CN204121795U - A kind of novel packed tower suppressing gas fractionation unit to block liquid - Google Patents
A kind of novel packed tower suppressing gas fractionation unit to block liquid Download PDFInfo
- Publication number
- CN204121795U CN204121795U CN201420554828.7U CN201420554828U CN204121795U CN 204121795 U CN204121795 U CN 204121795U CN 201420554828 U CN201420554828 U CN 201420554828U CN 204121795 U CN204121795 U CN 204121795U
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- packed tower
- liquid
- liquid phase
- type liquid
- tower
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- 239000007788 liquid Substances 0.000 title claims abstract description 52
- 238000005194 fractionation Methods 0.000 title claims abstract description 12
- 239000007791 liquid phase Substances 0.000 claims abstract description 30
- 238000012856 packing Methods 0.000 claims abstract description 14
- 239000007921 spray Substances 0.000 claims description 10
- 238000012546 transfer Methods 0.000 abstract description 12
- 238000000034 method Methods 0.000 abstract description 6
- 230000008569 process Effects 0.000 abstract description 5
- 239000012530 fluid Substances 0.000 abstract description 4
- 238000007670 refining Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 230000001131 transforming effect Effects 0.000 abstract description 2
- 239000000945 filler Substances 0.000 description 10
- 239000012071 phase Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 238000011049 filling Methods 0.000 description 3
- 239000010865 sewage Substances 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000004907 flux Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000016507 interphase Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 230000011218 segmentation Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a kind of novel packed tower suppressing gas fractionation unit to block liquid, comprise the cylindrical shell of packed tower, the anti-swirl baffle being arranged at the wire mesh demister in cylindrical shell, packing layer, liquid header from top to bottom and being arranged at the bottom of tower, it is characterized in that being provided with guide-plate type liquid phase distributor between wire mesh demister in cylindrical shell and packing layer, described guide-plate type liquid phase distributor is that guide plate is communicated with slot type liquid phase distributor.The novel packed tower that the utility model provides, by transforming packed tower internal structure, in system, gas-liquid is more evenly distributed, and resistance bubble performance is good, improve the performance of anti-blockage in fluid mass-transfer process, effectively inhibit gas fractionation unit to block the possibility of liquid, ensure that the long-period stable operation of packed tower and whole device, improve the operating efficiency of packed tower.The utility model is widely used in the separator of the process gas in the fields such as chemical industry, oil refining, pharmacy and environmental protection.
Description
Technical field
The utility model belongs to gas-liquid separation technical field, relates to a kind of novel packed tower, in particular, relates to a kind of novel packed tower suppressing gas fractionation unit to block liquid.
Background technology
Packed tower is very important gas-liquid mass transfer (contact) equipment, there is the advantages such as separating effect is high, flux is large, pressure drop is low, liquid holdup is little, and at vacuumizing, the separation of heat sensitive material and the aspect such as energy-conservation have superiority, so be widely used in the fields such as chemical industry, oil refining, pharmacy and environmental protection.Be mainly used to the heat and mass transfer processing fluid (gas or liquid), the purification realizing material be separated.Interphase mass transfer process between gas-liquid, all as the processes such as absorption, regeneration, stripping, distillation, extraction can carry out in packed tower.
In mass-transfer progress, by the impact of tower tray and tower internals framework and solution composition, inevitably there is the problems such as foaming in liquid phase component, that can cause packed tower time serious blocks liquid sometimes.
At present, packed tower in the gas fractionation unit of the industry such as chemical industry, oil refining, by the impact of tower internal structure, be circulated in the space that the impurity such as the solid particle in the liquid phase in device, greasy dirt very easily block tower internals, hinder the mass transfer of liquid phase component, cause tower to press to increase, that causes packing type absorption tower blocks liquid.The fluctuation of whole operating unit can be caused simultaneously, cause the instability that device operates.
Summary of the invention
The utility model is in order to overcome deficiency of the prior art, provide that a kind of entrainment is little, disposal ability is large, can effectively suppress gas fractionation unit to block the novel packed tower of liquid, thus the air content in reduction liquid phase, reduce the danger that liquid is blocked in tower inside, improve the flux of packed tower.
