CN204918242U - Sulphuric acid waste liquid edulcoration recovery unit - Google Patents
Sulphuric acid waste liquid edulcoration recovery unit Download PDFInfo
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- CN204918242U CN204918242U CN201520627480.4U CN201520627480U CN204918242U CN 204918242 U CN204918242 U CN 204918242U CN 201520627480 U CN201520627480 U CN 201520627480U CN 204918242 U CN204918242 U CN 204918242U
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- waste liquid
- extraction tank
- pipeline
- tank
- liquid pool
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Abstract
The utility model discloses a sulphuric acid waste liquid edulcoration recovery unit, including waste liquid pool, extraction tank, spent acid basin, first sink, reation kettle, second sink, filter -tank and pressure filter, be equipped with the acid pump between waste liquid pool and the extraction tank, the acid pump both ends are passed through the pipeline and are connected waste liquid pool and extraction tank respectively, and the extraction tank passes through the pipeline and connects waste liquor storage tank and first sink respectively, and reation kettle is connected to first sink, and reation kettle passes through the pipeline and connects filter -tank and second sink respectively, and the pressure filter is connected to the filter -tank, and the second sink passes through the pipe connection extraction tank. The utility model discloses a sulphuric acid waste liquid edulcoration recovery unit carries out the edulcoration to the sulphuric acid waste liquid, and sulphuric acid waste liquid after the edulcoration has effectively reduced the heavy metal content in the polyferric sulfate product as polyferric sulfate's raw materials for production, the rare metal that simultaneously can recycle wherein contains, but extractant cyclic utilization moreover, the abundant saving of whole recovery unit's overall arrangement the time of technology, with low costs, easy operation, pollution -free.
Description
Technical field
The utility model relates to waste reclaiming device technical field, particularly relates to a kind of sulfuric acid waste removal of impurities retrieving arrangement.
Background technology
Current industrial enterprise can produce a large amount of sulfuric acid waste, if sulfuric acid waste directly discharges, not only can make water body and soil acidification, work the mischief to ecotope, and waste ample resources.Have at present by the raw materials for production of sulfuric acid waste as bodied ferric sulfate, but containing heavy metal in sulfuric acid waste, if be directly used as to produce bodied ferric sulfate, the quality of polyaluminum sulfate iron product can be affected, therefore sulfuric acid waste is before for the production of bodied ferric sulfate, needs to carry out removal of impurities.
Utility model content
The purpose of this utility model there is provided a kind of sulfuric acid waste removal of impurities retrieving arrangement, removal of impurities can be carried out to sulfuric acid waste, sulfuric acid waste after removal of impurities can be used as the raw materials for production of bodied ferric sulfate, effectively reduce the heavy metal content in polyaluminum sulfate iron product, bodied ferric sulfate quality product is made to reach high-quality, the rare metal wherein contained can be recycled simultaneously, there is certain economic benefit, and extraction agent reusable edible, the layout of whole retrieving arrangement has saved the time of technique fully, cost is low, easy to operate, pollution-free.
The technical solution adopted in the utility model is as follows:
A kind of sulfuric acid waste removal of impurities retrieving arrangement, comprise waste liquid pool, extraction tank, spent acid basin, first rinse bath, reactor, second rinse bath, filter vat and pressure filter, sour pump is provided with between described waste liquid pool and extraction tank, described sour pump two ends connect waste liquid pool and extraction tank respectively by pipeline, and the sulfuric acid waste supernatant liquor of precipitated form in waste liquid pool is evacuated to extraction tank extracts, described extraction tank connects waste liquor storage tank and the first rinse bath respectively by pipeline, described first rinse bath ligation still, reactor connects filter vat and the second rinse bath respectively by pipeline, described filter vat connects pressure filter, second rinse bath connects extraction tank by pipeline.
Pipeline between the second described rinse bath and extraction tank is provided with control valve.
Described waste liquid pool is divided into two-layer up and down with coarse filtration plate, upper strata is settling tank, and lower floor is filtering basin, and settling tank avris is provided with sewage draining valve.
The pipeline of the sour pump of described connection waste liquid pool extends filtering basin bottom.
When the utility model uses, the sulfuric acid waste in waste liquid pool staticly settles, and supernatant liquor enters extraction tank by sour pump and extracts, and the removal of impurities spent acid after extraction enters spent acid basin, can be used as the raw materials for production of bodied ferric sulfate; What obtain after extraction enters the first rinse bath containing rare metal organic phase, by entering reactor after sulfuric acid scrubbing, back extraction is carried out with alkali lye in reactor, obtain strip liquor and waste liquid, strip liquor enters filter vat filtration and obtains impurity filtrate, then obtain filter cake by pressure filter press filtration, filter cake is recycled; Waste liquid enters the second rinse bath, and through sulfuric acid scrubbing, the extraction agent obtaining regenerating can cycling and reutilization.
Compared with the prior art, the beneficial effects of the utility model are as follows:
Sulfuric acid waste removal of impurities retrieving arrangement of the present utility model, removal of impurities can be carried out to sulfuric acid waste, sulfuric acid waste after removal of impurities can be used as the raw materials for production of bodied ferric sulfate, effectively reduce the heavy metal content in polyaluminum sulfate iron product, bodied ferric sulfate quality product is made to reach high-quality, the rare metal wherein contained can be recycled simultaneously, there is certain economic benefit, and extraction agent reusable edible, the layout of whole retrieving arrangement has saved the time of technique fully, cost is low, easy to operate, does not produce pollution.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Embodiment
Below in conjunction with embodiment and accompanying drawing, the utility model will be further described.
