CN201704219U - Concrete admixture production device - Google Patents
Concrete admixture production device Download PDFInfo
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- CN201704219U CN201704219U CN2010201629427U CN201020162942U CN201704219U CN 201704219 U CN201704219 U CN 201704219U CN 2010201629427 U CN2010201629427 U CN 2010201629427U CN 201020162942 U CN201020162942 U CN 201020162942U CN 201704219 U CN201704219 U CN 201704219U
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Abstract
The utility model discloses a concrete admixture production device comprising a melting kettle, a sulfonating kettle, a hydrolyzing kettle, a condensation kettle and a neutralizing kettle which are sequentially connected through material pipelines; heating mechanisms are arranged in the kettle bodies of the melting kettle, the sulfonating kettle, the hydrolyzing kettle and the condensation kettle; heating outer covers are arranged outside the kettle bodies of the melting kettle, the sulfonating kettle, the hydrolyzing kettle and the condensation kettle; a heat transfer media is arranged in the heating outer covers; and the heating outer covers outside the kettles are serially connected through heat transfer media pipes to form circulation. The device can precisely control the reaction conditions of all reaction processes, so that sulphonation reaction, hydrolysis reaction, condensation reaction and neutralization reaction are quickly and fully carried out, thereby ensuring the product quality. Meanwhile, all the reaction kettles have good heat insulation effect and high heat utilization rate, and reduce energy consumption as possible.
Description
Technical field
The utility model belongs to the concrete admixture field, is specifically related to a kind of production unit of concrete admixture.
Background technology
Naphthalene water reducer is a kind of concrete admixture of present domestic large usage quantity, and it is main raw material with the NAPTHALENE FLAKES. (INDUSTRIAL GRADE, forms through fusing naphthalene, sulfonation reaction, hydrolysis reaction, condensation reaction, neutralization reaction.
Two kinds of technologies of the general branch of the production of existing naphthalene water reducer, a kind of is that fusing naphthalene, sulfonation reaction, hydrolysis reaction, condensation reaction, neutralization reaction are all finished in same reactor successively, advantage is a saving equipment, shortcoming comprises: because temperature required and other condition differences of each operation, need reactor is cooled off temperature adjustment repeatedly, expense energy consuming time and quality product are difficult to control, and reactor need be selected valency height and the more weak enamel reactor of tolerance for use, production cycle is long, the processing requirement complexity.Another kind of technology is that each reaction is all carried out in different reactors, and its advantage is that each reaction conditions is controlled respectively, but continuous production and cycle are short, respectively goes on foot the problem that temperature of reaction control is difficult, power consumption is big but still exist.
Summary of the invention
The purpose of this utility model is on the basis of adopting a plurality of reactors, and a kind of new concrete admixture production equipment is provided, and in the hope of when accurately controlling the temperature of each reactor, reduces energy consumption, reduces production costs.
The purpose of this utility model can reach by following measure:
A kind of concrete admixture production equipment, comprise the melting kettle that connects successively by material pipe, sulfonation still, hydrolysis kettle, condensation still and in and still; In the kettle of described melting kettle, sulfonation still, hydrolysis kettle and condensation still, be equipped with heating arrangements, outside the kettle of described melting kettle, sulfonation still, hydrolysis kettle and condensation still, be equipped with and add hot jacket, described adding, be equipped with heat-conducting medium in the hot jacket, each still is outer adds hot jacket and be in series by the heat-conducting medium conduit and form circulation.
Melting kettle makes it to enter the sulfonation still and react, so the outlet of melting kettle communicates by the material pipeline with the inlet of sulfonation still in order to the naphthalene fusing.The material that sulfonation still internal reaction is finished feeds the reaction that is hydrolyzed in the hydrolysis kettle again by pipeline, reacted material feeds in the condensation still by the material pipeline again in the hydrolysis kettle, during the material that condensation reaction generates feeds by pipeline again and in the still, neutralization reaction finishes the back tests to product, can pack or put in storage after qualified.
Wherein for ease of the temperature control of each reaction, be equipped with heating arrangements in the kettle of melting kettle, sulfonation still, hydrolysis kettle and condensation still, this heating arrangements can adopt electric heating device or heat exchanger tube.Also can be provided with temperature-control device in each still, thereby reaction is heated and accurately controlled.
Outside the kettle of melting kettle, sulfonation still, hydrolysis kettle and condensation still, be equipped with and add hot jacket, not only can give the reactor even heating, can also be with unnecessary heat by heat transfer medium flows adding in the hot jacket to other reactors.The hot jacket that adds outside each still is in series by the heat-conducting medium conduit and forms under the round-robin situation, more can make heat fully mobile at each still place.Can also the heat-conducting medium pump be set at heat-conducting medium conduit place, circulate power to provide.