For solving the problems of the technologies described above, the utility model provides a kind of novel packed tower suppressing gas fractionation unit to block liquid, comprise the cylindrical shell of packed tower, the anti-swirl baffle being arranged at the wire mesh demister in cylindrical shell, packing layer, liquid header from top to bottom and being arranged at the bottom of tower, it is characterized in that being provided with guide-plate type liquid phase distributor between wire mesh demister in cylindrical shell and packing layer, described guide-plate type liquid phase distributor is that guide plate is communicated with slot type liquid phase distributor.
Further, described packed tower comprises at least one group of guide plate and is communicated with slot type liquid phase distributor.
Described guide plate is communicated with slot type liquid phase distributor and comprises distribution grid and slotted disk, and distribution grid is provided with riser, and riser is provided with liquid-blocking cap, support, upper strata spray apertures and lower floor's spray apertures, and slotted disk is provided with connectivity slot, draining plate and liquid distributing groove.
The utility model also comprises the solution inlet port pipe known by this field, hold-down grid, filler, screen, grid support device, top catch tray, bottom catch tray, feed tube, gas feed, sewage draining exit etc.
The suppression gas fractionation unit that the utility model provides blocks the novel packed tower of liquid, by transforming packed tower inside, effectively can realize Heat and mass transfer, cut resistance bubble performance good, improve operational stability and the operating efficiency of packed tower, cutter has following technique effect:
1) gas phase channel is more evenly distributed;
2) gas phase channel pressure drop is low, and gas rising resistance is little;
3) liquid distribution evenly, further, comprise geometry distribution and flow distribution evenly;
4) liquid phase processing load is large, is not easily formed and block liquid phenomenon in mass-transfer progress.
Accompanying drawing explanation
Fig. 1 is that embodiment suppresses gas fractionation unit to block the structural representation of the novel packed tower of liquid.
Fig. 2 is the structural representation that embodiment centering guide is communicated with slot type liquid phase distributor.
Fig. 3 is the partial enlargement structural representation in I portion in Fig. 2.
Fig. 4 is the plan structure schematic diagram of Fig. 2.
In figure, 1-cylindrical shell; 2-gas feed; 3-wire mesh demister; 4-solution inlet port pipe; 5,10-guide plate is communicated with slot type liquid phase distributor; 6-hold-down grid; 7-filler 7; 8-screen; 9-grid support device; 11-top catch tray; 12-bottom catch tray; 13-feed tube; 14-anti-swirl baffle; 15-sewage draining exit.
5-1 is liquid-blocking cap, and 5-2 is support, and 5-3 is upper strata spray apertures, and 5-4 is lower floor's spray apertures, and 5-5 is riser, and 5-6 is distribution grid, and 5-7 is connectivity slot, and 5-8 is draining plate, 5-9 liquid distributing groove.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the utility model is described in detail.
Embodiment: see Fig. 1, the suppression gas fractionation unit that the present embodiment provides blocks the novel packed tower of liquid, comprise the cylindrical shell 1 of packed tower, the anti-swirl baffle 14 being arranged at the wire mesh demister 3 in cylindrical shell 1, packing layer, liquid header from top to bottom and being arranged at the bottom of tower, its main feature is wire mesh demister 3 in cylindrical shell 1 and is provided with guide-plate type liquid phase distributor between packing layer, and described guide-plate type liquid phase distributor is that guide plate is communicated with slot type liquid phase distributor.
In embodiment, packed tower comprises one group of guide plate and is communicated with slot type liquid phase distributor 5,10.
See Fig. 2-4, guide plate is communicated with slot type liquid phase distributor and comprises distribution grid 5-6 and slotted disk, distribution grid 5-6 is provided with riser 5-5, riser 5-5 is provided with liquid-blocking cap 5-1, support 5-2, upper strata spray apertures 5-3 and lower floor spray apertures 5-4, and slotted disk is provided with connectivity slot 5-7, draining plate 5-8 and liquid distributing groove 5-9.
