in aluminium foil (10) from the inside to the outside, heat-preservation cotton (9) and woven wire (7).
2. according to claim 1ly stir microwave horizontal pipe atmosphere reactor, it is characterized in that: this reactor described also comprises the stove hook (16) being provided with LED (17).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520611926.4U CN204973885U (en) | 2015-08-14 | 2015-08-14 | Can stir horizontal tubular atmosphere reactor of microwave |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520611926.4U CN204973885U (en) | 2015-08-14 | 2015-08-14 | Can stir horizontal tubular atmosphere reactor of microwave |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204973885U true CN204973885U (en) | 2016-01-20 |
Family
ID=55108305
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520611926.4U Expired - Fee Related CN204973885U (en) | 2015-08-14 | 2015-08-14 | Can stir horizontal tubular atmosphere reactor of microwave |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204973885U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786658A (en) * | 2018-06-27 | 2018-11-13 | 安徽科幂机械科技有限公司 | A kind of high-temperature vacuum tubular type stove carrying out light-catalyzed reaction |
-
2015
- 2015-08-14 CN CN201520611926.4U patent/CN204973885U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786658A (en) * | 2018-06-27 | 2018-11-13 | 安徽科幂机械科技有限公司 | A kind of high-temperature vacuum tubular type stove carrying out light-catalyzed reaction |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160120 Termination date: 20170814 |