A kind of approach that preferably circulates of heat-conducting medium is as follows: melting kettle adds hot jacket and adds hot jacket by the heat-conducting medium conduit with the sulfonation still and communicate, the sulfonation still adds hot jacket and adds hot jacket by heat-conducting medium conduit and hydrolysis kettle and communicate, hydrolysis kettle adds hot jacket and adds hot jacket by the heat-conducting medium conduit with the condensation still and communicate, and the condensation still adds hot jacket and adds hot jacket with melting kettle again by the heat-conducting medium conduit and communicate; Thereby medium flows by adding the circulation passage internal recycle that hot jacket and heat-conducting medium conduit constitute at this, reaches the purpose that cuts down the consumption of energy as far as possible.
Also be provided with the sulfuric acid inlet on the sulfonation still, this sulfuric acid inlet links to each other with sulfuric acid volume pump or sour scale tank, in order to add the required sulfuric acid of sulfonation.
Hydrolysis kettle is provided with the hydrolysis water inlet, and this hydrolysis water inlet links to each other with hydrolysis water volume pump or water tank.
The condensation still is provided with the formaldehyde inlet, and this formaldehyde inlet links to each other with formaldehyde volume pump or formaldehyde storage tank.
In and still be provided with liquid caustic soda inlet, this liquid caustic soda inlet links to each other with the liquid caustic soda volume pump, in order to adding neutralization reaction desired raw material.
The beneficial effects of the utility model:
Device of the present utility model can accurately be controlled the reaction conditions of each reaction, makes the very fast and reaction fully of sulfonation reaction, hydrolysis reaction, condensation reaction and neutralization reaction, has thickly guaranteed quality product.Each reactor good heat insulation of while, the heat utilization efficiency height has reduced energy consumption as much as possible.
Description of drawings
Fig. 1 is a structural representation of the present utility model.
Among 1-melting kettle, 2-sulfonation still, 3-hydrolysis kettle, 4-condensation still, the 5-and still, 6-heating arrangements, 7-add hot jacket, 8-heat-conducting medium conduit, 9-material pipeline, 10-heat-conducting medium.
Embodiment
Device of the present invention as shown in Figure 1, comprise melting kettle 1, sulfonation still 2, hydrolysis kettle 3, condensation still 4 and in and still 5.The outlet of melting kettle 1 communicates by material pipeline 9 with the inlet of sulfonation still 2, the outlet of sulfonation still 1 feeds in the hydrolysis kettle 3 by pipeline 9 again, the outlet of hydrolysis kettle 3 feeds in the condensation still 4 by material pipeline 9 again, during the material outlet of condensation still 4 feeds by pipeline 9 again and in the still 5, in and the neutralization reaction in the still 5 finish the back check and put in storage.
In the kettle of melting kettle 1, sulfonation still 2, hydrolysis kettle 3 and condensation still 4, be equipped with heating arrangements 6, outside the kettle of melting kettle 1, sulfonation still 2, hydrolysis kettle 3 and condensation still 4, be equipped with and add hot jacket 7, add heat-conducting medium 10 is housed in the hot jacket 7.
The hot jacket 7 that adds of melting kettle 1 communicates with the hot jacket 7 that adds of sulfonation still 2 by heat-conducting medium conduit 8, the hot jacket 7 that adds of sulfonation still 2 communicates with the hot jacket 7 that adds of hydrolysis kettle 3 by heat-conducting medium conduit 8, the hot jacket 7 that adds of hydrolysis kettle 3 communicates with the hot jacket 7 that adds of condensation still 4 by heat-conducting medium conduit 8, and the hot jacket 7 that adds of condensation still 4 communicates with the hot jacket 7 that adds of melting kettle 1 again by heat-conducting medium conduit 8; Thereby medium 10 flows by adding the circulation passage internal recycle that hot jacket 7 and heat-conducting medium conduit 8 constitute at this, reaches the purpose that cuts down the consumption of energy as far as possible.
Also be provided with the sulfuric acid inlet on the sulfonation still, this sulfuric acid inlet links to each other with sulfuric acid volume pump or sour scale tank; Hydrolysis kettle is provided with the hydrolysis water inlet, and this hydrolysis water inlet links to each other with hydrolysis water volume pump or water tank.The condensation still is provided with the formaldehyde inlet, and this formaldehyde inlet links to each other with formaldehyde volume pump or formaldehyde storage tank.In and still be provided with liquid caustic soda inlet, this liquid caustic soda inlet links to each other with the liquid caustic soda volume pump.
