CN204746321U - A automatic reation kettle device for producing graphite alkene - Google Patents
A automatic reation kettle device for producing graphite alkene Download PDFInfo
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- CN204746321U CN204746321U CN201520481008.4U CN201520481008U CN204746321U CN 204746321 U CN204746321 U CN 204746321U CN 201520481008 U CN201520481008 U CN 201520481008U CN 204746321 U CN204746321 U CN 204746321U
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Abstract
The utility model belongs to the technical field of the chemical equipment manufacture, concretely relates to an automatic reation kettle device for producing graphite alkene, reation kettle's outer wall is provided with circulating water channel, reation kettle's outside is provided with three feeding valve, reation kettle's top is provided with the agitator, reation kettle's the upper right side is provided with the temperature controller who has temperature transmitter, reation kettle's right side outside is provided with the liquid level derailleur, reation kettle's outside right side below is provided with the low -temperature constant -temperature water bath, the right side below of low -temperature constant -temperature water bath is provided with the discharging pump, control cabinet and reation kettle independent setting, each part is joined in marriage and is constituted an automatic reation kettle device for producing graphite alkene, the automation mechanized operation of adopting control cabinet controlled reaction cauldron to realize replaces manual operation, the efficiency of the preparation of graphite alkene is improved, preventing human body health injury. Its structural design is reasonable, the principle science, and safe and reliable uses portably, energy -concerving and environment -protective, with low costs, efficient.
Description
Technical field:
The utility model belongs to chemical industry equipment manufacturing technology field, is specifically related to a kind of automation reactor device for the production of Graphene, to improve the efficiency of Graphene manufacture.
Background technology:
Graphene came out in 2004, it is a kind of Two-dimensional Carbon material, it is the general designation of single-layer graphene, bilayer graphene and multi-layer graphene, Graphene with independent carbon atom for base, using the gesture of carbon atom generation around as perturbation, the energy level distribution of Graphene can be calculated by the method for matrix, launch near dirac point, energy can be obtained and wave vector linear (being similar to the dispersion relation of photon), and there is singular point at dirac point, this means near Fermi surface, in Graphene, the effective mass of electronics is zero; Graphene is thin, the hardest nano material in known world, be almost completely transparent, only absorb the light of 2.3%, thermal conductivity factor is up to 5300W/mK, higher than CNT and diamond, under normal temperature, electron mobility is more than 15000cm2/Vs, than CNT or silicon wafer height, and resistivity about 1 Ω m, than copper and silver low, for the material that resistivity is minimum, Graphene is used for electronic component of new generation or transistor, also for the manufacture of transparent touch screen, tabula rasa or even solar cell.
China also has unique advantage in the research of Graphene, from production angle, as the graphite of Graphene raw materials for production, enriches in China's energy storage, cheap; In addition, it is hinder the extensive commercial main factor of Graphene that mass production and large scale are produced, and the up-to-date achievement in research of China successfully breaks through this two hang-up, manufacturing cost is down to 3 yuan/gram from 5000 yuan/gram, solve a volume production difficult problem for this material, utilize chemical vapour deposition technique successfully to produce the single-layer graphene of domestic first sheet 15 inches, and successfully graphene transparent electrode is applied on electric resistance touch screen, prepare 7 inches of Graphene touch-screens; Along with the progressively breakthrough of the difficult problem such as mass production and large scale, the commercial application paces of Graphene are accelerated, and current Graphene manufacture is based on manual operation, and efficiency is low, and has very large harmfulness to health.Therefore, research and develop a kind of automation reactor device for the production of Graphene, control reactor with console and realize automation mechanized operation, improve Graphene production efficiency, avoid being detrimental to health, have very much social value and application prospect.
Summary of the invention:
The purpose of this utility model is the shortcoming overcoming prior art existence, seeks to design a kind of automation reactor device for the production of Graphene, controls reactor and realizes automation mechanized operation, improve Graphene production efficiency, avoid being detrimental to health with console.
