CN204911485U - Reaction kettle device of high -efficient fast speed adjusting accuse temperature - Google Patents
Reaction kettle device of high -efficient fast speed adjusting accuse temperature Download PDFInfo
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- CN204911485U CN204911485U CN201520511703.0U CN201520511703U CN204911485U CN 204911485 U CN204911485 U CN 204911485U CN 201520511703 U CN201520511703 U CN 201520511703U CN 204911485 U CN204911485 U CN 204911485U
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- coil pipe
- oil
- conduction oil
- tank body
- temperature
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Abstract
The utility model discloses a reaction kettle device of high -efficient fast speed adjusting accuse temperature, including the retort body, the internal circulating water cooling coil pipe that is equipped with the heat conduction oil coil pipe who has oil inlet and oil -out and has water inlet and delivery port of retort, heat conduction oil coil pipe's oil inlet is connected with hot oil sources of thermal conductance and cold heat conduction oil sources through hot oil valve of thermal conductance no. 1 and cold heat conduction oil valve no. 1 respectively, the water inlet of circulating water cooling coil pipe passes through inlet valve and is connected with the water source. The unusual is the new and effective binary of the internal portion's reaction temperature regulation and control system adoption of this jar is the temperature facility that goes up and down. The binary is that the facility includes conduction oil lift temperature circulation system and stainless steel disc pipe running water circulative cooling system. In addition, this reaction kettle system well just adjusts the convenience with production technological parameter's suitability. This reaction kettle system structural design is reasonable, and well -equipped flexible operation is convenient, and the fault rate is low, and it is convenient to maintain, long service life.
Description
Technical field
The utility model belongs to chemical technology field, is specifically related to a kind of reactor device for chemical products synthesis.
Background technology
Reactor is the equipment that chemical industry is commonly used, and generally comprises reacting tank body and the reflux condenser and the volatile gas collection device that are arranged on tank body top, and tank interior is provided with the agitating device that homogenizing material promotes chemosynthesis reaction.Needs are reacted in certain temperature range, circulating-heating is also set usually in tank body and surveys temperature regulating device.
At present, the regulating and controlling temperature device of chemical industry reactor used generally has following two class single mass system devices; Reactor heater and heat-conducting oil furnace are carried out pipeline and connect by the first, make to drop into material temperature reaction in tank body by Circulation and Hot Oil Spray; When phase needs to lower the temperature after the reaction, then high-temperature hot oil is pumped outside still, again import circulation cold oil and cooling regulation and control are carried out to sintetics, make it to reach manufacturing technique requirent, guarantee product quality.The one-time investment that this device exists the auxiliary device of regulating and controlling temperature and junction line is high, and supporting superfluous many, flexible operation degree is poor, and fault rate high maintenance is inconvenient.Secondly; due to the thermal conductivity factor of conduction oil lower (compared with water); the speed that cools is slow; therefore for the cooling of the chemical reaction between some high viscosity liquid material and solid material; usually there will be the reaction temperature delayed long period; What is more there will be temperature and rises on the contrary, will likely cause sintetics high-temperature oxydation, polymerization like this, thus affect product quality and yield rate.
Another kind of device is that the high-voltage high-temperature steam produced by steam boiler by pipeline imports in the heater of reactor, by the reaction mass of circulating-heating tank interior, when question response closes on terminal and needs fast cooling, then first close high-pressure and high-temperature steam entrance, imported by cooling water in reactor regulation device after pressure release, the temperature being reduced sintetics by SAPMAC method reaches manufacturing technique requirent index.The advantage of this device and application process is that cooling velocity is fast, can avoid the unexpected appearance affecting product quality.But the security performance of this apparatus system to auxiliary device and pipeline requires very high, and operating procedure is complicated, and device is safeguarded inconvenient.Therefore operating cost is too high, uneconomical.
Utility model content
For solving the problem, the utility model provides a kind of efficient regulating and controlling temperature reactor device device fast, this device can with lower cost and the efficient effect regulating and controlling synthesis reaction temperature fast, thus realize abolishing synthetic reaction chronic disease, improves the quality of products further and yield rate.
