CN204745734U - Filler extraction tower redistributor - Google Patents

Filler extraction tower redistributor Download PDF

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Publication number
CN204745734U
CN204745734U CN201520404994.3U CN201520404994U CN204745734U CN 204745734 U CN204745734 U CN 204745734U CN 201520404994 U CN201520404994 U CN 201520404994U CN 204745734 U CN204745734 U CN 204745734U
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China
Prior art keywords
extraction tower
redistributor
downspout
distribution grid
distribution
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CN201520404994.3U
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Chinese (zh)
Inventor
朱慎林
钱建兵
施龙生
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QIDONG JULONG PETROLEUM CHEMICAL EQUIPMENT CO Ltd
Tsinghua University
Original Assignee
QIDONG JULONG PETROLEUM CHEMICAL EQUIPMENT CO Ltd
Tsinghua University
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Priority to CN201520404994.3U priority Critical patent/CN204745734U/en
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model discloses a filler extraction tower redistributor, including discoid distributing plate and a plurality of root with the perpendicular circular downspout that sets up of distributing plate, it has a plurality of distribution hole to open on the distributing plate, downspout top seal, the relative both sides of lateral wall are equipped with same trompil, and the bottom is provided with and keeps off the liquid cap, it has the annulus to keep off between liquid cap and the downspout bottom. This extraction tower redistributor is rational in infrastructure, and the congruence decentralized photo distributes evenly in succession, has eliminated the axial back mixing, the percent opening is big, and the mass transfer is efficient, can satisfy the requirement of big handling capacity and device maximization.