To achieve these goals, agent structure of the present utility model comprises material inlet valve, console, agitator, temperature controller, temperature transmitter, liquid level speed changer, cryogenic thermostat water bath, discharging pump, circulating water chennel, reactor, cooling water pipeline, discharge pipe and feed pipe, the outer wall of the reactor of U-shaped structure is provided with circulating water chennel, three material inlet valves are provided with above the external left of reactor, material inlet valve enters reactor by feed pipe, the top of reactor is provided with agitator, the upper right side of reactor is provided with the temperature controller with temperature transmitter, the right hand external of reactor is provided with the liquid level speed changer be connected with reactor, cryogenic thermostat water bath is provided with below the external right of reactor, cryogenic thermostat water bath is connected with circulating water chennel by cooling water pipeline, the lower right of cryogenic thermostat water bath is provided with discharging pump, discharging pump enters the bottom of reactor through circulating water chennel by discharge pipe, console and reactor are independently arranged, equal telecommunications manner of breathing connects between console and material inlet valve, between console and agitator, between console and temperature controller, between console and liquid level speed changer, between console and cryogenic thermostat water bath, between console and discharging pump and between temperature controller and cryogenic thermostat water bath, and each parts are joined and are configured for producing the automation reactor device of Graphene.
Compared with prior art, the automation mechanized operation controlling reactor realization with console replaces manual operation to the utility model, improves the preparation efficiency of Graphene, avoids being detrimental to health, its reasonable in design, scientific in principle, safe and reliable, easy to use, energy-conserving and environment-protective, cost is low, and efficiency is high.
Accompanying drawing illustrates:
Fig. 1 is agent structure principle schematic of the present utility model.
Detailed description of the invention:
Also by reference to the accompanying drawings the utility model is described further below by embodiment.
Embodiment:
The agent structure of the automation reactor device for the production of Graphene that the present embodiment relates to comprises material inlet valve 1, console 2, agitator 3, temperature controller 4, temperature transmitter 5, liquid level speed changer 6, cryogenic thermostat water bath 7, discharging pump 8, circulating water chennel 9, reactor 10, cooling water pipeline 11, discharge pipe 12 and feed pipe 13, the outer wall of the reactor 10 of U-shaped structure is provided with circulating water chennel 9, three material inlet valves 1 are provided with above the external left of reactor 10, material inlet valve 1 enters reactor 10 by feed pipe 13, the top of reactor 10 is provided with agitator 3, the upper right side of reactor 10 is provided with the temperature controller 4 with temperature transmitter 5, the right hand external of reactor 10 is provided with the liquid level speed changer 6 be connected with reactor 10, cryogenic thermostat water bath 7 is provided with below the external right of reactor 10, cryogenic thermostat water bath 7 is connected with circulating water chennel 9 by cooling water pipeline 11, the lower right of cryogenic thermostat water bath 7 is provided with discharging pump 8, discharging pump 8 enters the bottom of reactor 10 through circulating water chennel 9 by discharge pipe 12, console 2 is arranged with reactor 10 is independent, equal telecommunications manner of breathing connects between console 2 and material inlet valve 1, between console 2 and agitator 3, between console 2 and temperature controller 4, between console 2 and liquid level speed changer 6, between console 2 and cryogenic thermostat water bath 7, between console 2 and discharging pump 8 and between temperature controller 4 and cryogenic thermostat water bath 7, and each parts are joined and are configured for producing the automation reactor device of Graphene.
When the automation reactor device for the production of Graphene that the present embodiment relates to uses, the parameter of three material inlet valves 1 is set respectively in console 2, console 2 controls material inlet valve 1 respectively according to setup parameter, make each feed pipe 13 charging, the liquid level registration recorded is passed to console 2 by liquid level speed changer 6 in real time, console 2 controls material inlet valve 1 according to registration size, in the process of charging, for ensureing that the temperature of reactor 10 is at 0-5 DEG C, the temperature data recorded is passed to console 2 by temperature transmitter 5 and temperature controller 4 in real time, console 2 controls the temperature of cryogenic thermostat water bath 7 according to the temperature data information received, the information that cryogenic thermostat water bath 7 transmits according to console 2 controls the temperature of reactor 10 by the cooling water in controlled circulation tank 9, after feed operation terminates, console 2 controls agitator 3 action, in whole course of reaction, console 2 controls each parts according to the parameter automatization pre-entered and has worked in coordination with reaction.
