CN204816546U - Hydrolysis reactor - Google Patents
Hydrolysis reactor Download PDFInfo
- Publication number
- CN204816546U CN204816546U CN201520486528.4U CN201520486528U CN204816546U CN 204816546 U CN204816546 U CN 204816546U CN 201520486528 U CN201520486528 U CN 201520486528U CN 204816546 U CN204816546 U CN 204816546U
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- CN
- China
- Prior art keywords
- reactive moieties
- mixing portion
- reaction
- hydrolysis
- heat exchanger
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006460 hydrolysis reaction Methods 0.000 title claims abstract description 35
- 230000007062 hydrolysis Effects 0.000 title claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 239000000498 cooling water Substances 0.000 claims abstract description 8
- 125000004122 cyclic group Chemical group 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 abstract description 11
- 239000002994 raw material Substances 0.000 description 9
- 230000005484 gravity Effects 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 206010024769 Local reaction Diseases 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model relates to a hydrolysis reactor, including mixing part, reaction subtotal heat transfer part, it is provided with three feed inlet to mix the part, the feed inlet all is provided with the injector head on the inside wall that mixes the part, the reaction part adopts tubular reactor, the reaction part is provided with the water inlet, the water inlet is provided with the injector head on the inside wall of reaction part, the heat transfer part adopts tubular heat exchanger, it connects to mix the part the reaction part mix the subtotal the junction of reaction part is provided with liquid distributor, tubular heat exchanger's tube side is hydrolysis reactor's reaction part, tubular heat exchanger's shell side leads to the cooling water. The utility model discloses with hydrolysis reaction control at within range less relatively to can control the hydrolysis reaction temperature effectively at less within range, make hydrolysis reaction steadily go on, guarantee the controllability of hydrolysis reaction condition and higher security.
Description
Technical field
The utility model relates to a kind of reactor, especially relates to a kind of hydrolysis reactor.
Background technology
Traditional reactor is generally closed reactor, in this closed reactor, add reaction raw materials, stirs and keeps certain temperature and pressure.Application traditional reactor is in the shortcoming of hydrolysis, exist in traditional reactor and stir dead angle, thus make the local concentration of reactant too high, thus cause the runaway reaction in whole reactor, reaction can not be reacted under controlled conditions, thus cause product impure, more seriously even cause the temperature of hydrolysis control out of control and produce dangerous.
Summary of the invention
For this reason, the utility model provides a kind of hydrolysis reactor, and object is, stir uneven, thus the local reaction substrate concentration produced is too high, and the reaction produced is violent, and the local temperature brought crosses the problems such as high in the traditional reactor of solution hydrolysis.
The technical solution adopted in the utility model is:
A kind of hydrolysis reactor, comprise mixing portion, reactive moieties and heat exchanging part, described mixing portion is provided with three charging apertures, described charging aperture is provided with injector head on the madial wall of mixing portion, described reactive moieties adopts tubular reactor, described reactive moieties is provided with water inlet, described water inlet is provided with injector head on the madial wall of reactive moieties, described heat exchanging part adopts pipe heat exchanger, described mixing portion connects described reactive moieties, the junction of described mixing portion and described reactive moieties is provided with liquid distributor, the tube side of described pipe heat exchanger is the reactive moieties of hydrolysis reactor, the shell side of described pipe heat exchanger leads to cooling water.
Further, can also comprise storage compartment and cyclic part, described storage compartment adopts accumulator tank, and described cyclic part adopts circulating pump and circulation pipe; The tube side of described pipe heat exchanger is connected with the entrance of described accumulator tank, the outlet of described accumulator tank is connected with one end of the circulation pipe of cyclic part, the other end of described circulation pipe connects the charging aperture of described mixing portion, is provided with circulating pump in the middle of described circulation pipe.
Further, the circulation pipe between circulating pump and recycle stock charging aperture is provided with discharge valve.
Further, the charging aperture be connected with described circulation pipe is arranged on the top of described mixing portion.