Description

A kind of packed extraction tower redistributor
Technical field
The utility model relates to separation equipment technical field, specifically a kind of packed extraction tower redistributor.
Background technology
Liquid-liquid extraction is one of important method of chemical separating, is the separation or the purification that utilize the difference of the distribution ratio between the solvent of solute or partial miscibility immiscible at two kinds to realize each component.Packed extraction tower is one of capital equipment realizing Liquid-liquid Extraction Processes, and its main advantage is to realize large-scale continuous production.In packed extraction tower, mainly rely on density contrast, under gravity, decentralized photo, with the form of droplet cluster and continuous phase counter current contacting, carries out mass transfer.
For packed extraction tower, the effect of filler mainly contains two aspects, and one is the axial backmixing suppressing continuous phase and decentralized photo, and two are to provide surface area to promote the pulverizing of decentralized photo, polymerization and to disperse to strengthen mass transfer again.But,, continuous phase ratio of viscosities smaller at two-phase density contrast is larger, axial backmixing in packed extraction tower is very serious, especially the axial backmixing of continuous phase, and along with chemical industry unit scale maximize development, the enlarge-effect of packed extraction tower is particularly evident, and its tower height of about 90% is for making up axial backmixing, this not only constrains extraction output of column, and has a strong impact on the separative efficiency of extraction tower.
Chinese patent 201210177128.6 discloses a kind of packed extraction tower with redistributor and/or vertical baffle, circular downeomer offered by the redistributor wherein arranged, continuous phase enters lower floor's filler by downspout, and decentralized photo then enters upper strata filler by the circular hole on metal dish.But this structure, eddy current can be formed at downspout top, the drop disperseed is made again to bring in downspout and enter lower floor's filler, and lower floor's filler dispersed phase drop from bottom to top can not be redistributed by circular hole in disk bottom polymerization completely again, part directly will enter upper strata filler by downspout, forms short circuit.These two kinds of bad flow regimes will directly cause the axial backmixing of continuous phase and decentralized photo, have impact on the raising of mass-transfer efficiency.
Utility model content
In order to solve the problems of the technologies described above, the utility model provides a kind of rational in infrastructure, the packed extraction tower redistributor that can eliminate continuous phase and decentralized photo axial backmixing.
The technical solution adopted in the utility model is: a kind of packed extraction tower redistributor, comprise discoid distribution grid and some and the vertically disposed circular downeomer of described distribution grid, described distribution grid has some distribution holes, described downspout top seal, sidewall is provided with same perforate relative to both sides, bottom is provided with liquid-blocking cap, has annular space between bottom described liquid-blocking cap and downspout.
The discoid distribution grid of above-mentioned redistributor is welded with some pieces of metallic plates vertically upward, sheetmetal side has perforate.These metallic plates be some rectangular slabs be combined into a cuboid and discoid distribution grid integrally welded, have perforate in cuboid side.
In above-mentioned redistributor, described circular downeomer top shrouding seals, and downspout diameter is 20mm ~ 300mm, is highly 50 ~ 400mm, and the downspout cross section gross area accounts for 0.5 ~ 20% of the distribution grid gross area.
The distribution hole diameter of above-mentioned redistributor is 2mm ~ 15mm, and distribution hole can adopt equilateral triangle or square arrangement.
In above-mentioned redistributor, the perforate of downcomer side walls is circular, oval or rectangle.
In above-mentioned redistributor, the annular space height between bottom described liquid-blocking cap and downspout is 20 ~ 100mm.
The utility model advantage is: this extraction tower redistributor is rational in infrastructure, and continuous phase and dispersed phase distribution evenly, eliminate axial backmixing; Percent opening is large, and mass-transfer efficiency is high, can meet the requirement of high throughput and larger-scale unit.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
In figure, 1, distribution grid, 2, distribution hole, 3, downspout, 4, shrouding, 5, perforate, 6, liquid-blocking cap, 7, annular space, 8, metallic plate.
detailed description of the invention:
Below in conjunction with the drawings and specific embodiments, the technical solution of the utility model is further described, but protection domain of the present utility model is not limited thereto.
The extraction tower redistributor of different-diameter can be embodied as:
Embodiment one: diameter is be provided with redistributor of the present utility model in the packed extraction tower of 600mm, on the discoid distribution grid 1 of this redistributor, bending is welded with the metallic plate 8 that 1 piece of height is vertically upward 50mm, distribution grid has 68 10mm distribution holes 2, distribution hole 2 can adopt equilateral triangle or square arrangement, the circular downeomer 3 of 4 50mm is vertical with distribution grid 1 to be arranged, downspout height 200mm, downspout top shrouding 4 seals, sidewall opens strip hole 40mm × 30mm, liquid-blocking cap 6 is provided with bottom downspout 3, between bottom liquid-blocking cap 6 and downspout 3, there is annular space, annular space height 50mm, liquid-blocking cap diameter 60mm.
This extraction tower redistributor downspout 3 cross section gross area accounts for 2.78% of distribution grid 1 gross area, and percent opening is 1.9%.(percent opening is exactly the perforate gross area of the perforate gross area divided by distribution grid of downspout)
Embodiment two: diameter is be provided with redistributor of the present utility model in the packed extraction tower of 1800mm, the discoid distribution grid 1 of this redistributor is welded with the metallic plate 8 that 5 pieces of height are vertically upward 50mm, distribution grid has 764 5mm distribution holes 2, distribution hole 2 can adopt equilateral triangle or square arrangement, the circular downeomer 3 of 14 80mm is vertical with distribution grid 1 to be arranged, downspout height 300mm, downspout top shrouding 4 seals, sidewall opens strip hole 70mm × 40mm, liquid-blocking cap 6 is provided with bottom downspout 3, between bottom liquid-blocking cap 6 and downspout 3, there is annular space, annular space height 50mm, liquid-blocking cap diameter 100mm.
This extraction tower redistributor downspout 3 cross section gross area accounts for 2.76% of distribution grid 1 gross area, and percent opening is 0.59%.
Embodiment three: diameter is be provided with redistributor of the present utility model in the packed extraction tower of 4000mm, the discoid distribution grid 1 of this redistributor is welded with the metallic plate 8 that 23 pieces of height are vertically upward 80mm, distribution grid has 5480 10mm distribution holes 2, distribution hole 2 can adopt equilateral triangle or square arrangement, the circular downeomer 3 of 40 80mm is vertical with distribution grid 1 to be arranged, downspout height 250mm, downspout top shrouding 4 seals, sidewall opens strip hole 70mm × 30mm, liquid-blocking cap 6 is provided with bottom downspout 3, between bottom liquid-blocking cap 6 and downspout 3, there is annular space, annular space height 50mm, liquid-blocking cap diameter 100mm.
This extraction tower redistributor downspout 3 cross section gross area accounts for 1.6% of distribution grid 1 gross area, and percent opening is 3.42%.
This extraction tower redistributor is rational in infrastructure, can meet the requirement of high throughput and larger-scale unit, can be widely used in desulfuration of liquefied gas, lube oil finishing, propane deasphalting, ethylene unit scrubbing tower, the extract and separate unit operations systems such as wastewater treatment.