NAPTHALENE FLAKES. (INDUSTRIAL GRADE fusion in melting kettle 1 earlier, feed then in the sulfonation still 2, add sulfuric acid by the sulfuric acid volume pump, carry out sulfonation reaction, after the reaction material is fed in the hydrolysis kettle 3, add the entry reaction that is hydrolyzed by the hydrolysis water volume pump, after the reaction material is fed in the condensation still 4, carry out condensation reaction after adding formaldehyde by the formaldehyde volume pump again, in feeding again after the reaction and in the still 5, add liquid caustic soda by the liquid caustic soda volume pump and carry out neutralization reaction, each temperature of reaction is by heating arrangements in each reactor and temperature controlling system control.Product after the neutralization reaction is through packing after the assay was approved and putting in storage.
Heat-conducting medium 10 flows at the passage internal recycle that hot jacket 7 and heat-conducting medium conduit 8 form that adds by each reactor, to keep each temperature of reaction kettle.
Claims (7)
1. concrete admixture production equipment, comprise the melting kettle (1) that connects successively by material pipe, sulfonation still (2), hydrolysis kettle (3), condensation still (4) and in and still (5); It is characterized in that: in the kettle of described melting kettle (1), sulfonation still (2), hydrolysis kettle (3) and condensation still (4), be equipped with heating arrangements (6), outside the kettle of described melting kettle (1), sulfonation still (2), hydrolysis kettle (3) and condensation still (4), be equipped with and add hot jacket (7), described adding, be equipped with heat-conducting medium (10) in the hot jacket (7), each still is outer adds hot jacket (7) and be in series by heat-conducting medium conduit (8) and form circulation.
2. concrete admixture production equipment according to claim 1, it is characterized in that melting kettle adds hot jacket and adds hot jacket by the heat-conducting medium conduit with the sulfonation still and communicate, the sulfonation still adds hot jacket and adds hot jacket by heat-conducting medium conduit and hydrolysis kettle and communicate, hydrolysis kettle adds hot jacket and adds hot jacket by the heat-conducting medium conduit with the condensation still and communicate, and the condensation still adds hot jacket and adds hot jacket with melting kettle again by the heat-conducting medium conduit and communicate.
3. concrete admixture production equipment according to claim 1 is characterized in that described heating arrangements (6) adopts electric heating device or heat exchanger tube.
4. concrete admixture production equipment according to claim 1 is characterized in that described sulfonation still (2) is provided with the sulfuric acid inlet, and this sulfuric acid inlet links to each other with the sulfuric acid volume pump.
5. concrete admixture production equipment according to claim 1 is characterized in that described hydrolysis kettle (3) is provided with the hydrolysis water inlet, and this hydrolysis water inlet links to each other with the hydrolysis water volume pump.
6. concrete admixture production equipment according to claim 1 is characterized in that described condensation still (4) is provided with the formaldehyde inlet, and this formaldehyde inlet links to each other with the formaldehyde volume pump.
7. concrete admixture production equipment according to claim 1, it is characterized in that described in and still (5) be provided with liquid caustic soda inlet, this liquid caustic soda inlet links to each other with the liquid caustic soda volume pump.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2010201629427U CN201704219U (en) | 2010-04-19 | 2010-04-19 | Concrete admixture production device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN2010201629427U CN201704219U (en) | 2010-04-19 | 2010-04-19 | Concrete admixture production device |
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CN201704219U true CN201704219U (en) | 2011-01-12 |
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CN2010201629427U Expired - Fee Related CN201704219U (en) | 2010-04-19 | 2010-04-19 | Concrete admixture production device |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105417984A (en) * | 2015-12-17 | 2016-03-23 | 重庆天珠科技有限公司 | Naphthalene product production system |
CN105536665A (en) * | 2015-12-17 | 2016-05-04 | 重庆天珠科技有限公司 | Naphthalene product production system |
CN113087867A (en) * | 2021-04-12 | 2021-07-09 | 罗小泉 | Water reducing agent and preparation method thereof |
-
2010
- 2010-04-19 CN CN2010201629427U patent/CN201704219U/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105417984A (en) * | 2015-12-17 | 2016-03-23 | 重庆天珠科技有限公司 | Naphthalene product production system |
CN105536665A (en) * | 2015-12-17 | 2016-05-04 | 重庆天珠科技有限公司 | Naphthalene product production system |
CN113087867A (en) * | 2021-04-12 | 2021-07-09 | 罗小泉 | Water reducing agent and preparation method thereof |
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Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110112 Termination date: 20130419 |