Claims (1)
1., for the production of an automation reactor device for Graphene, it is characterized in that agent structure comprises material inlet valve, console, agitator, temperature controller, temperature transmitter, liquid level speed changer, cryogenic thermostat water bath, discharging pump, circulating water chennel, reactor, cooling water pipeline, discharge pipe and feed pipe, the outer wall of the reactor of U-shaped structure is provided with circulating water chennel, three material inlet valves are provided with above the external left of reactor, material inlet valve enters reactor by feed pipe, the top of reactor is provided with agitator, the upper right side of reactor is provided with the temperature controller with temperature transmitter, the right hand external of reactor is provided with the liquid level speed changer be connected with reactor, cryogenic thermostat water bath is provided with below the external right of reactor, cryogenic thermostat water bath is connected with circulating water chennel by cooling water pipeline, the lower right of cryogenic thermostat water bath is provided with discharging pump, discharging pump enters the bottom of reactor through circulating water chennel by discharge pipe, console and reactor are independently arranged, equal telecommunications manner of breathing connects between console and material inlet valve, between console and agitator, between console and temperature controller, between console and liquid level speed changer, between console and cryogenic thermostat water bath, between console and discharging pump and between temperature controller and cryogenic thermostat water bath, and each parts are joined and are configured for producing the automation reactor device of Graphene.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520481008.4U CN204746321U (en) | 2015-07-06 | 2015-07-06 | A automatic reation kettle device for producing graphite alkene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520481008.4U CN204746321U (en) | 2015-07-06 | 2015-07-06 | A automatic reation kettle device for producing graphite alkene |
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| CN204746321U true CN204746321U (en) | 2015-11-11 |
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| CN201520481008.4U Active CN204746321U (en) | 2015-07-06 | 2015-07-06 | A automatic reation kettle device for producing graphite alkene |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106123558A (en) * | 2016-06-28 | 2016-11-16 | 西部宝德科技股份有限公司 | A kind of Apparatus and method for being dried metal-based porous gel film |
| CN108417834A (en) * | 2018-05-07 | 2018-08-17 | 福州鼎烯飞扬科技有限公司 | A kind of process units for producing graphene-based negative material |
| CN108461735A (en) * | 2018-03-20 | 2018-08-28 | 福州鼎烯飞扬科技有限公司 | A kind of process units and production method for graphene-based composite negative pole material |
-
2015
- 2015-07-06 CN CN201520481008.4U patent/CN204746321U/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106123558A (en) * | 2016-06-28 | 2016-11-16 | 西部宝德科技股份有限公司 | A kind of Apparatus and method for being dried metal-based porous gel film |
| CN106123558B (en) * | 2016-06-28 | 2019-02-05 | 西部宝德科技股份有限公司 | A kind of device and method for drying metal-based porous gel mould |
| CN108461735A (en) * | 2018-03-20 | 2018-08-28 | 福州鼎烯飞扬科技有限公司 | A kind of process units and production method for graphene-based composite negative pole material |
| CN108461735B (en) * | 2018-03-20 | 2020-07-10 | 福州鼎烯飞扬科技有限公司 | Production device and production method for graphene-based composite negative electrode material |
| CN108417834A (en) * | 2018-05-07 | 2018-08-17 | 福州鼎烯飞扬科技有限公司 | A kind of process units for producing graphene-based negative material |
| CN108417834B (en) * | 2018-05-07 | 2024-01-05 | 深圳市恒利德科技有限公司 | Production device for producing graphene-based anode material |
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