Claims (8)

1. a packed extraction tower redistributor, comprise discoid distribution grid and some and the vertically disposed circular downeomer of described distribution grid, it is characterized in that: described distribution grid has some distribution holes, described downspout top seal, sidewall is provided with same perforate relative to both sides, bottom is provided with liquid-blocking cap, has annular space between bottom described liquid-blocking cap and downspout.
2. a kind of packed extraction tower redistributor according to claim 1, is characterized in that: described discoid distribution grid is welded with some pieces of metallic plates vertically upward.
3. a kind of packed extraction tower redistributor according to claim 1, it is characterized in that: described circular downeomer diameter is 20mm ~ 300mm, is highly 50 ~ 400mm, and the downspout cross section gross area accounts for 0.5 ~ 20% of the distribution grid gross area.
4. a kind of packed extraction tower redistributor according to claim 1, is characterized in that: described circular downeomer top shrouding seals.
5. a kind of packed extraction tower redistributor according to claim 1, is characterized in that: the diameter of described distribution hole is 2mm ~ 15mm.
6. a kind of packed extraction tower redistributor according to claim 1 or 5, is characterized in that: described distribution hole adopts equilateral triangle or square arrangement.
7. extraction tower redistributor according to claim 1, is characterized in that: described perforate is circular, oval or rectangle.
8. extraction tower redistributor according to claim 1, is characterized in that: described annular space height is 20 ~ 100mm.
CN201520404994.3U 2015-06-12 2015-06-12 Filler extraction tower redistributor Active CN204745734U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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CN201520404994.3U CN204745734U (en) 2015-06-12 2015-06-12 Filler extraction tower redistributor

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105413622A (en) * 2015-12-29 2016-03-23 天津市创举科技有限公司 Low-backmixing uniform-efficiency tower plate
CN106267886A (en) * 2016-08-29 2017-01-04 中冶焦耐(大连)工程技术有限公司 Liquid distribution trough and method of work thereof in a kind of extraction tower
CN114425182A (en) * 2020-10-29 2022-05-03 中国石油化工股份有限公司 Liquid disperser for small extraction tower and small extraction tower

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105413622A (en) * 2015-12-29 2016-03-23 天津市创举科技有限公司 Low-backmixing uniform-efficiency tower plate
CN105413622B (en) * 2015-12-29 2017-05-03 天津市创举科技有限公司 Low-backmixing uniform-efficiency tower plate
CN106267886A (en) * 2016-08-29 2017-01-04 中冶焦耐(大连)工程技术有限公司 Liquid distribution trough and method of work thereof in a kind of extraction tower
CN106267886B (en) * 2016-08-29 2018-02-27 中冶焦耐(大连)工程技术有限公司 Liquid distribution trough and its method of work in a kind of extraction tower
CN114425182A (en) * 2020-10-29 2022-05-03 中国石油化工股份有限公司 Liquid disperser for small extraction tower and small extraction tower
CN114425182B (en) * 2020-10-29 2023-09-12 中国石油化工股份有限公司 Liquid disperser for small extraction tower and small extraction tower

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