Concrete technological process is: first, by water through transport pump to water inlet, then reactive moieties is spurted into through the injector head be arranged on water inlet, then raw material is delivered to charging aperture through dehvery pump, mixing portion is injected into through the injector head be arranged on charging aperture, the liquid distributor of raw material under gravity through being arranged on reactive moieties entrance flows into reactive moieties, and at reactive moieties and water generation hydrolysis, then accumulator tank is entered, after under the effect of circulating pump, the product in accumulator tank is delivered to the charging aperture be arranged on bottom mixing portion, recycle stock spurts into mixing portion through the injector head be arranged on charging aperture, recycle stock fully mixes at mixing portion with raw material, then the liquid distributor under gravity through being arranged on reactive moieties entrance flows into reactive moieties, and at reactive moieties and water generation hydrolysis, then accumulator tank is entered, according to described regular cycles.Circulation pipe between circulating pump and recycle stock charging aperture is provided with discharge valve, can judges whether to reach quantity-produced requirement by the concentration detecting product in discharge valve place recycle stock, thus judge whether to open discharge valve.
Hydrolysis controls in relatively little scope by the utility model, hydrolysis in less space makes the control of condition relatively easy, the injector head being arranged on charging aperture and water inlet makes raw material, recycle stock and water fully to mix, the exchange heat that hydrolysis produces can promptly be walked by the pipe heat exchanger of heat exchanging part, thus can in more among a small circle controlled hydrolysis reaction temperature effectively, hydrolysis is steadily carried out, ensures the controllability of hydrolysis condition and higher security.
Accompanying drawing explanation
Fig. 1 is the overall schematic of hydrolysis reactor of the present utility model;
Fig. 2 is the schematic diagram of the mixing portion of hydrolysis reactor of the present utility model, reactive moieties and heat exchanging part;
In figure: 1 hydrolysis reactor; 2 accumulator tanks; 3 circulating pumps; 4 discharge valves; 5 raw materials; 6 water; 7 entrance cooling waters; 8 outlet cooling waters; 9 recycle stocks; 10 mixing portions; 11 reactive moieties; 12 recycle stock charging apertures; 13 material inlets; 14 water inlets; 15 cooling water outlets; 16 cooling water intakes; 17 injector heads; 18 liquid distributors.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the utility model is described in detail.
A kind of hydrolysis reactor, comprise mixing portion 10, reactive moieties 11 and heat exchanging part, described mixing portion 10 is provided with three charging apertures, be respectively two material inlets 13 and a recycle stock charging aperture 12, described charging aperture is provided with injector head 17 on the madial wall of mixing portion 10, described reactive moieties 11 adopts tubular reactor, described reactive moieties 11 is provided with water inlet 14, described water inlet 14 is provided with injector head 17 on the madial wall of reactive moieties 11, described heat exchanging part adopts pipe heat exchanger, described mixing portion 10 connects described reactive moieties 11, the junction of described mixing portion 10 and described reactive moieties 11 is provided with liquid distributor 18, the tube side of described pipe heat exchanger is the reactive moieties 11 of hydrolysis reactor, the shell side of described pipe heat exchanger leads to cooling water.
Further, can also comprise storage compartment and cyclic part, described storage compartment adopts accumulator tank 2, and described cyclic part adopts circulating pump 3 and circulation pipe; The tube side of described pipe heat exchanger is connected with the entrance of described accumulator tank 2, the described outlet of accumulator tank 2 is connected with one end of the circulation pipe of cyclic part, the other end of described circulation pipe connects the recycle stock charging aperture 12 of described mixing portion, is provided with circulating pump 3 in the middle of described circulation pipe.
Further, the circulation pipe between circulating pump 3 and recycle stock charging aperture 12 is provided with discharge valve 4.
Further, the recycle stock charging aperture 12 be connected with described circulation pipe is arranged on the top of described mixing portion 10.