See accompanying drawing 1, a kind of sulfuric acid waste removal of impurities retrieving arrangement, comprise waste liquid pool 1, extraction tank 2, spent acid basin 3, first rinse bath 4, reactor 5, second rinse bath 6, filter vat 7 and pressure filter 8, described waste liquid pool 1 is divided into two-layer up and down with coarse filtration plate 9, upper strata is settling tank 101, lower floor is filtering basin 102, settling tank 101 avris is provided with sewage draining valve 10, sour pump 11 is provided with between described waste liquid pool 1 and extraction tank 2, described sour pump 11 two ends connect waste liquid pool 1 and extraction tank 2 respectively by pipeline, the pipeline of the sour pump of described connection waste liquid pool 1 extends filtering basin 102 bottom, and the sulfuric acid waste supernatant liquor of precipitated form in waste liquid pool 1 is evacuated to extraction tank 2 extracts, described extraction tank 2 connects waste liquor storage tank 3 and the first rinse bath 4 respectively by pipeline, described first rinse bath 4 ligation still 5, reactor 5 connects filter vat 7 and the second rinse bath 6 respectively by pipeline, described filter vat 7 connects pressure filter 8, second rinse bath 6 connects extraction tank 2 by pipeline, pipeline between the second described rinse bath 6 and extraction tank 2 is provided with control valve 12.When the utility model uses, the sulfuric acid waste in waste liquid pool 1 staticly settles, and supernatant liquor enters extraction tank 2 by sour pump 11 and extracts, and the removal of impurities spent acid after extraction enters spent acid basin 3, can be used as the raw materials for production of bodied ferric sulfate; What obtain after extraction enters the first rinse bath 4 containing rare metal organic phase, by entering reactor 5 after sulfuric acid scrubbing, back extraction is carried out with alkali lye in reactor 5, obtain strip liquor and waste liquid, strip liquor enters filter vat 7 filtration and obtains impurity filtrate, then obtain filter cake by pressure filter 8 press filtration, filter cake is recycled; Waste liquid enters the second rinse bath 6, and through sulfuric acid scrubbing, the extraction agent obtaining regenerating can cycling and reutilization.Sulfuric acid waste removal of impurities retrieving arrangement of the present utility model, removal of impurities can be carried out to sulfuric acid waste, sulfuric acid waste after removal of impurities can be used as the raw materials for production of bodied ferric sulfate, effectively reduce the heavy metal content in polyaluminum sulfate iron product, bodied ferric sulfate quality product is made to reach high-quality, the rare metal wherein contained can be recycled simultaneously, there is certain economic benefit, and extraction agent reusable edible, the layout of whole retrieving arrangement has saved the time of technique fully, cost is low, easy to operate, does not produce pollution.
Claims (4)
1. a sulfuric acid waste removal of impurities retrieving arrangement, it is characterized in that: comprise waste liquid pool, extraction tank, spent acid basin, first rinse bath, reactor, second rinse bath, filter vat and pressure filter, sour pump is provided with between described waste liquid pool and extraction tank, described sour pump two ends connect waste liquid pool and extraction tank respectively by pipeline, and the sulfuric acid waste supernatant liquor of precipitated form in waste liquid pool is evacuated to extraction tank extracts, described extraction tank connects waste liquor storage tank and the first rinse bath respectively by pipeline, described first rinse bath ligation still, reactor connects filter vat and the second rinse bath respectively by pipeline, described filter vat connects pressure filter, second rinse bath connects extraction tank by pipeline.
2. sulfuric acid waste removal of impurities retrieving arrangement according to claim 1, is characterized in that: the pipeline between the second described rinse bath and extraction tank is provided with control valve.
3. sulfuric acid waste removal of impurities retrieving arrangement according to claim 1, it is characterized in that: described waste liquid pool is divided into two-layer up and down with coarse filtration plate, upper strata is settling tank, and lower floor is filtering basin, and settling tank avris is provided with sewage draining valve.
4. sulfuric acid waste removal of impurities retrieving arrangement according to claim 3, is characterized in that: the pipeline of the sour pump of described connection waste liquid pool extends filtering basin bottom.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520627480.4U CN204918242U (en) | 2015-08-18 | 2015-08-18 | Sulphuric acid waste liquid edulcoration recovery unit |
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CN201520627480.4U CN204918242U (en) | 2015-08-18 | 2015-08-18 | Sulphuric acid waste liquid edulcoration recovery unit |
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CN204918242U true CN204918242U (en) | 2015-12-30 |
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CN201520627480.4U Expired - Fee Related CN204918242U (en) | 2015-08-18 | 2015-08-18 | Sulphuric acid waste liquid edulcoration recovery unit |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105110502A (en) * | 2015-08-18 | 2015-12-02 | 铜陵海陵环保科技有限责任公司 | Apparatus for removing impurities from and recovering sulfuric acid waste liquid |
CN107539959A (en) * | 2017-08-25 | 2018-01-05 | 金川集团股份有限公司 | A kind of sulfuric acid waste reclaiming clean device |
CN109650347A (en) * | 2019-03-01 | 2019-04-19 | 肇庆学院 | A kind of Intelligent purifying recyclable device of sulfuric acid |
-
2015
- 2015-08-18 CN CN201520627480.4U patent/CN204918242U/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105110502A (en) * | 2015-08-18 | 2015-12-02 | 铜陵海陵环保科技有限责任公司 | Apparatus for removing impurities from and recovering sulfuric acid waste liquid |
CN107539959A (en) * | 2017-08-25 | 2018-01-05 | 金川集团股份有限公司 | A kind of sulfuric acid waste reclaiming clean device |
CN109650347A (en) * | 2019-03-01 | 2019-04-19 | 肇庆学院 | A kind of Intelligent purifying recyclable device of sulfuric acid |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151230 Termination date: 20170818 |
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CF01 | Termination of patent right due to non-payment of annual fee |