Embodiment device, also comprises the solution inlet port pipe 4 known by this field, hold-down grid 6, filler 7, screen 8, grid support device 9, top catch tray 11, bottom catch tray 12, feed tube 13, gas feed 2, sewage draining exit 15 etc.
The novel packed tower of embodiment is the mass transfer apparatus using the filler in tower as gas-liquid two-phase Contact component, belongs to continuous contact gas-liquid mass transfer (contact) equipment, and two phase compositions are along tower height consecutive variations, and under normal operating condition, gas phase is continuous phase, and liquid phase is decentralized photo.The tower body of packed tower is vertical cylinder always, and supporting plate is equipped with in bottom, and filler is to huddle or the mode of whole block is placed on support plate.Hold-down grid is installed, in case blown by ascending air in the top of filler.Liquid sprays filler from tower top through guide-plate type liquid phase distributor, and flows down along filling surface.Gas is sent at the bottom of tower, and after distribution device in gas-fluid (minor diameter tower does not generally establish distribution device in gas-fluid) distribution, be the space that adverse current continues through packing layer with liquid, on filling surface, gas-liquid two-phase close contact carries out mass transfer.
When liquid flows downward along packing layer, have gradually to the trend that tower wall is concentrated, the flow quantity near tower wall is increased gradually, form wall stream.Wall stream effect causes gas-liquid two-phase skewness in packing layer, thus mass-transfer efficiency is declined.Therefore, when packing layer is higher, need to carry out segmentation to described packed tower, centre arranges apparatus for redistributing.Liquid redistribution device comprises liquid header and liquid re-distributor two parts, and the liquid under the filler stream of upper strata, after liquid header is collected, delivers to liquid re-distributor, sprays on lower floor's filler after redistribution.
The Novel guide plate formula liquid phase distributor of embodiment is arranged on above described packing layer, and the two ends of each Novel guide plate formula liquid phase distributor are fixed on same plane.The advantages such as it is comparatively simple that described guide-plate type liquid phase distributor has structure, easy for installation, and pressure drop is little, anti-carries secretly, occupy-place is low, make gas and liquid distribution evenly.Be suitable for the conditions such as charging, side take-off and liquid collection distribute again simultaneously.It is the development of disc type liquid distribution trough, and has some advantage of tank type liquid distributor.Slotted disc type distributor is by rising gas cap, and riser, catheter and chassis form.Just be that up big and down small two arrange aperture and open at the top of rectangle riser and middle part respectively with the essential difference of disc type distributor, by special catheter, liquid imported the low gas velocity district of filling surface.Design adopts full-mesh formula first-stage tank and guide plate stream, adopt and add special support distribution groove structure.Described distributor can play the function of liquid collecting, distribution of gas, liquid distribution and side take-off simultaneously.Be equipped with flow-guiding type filler pressing and can make Novel guide plate formula gas-liquid distributor liquid distribution better effects if, antiblocking ability is strong, the sedimentation being more conducive to drop with the feature such as to be separated.Operating flexibility and the operational load of device are larger.
The present embodiment, by the transformation to packed tower internal structure, is widely used in the separator of the process gas in the fields such as chemical industry, oil refining, pharmacy and environmental protection; Because its operating flexibility is large, device stability is high, therefore has good application prospect.
It should be noted last that, above detailed description of the invention is only in order to illustrate the technical solution of the utility model and unrestricted, although be described in detail the utility model with reference to the practical structures in example, but can modify to the technical solution of the utility model or equivalent replacement, should be those skilled in the art in common knowledge, and not departing from the spirit and scope of technical solutions of the utility model, it all should be encompassed in right of the present utility model.
Claims (3)
1. the novel packed tower suppressing gas fractionation unit to block liquid, comprise the cylindrical shell of packed tower, the anti-swirl baffle being arranged at the wire mesh demister in cylindrical shell, packing layer, liquid header from top to bottom and being arranged at the bottom of tower, it is characterized in that being provided with guide-plate type liquid phase distributor between wire mesh demister in cylindrical shell and packing layer, described guide-plate type liquid phase distributor is that guide plate is communicated with slot type liquid phase distributor.