The technical solution adopted in the utility model is as follows:
A reactor device for efficient regulating and controlling temperature fast, comprises reacting tank body, is provided with the conduction oil coil pipe with oil-in and oil-out and the circulating water coil pipe with water inlet and delivery port in reacting tank body; The oil-in of conduction oil coil pipe is connected with thermal conductance deep fat source and cold heat conduction oil sources with cold conduction oil valve one respectively by thermal conductance deep fat valve one; The water inlet of circulating water coil pipe is connected with water source by inlet valve.
Described conduction oil coil pipe and circulating water coil pipe are arranged alternately in reacting tank body.
The utility model also comprises PLC cyclelog and is arranged on the temperature measurer in reacting tank body, and the signal output part of temperature measurer is connected with PLC cyclelog, and the signal output part of PLC cyclelog connects thermal conductance deep fat source.
The utility model reacting tank body top is provided with cycle condenser and volatile gas collection device.
Described volatile gas collection device and volatile gas collection utensil have a common cavity, cavity and reacting tank body UNICOM, cavity bottom is provided with condensate outlet, cavity has cooling water inlet and coolant outlet, is provided with the cooling coil be communicated with coolant outlet with cooling water inlet respectively in cavity.
Reactor heating-cooling device is connected with the reasonably optimizing such as heat-conducting oil furnace and water cooling tank by pipeline by the utility model by the PLC cyclelog system of described observing and controlling temperature, and monitoring runs, and realizes the Appropriate application of resource, the excellent heat superposition of equipment, upgrading.
The beneficial effects of the utility model have:
Facility structure is reasonable in design, well-equipped, has complementary advantages, flexible and convenient operation, and equipment adopts resistant material preparation, long service life.Full-automatic continuous control manipulation, failure rate is low is easy to maintenance.
This reactor apparatus system can realize safety and environmental protection formula and produce, and improves product synthesis quality and yield rate, enterprise technology economic benefit is significantly promoted.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
Below in conjunction with accompanying drawing, the utility model is further described:
As shown in Figure 1, the utility model mainly comprises the reacting tank body 1 with charging aperture 8, discharging opening 18 and agitating device 2, be provided with in reacting tank body 1 there is oil-in and oil-out conduction oil coil pipe 15(as required the utility model also can adopt interlayer heat-conducting oil heating mode) and there is the circulating water coil pipe 16 of water inlet 3 and delivery port 4; The oil-in 17 of conduction oil coil pipe 15 is connected with thermal conductance deep fat source and cold heat conduction oil sources with cold conduction oil valve 1 respectively by thermal conductance deep fat valve 1; The oil-out 18 of conduction oil coil pipe 15 to be connected with oil storage tank by valve 6 or to get back to thermal conductance deep fat source or cold heat conduction oil sources.The water inlet 3 of circulating water coil pipe 16 is connected with water source by inlet valve 13.
Described conduction oil coil pipe 15 and circulating water coil pipe 16 are arranged alternately in reacting tank body 1.
The utility model also comprises PLC cyclelog and is arranged on the temperature measurer 7 in reacting tank body, and the signal output part of temperature measurer 7 is connected with PLC cyclelog, and the signal output part of PLC cyclelog connects thermal conductance deep fat source.
The utility model reacting tank body 1 top is provided with cycle condenser and volatile gas collection device.
Described volatile gas collection device and volatile gas collection utensil have a common cavity 9, cavity 9 and reacting tank body 1 UNICOM, cavity bottom is provided with condensate outlet 12, cavity 9 has cooling water inlet 10 and coolant outlet 11, is provided with the cooling coil be communicated with coolant outlet with cooling water inlet respectively in cavity 9.
In the utility model, each pipeline connects PLC cyclelog, for the automatic operation of whole system.
When the utility model uses, first start imported valve 5 and the outlet valve 6 of agitating device 2 and conduction oil coil pipe 15, and survey temperature regulating device 7; Followed by charging aperture 8, add synthetic reaction material by first throwing the solid-state principle of liquid rear throwing; After material adds, add a cover closed charging aperture immediately, ON cycle condenser cold water terminal valve 10 and 11 carries out condensation cycle simultaneously.The liquid material of condensation is recycled through recovery tube 12.