Concrete technological process is: first, by water through transport pump to water inlet, then reactive moieties is spurted into through the injector head be arranged on water inlet, then raw material is delivered to charging aperture through dehvery pump, mixing portion is injected into through the injector head be arranged on charging aperture, the liquid distributor of raw material under gravity through being arranged on reactive moieties entrance flows into reactive moieties, and at reactive moieties and water generation hydrolysis, then accumulator tank is entered, after under the effect of circulating pump, the product in accumulator tank is delivered to the charging aperture be arranged on bottom mixing portion, recycle stock spurts into mixing portion through the injector head be arranged on charging aperture, recycle stock fully mixes at mixing portion with raw material, then the liquid distributor under gravity through being arranged on reactive moieties entrance flows into reactive moieties, and at reactive moieties and water generation hydrolysis, then accumulator tank is entered, according to described regular cycles.Circulation pipe between circulating pump and recycle stock charging aperture is provided with discharge valve, can judges whether to reach quantity-produced requirement by the concentration detecting product in discharge valve place recycle stock, thus judge whether to open discharge valve.
Above-mentioned detailed description of the invention is used for explaining and the utility model is described; be only preferred embodiment of the present utility model; instead of the utility model is limited; in the protection domain of spirit of the present utility model and claim; the any amendment made the utility model, equivalent replacement, improvement etc., all fall into protection domain of the present utility model.
Claims (4)
1. a hydrolysis reactor, it is characterized in that, comprise mixing portion, reactive moieties and heat exchanging part, described mixing portion is provided with three charging apertures, described charging aperture is provided with injector head on the madial wall of mixing portion, described reactive moieties adopts tubular reactor, described reactive moieties is provided with water inlet, described water inlet is provided with injector head on the madial wall of reactive moieties, described heat exchanging part adopts pipe heat exchanger, described mixing portion connects described reactive moieties, the junction of described mixing portion and described reactive moieties is provided with liquid distributor, the tube side of described pipe heat exchanger is the reactive moieties of hydrolysis reactor, the shell side of described pipe heat exchanger leads to cooling water.
2. a kind of hydrolysis reactor according to claim 1, is characterized in that, further, also comprises storage compartment and cyclic part, and described storage compartment adopts accumulator tank, and described cyclic part adopts circulating pump and circulation pipe; The tube side of described pipe heat exchanger is connected with the entrance of described accumulator tank, the outlet of described accumulator tank is connected with one end of the circulation pipe of cyclic part, the other end of described circulation pipe connects the charging aperture of described mixing portion, is provided with circulating pump in the middle of described circulation pipe.
3. a kind of hydrolysis reactor according to claim 2, is characterized in that, the circulation pipe between circulating pump and recycle stock charging aperture is provided with discharge valve.
4. a kind of hydrolysis reactor according to claim 2, is characterized in that, the charging aperture be connected with described circulation pipe is arranged on the top of described mixing portion.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520486528.4U CN204816546U (en) | 2015-07-03 | 2015-07-03 | Hydrolysis reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520486528.4U CN204816546U (en) | 2015-07-03 | 2015-07-03 | Hydrolysis reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204816546U true CN204816546U (en) | 2015-12-02 |
Family
ID=54674189
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520486528.4U Expired - Fee Related CN204816546U (en) | 2015-07-03 | 2015-07-03 | Hydrolysis reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204816546U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106045861A (en) * | 2016-05-26 | 2016-10-26 | 山东润博生物科技有限公司 | Method and system for continuously producing 5-fluoro-2-nitrophenol |
| CN106492731A (en) * | 2016-12-23 | 2017-03-15 | 马鞍山科英合成材料有限公司 | A kind of production equipment for preparing blocked isocyanate |
-
2015
- 2015-07-03 CN CN201520486528.4U patent/CN204816546U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106045861A (en) * | 2016-05-26 | 2016-10-26 | 山东润博生物科技有限公司 | Method and system for continuously producing 5-fluoro-2-nitrophenol |
| CN106045861B (en) * | 2016-05-26 | 2019-04-19 | 山东润博生物科技有限公司 | A kind of method and its system of the fluoro- 2- nitrophenol of continuous production 5- |
| CN106492731A (en) * | 2016-12-23 | 2017-03-15 | 马鞍山科英合成材料有限公司 | A kind of production equipment for preparing blocked isocyanate |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151202 |