2. novel packed tower according to claim 1, is characterized in that packed tower comprises at least one group of guide plate and is communicated with slot type liquid phase distributor.
3. novel packed tower according to claim 1 and 2, it is characterized in that described guide plate is communicated with slot type liquid phase distributor and comprises distribution grid and slotted disk, distribution grid is provided with riser, riser is provided with liquid-blocking cap, support, upper strata spray apertures and lower floor's spray apertures, and slotted disk is provided with connectivity slot, draining plate and liquid distributing groove.
Priority Applications (1)
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CN201420554828.7U CN204121795U (en) | 2014-09-25 | 2014-09-25 | A kind of novel packed tower suppressing gas fractionation unit to block liquid |
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CN201420554828.7U CN204121795U (en) | 2014-09-25 | 2014-09-25 | A kind of novel packed tower suppressing gas fractionation unit to block liquid |
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CN204121795U true CN204121795U (en) | 2015-01-28 |
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CN201420554828.7U Expired - Lifetime CN204121795U (en) | 2014-09-25 | 2014-09-25 | A kind of novel packed tower suppressing gas fractionation unit to block liquid |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106693432A (en) * | 2017-03-22 | 2017-05-24 | 中国石油大学(华东) | Centrifugal rotational flow defomaing type gas-liquid mixture feeding distributor |
CN106731518A (en) * | 2016-12-23 | 2017-05-31 | 青上化工(惠州)有限公司 | A kind of hydrochloric acid absorption tower |
CN114225449A (en) * | 2021-12-25 | 2022-03-25 | 东营威联化学有限公司 | Xylene tower |
CN115177963A (en) * | 2022-07-17 | 2022-10-14 | 中国石油化工股份有限公司 | Double-dispersion gas-liquid mass transfer device |
CN115364506A (en) * | 2022-10-24 | 2022-11-22 | 北京先锋创新科技发展有限公司 | Industrial efficient packing type heat and mass transfer equipment |
-
2014
- 2014-09-25 CN CN201420554828.7U patent/CN204121795U/en not_active Expired - Lifetime
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106731518A (en) * | 2016-12-23 | 2017-05-31 | 青上化工(惠州)有限公司 | A kind of hydrochloric acid absorption tower |
CN106693432A (en) * | 2017-03-22 | 2017-05-24 | 中国石油大学(华东) | Centrifugal rotational flow defomaing type gas-liquid mixture feeding distributor |
CN106693432B (en) * | 2017-03-22 | 2023-12-12 | 中国石油大学(华东) | Centrifugal rotational flow defoaming type gas-liquid mixed phase feeding distributor |
CN114225449A (en) * | 2021-12-25 | 2022-03-25 | 东营威联化学有限公司 | Xylene tower |
CN115177963A (en) * | 2022-07-17 | 2022-10-14 | 中国石油化工股份有限公司 | Double-dispersion gas-liquid mass transfer device |
CN115177963B (en) * | 2022-07-17 | 2024-03-26 | 中国石油化工股份有限公司 | Double-dispersion gas-liquid mass transfer device |
CN115364506A (en) * | 2022-10-24 | 2022-11-22 | 北京先锋创新科技发展有限公司 | Industrial efficient packing type heat and mass transfer equipment |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CP01 | Change in the name or title of a patent holder |
Address after: Liuhe District of Nanjing City, Jiangsu province 210048 geguan Road No. 699 Patentee after: CHINA PETROLEUM & CHEMICAL Corp. Patentee after: SINOPEC NANJING CHEMICAL RESEARCH INSTITUTE Co.,Ltd. Address before: Liuhe District of Nanjing City, Jiangsu province 210048 geguan Road No. 699 Patentee before: China Petroleum & Chemical Corp. Patentee before: RESEARCH INSTITUTE OF NANJING CHEMICAL INDUSTRIAL Group |
|
CP01 | Change in the name or title of a patent holder | ||
CX01 | Expiry of patent term |
Granted publication date: 20150128 |