After the synthesis reaction temperature of reaction mass reaches the high-temperature area of production technology setting, should in time by surveying the high-temperature temperature of temperature regulating device and heater appropriateness adjustment heat medium, thus the temperature of reaction mass is controlled in best production technology temperature range, and prevent because temperature of charge is delayed and bounce-back with this, cause material high-temperature oxydation, the generation of the negative reactions such as polymerization.
Through inspection by sampling, after judging that synthetic reaction completes substantially, the Inlet and outlet water valve opening the circulating water coil pipe 16 of material in reacting tank body immediately carries out Rapid Circulation cooling.
In order to accelerate material cooling velocity in tank, the various harmful negative reaction as far as possible avoiding high-temperature instantaneous to cause, while coil pipe water-cooled, again by temperature regulating device and PLC cyclelog, hot oil medium in conduction oil coil pipe 15 is pumped, and the cold conduction oil of importing carries out pipeline circulating cooling in time, until synthesis material reaches the temperature required by production technology.
After synthetic reaction completes, close all pipeloops and running gear immediately, open discharging opening valve, the sintetics qualified through test is carried out filling for subsequent use.
Above the embodiment of the warm reactor system of efficient regulation and control fast that the utility model provides is described in detail, specific case herein implements novel principle to this and embodiment is illustrated, and it just understands method of the present utility model and core concept for helping; Simultaneously for those skilled in the art, according to thought of the present utility model, all may change part in specific embodiments and applications.In sum, the content of the present embodiment should not be construed as restriction of the present utility model.
Claims (5)
1. a reactor device for efficient regulating and controlling temperature fast, comprises reacting tank body, it is characterized in that: be provided with the conduction oil coil pipe with oil-in and oil-out and the circulating water coil pipe with water inlet and delivery port in reacting tank body; The oil-in of conduction oil coil pipe is connected with thermal conductance deep fat source and cold heat conduction oil sources with cold conduction oil valve one respectively by thermal conductance deep fat valve one; The water inlet of circulating water coil pipe is connected with water source by inlet valve.
2. reactor device according to claim 1, is characterized in that: described conduction oil coil pipe and circulating water coil pipe are arranged alternately in reacting tank body.
3. reactor device according to claim 1 and 2, it is characterized in that: also comprise PLC cyclelog and be arranged on the temperature measurer in reacting tank body, the signal output part of temperature measurer is connected with PLC cyclelog, and the signal output part of PLC cyclelog connects thermal conductance deep fat source.
4. reactor device according to claim 1 and 2, is characterized in that: reacting tank body top is provided with cycle condenser and volatile gas collection device.
5. reactor device according to claim 4, it is characterized in that: described volatile gas collection device and volatile gas collection utensil have a common cavity, cavity and reacting tank body UNICOM, cavity bottom is provided with condensate outlet, cavity has cooling water inlet and coolant outlet, is provided with the cooling coil be communicated with coolant outlet with cooling water inlet respectively in cavity.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520511703.0U CN204911485U (en) | 2015-07-15 | 2015-07-15 | Reaction kettle device of high -efficient fast speed adjusting accuse temperature |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520511703.0U CN204911485U (en) | 2015-07-15 | 2015-07-15 | Reaction kettle device of high -efficient fast speed adjusting accuse temperature |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204911485U true CN204911485U (en) | 2015-12-30 |
Family
ID=54960671
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520511703.0U Expired - Fee Related CN204911485U (en) | 2015-07-15 | 2015-07-15 | Reaction kettle device of high -efficient fast speed adjusting accuse temperature |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204911485U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108525620A (en) * | 2018-04-24 | 2018-09-14 | 江苏省宜兴中等专业学校 | A kind of dual-heated reaction kettle |
-
2015
- 2015-07-15 CN CN201520511703.0U patent/CN204911485U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108525620A (en) * | 2018-04-24 | 2018-09-14 | 江苏省宜兴中等专业学校 | A kind of dual-heated reaction kettle |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151230 Termination date: 20170715 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |