CN204709819U - A kind of pharmacology experimental provision - Google Patents
A kind of pharmacology experimental provision Download PDFInfo
- Publication number
- CN204709819U CN204709819U CN201520214010.5U CN201520214010U CN204709819U CN 204709819 U CN204709819 U CN 204709819U CN 201520214010 U CN201520214010 U CN 201520214010U CN 204709819 U CN204709819 U CN 204709819U
- Authority
- CN
- China
- Prior art keywords
- rotating shaft
- condenser
- revolving bottle
- experimental provision
- receiving flask
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000008236 heating water Substances 0.000 claims abstract description 7
- 238000000498 ball milling Methods 0.000 claims description 9
- 238000001704 evaporation Methods 0.000 abstract description 11
- 239000003814 drug Substances 0.000 abstract description 4
- 238000000746 purification Methods 0.000 abstract description 3
- 238000010438 heat treatment Methods 0.000 description 11
- 238000001816 cooling Methods 0.000 description 7
- 230000008020 evaporation Effects 0.000 description 7
- 239000002904 solvent Substances 0.000 description 5
- KJFMBFZCATUALV-UHFFFAOYSA-N phenolphthalein Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)C2=CC=CC=C2C(=O)O1 KJFMBFZCATUALV-UHFFFAOYSA-N 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000011344 liquid material Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 229960000074 biopharmaceutical Drugs 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of pharmacology experimental provision, comprise revolving bottle, support, rotating shaft, condenser and receiving flask, described rotating shaft is located at support top, described rotating shaft is that hollow is arranged, described revolving bottle includes heated water bath and crosses pot and lock nut, described revolving bottle is located at above heating water bath, described lock nut is threaded with revolving bottle, described rotating shaft and lock nut are rotationally connected, described condenser is located at above receiving flask, vacuum orifice and condenser pipe is provided with in described condenser, described condenser is communicated with rotating shaft, described condenser pipe is spiral cold-finger, described condenser pipe is provided with water inlet and delivery port, described condenser one end is provided with valve charge pipe, the utility model can high-efficiency evaporating, to the concentrated purification of medicine, easy to use.
Description
Technical field
The utility model relates to a kind of pharmacology experimental provision.
Background technology
A kind of evaporator of laboratory extensive use, be applicable to the course of reaction etc. that reflux operation, the rapid evaporation of a large amount of solvent, the concentrated of microcomponent and needs stir, rotary evaporator system can seal and be decompressed to 400 ~ 600 millimetress of mercury, with the solvent in heating bath heating cucurbit, heating-up temperature can close to the boiling point of this solvent; Also can rotate, speed is 50 ~ 160 revs/min simultaneously, makes solvent form film, increase disengagement area, in addition, under high-effect cooling device effect, heat steam can be liquefied rapidly, accelerate evaporation rate, be mainly used in concentrated, crystallization, the drying of the industries such as medicine, chemical industry and bio-pharmaceuticals, be separated and solvent reclaims, its principle is under vacuum, heated at constant temperature, make revolving bottle constant speed rotary, material forms large area film at bottle wall, high-efficiency evaporating.
Leakage is the common phenomenon of the failure of evaporimeter, in use should note frequent leak detection, can check with phenolphthalein test paper leak, because ammonia is alkalescence, chance phenolphthalein test paper reddens, with time soon, general is exactly leakage point in the place of the somewhere frost-free of evaporimeter, also can look for leakage at leak suds, the inspection that Freon-Evaporator leaks can use Halogen lamp LED and halogen leak detector, also can look for leakage with suds, the appearance leakage phenomenon that existing evaporimeter can be regular, that makes to experiment is implemented as inconvenience.
Summary of the invention
The technical problems to be solved in the utility model is to provide one can high-efficiency evaporating, to the concentrated purification of medicine, easy to use, effectively avoids the pharmacology experimental provision revealed.
For solving the problem, the utility model adopts following technical scheme:
A kind of pharmacology experimental provision, comprise revolving bottle, support, rotating shaft, condenser and receiving flask, described rotating shaft is located at support top, revolving bottle can rotary heating, greatly improve evaporation efficiency, described rotating shaft is that hollow is arranged, described revolving bottle includes heated water bath and crosses pot and lock nut, lock nut prevents from occurring when heating revealing, described revolving bottle is located at above heating water bath, heating water bath can provide heating for revolving bottle, described lock nut is threaded with revolving bottle, described rotating shaft and lock nut are rotationally connected, described condenser is located at above receiving flask, vacuum orifice and condenser pipe is provided with in described condenser, condenser pipe can high efficiency cooling, receiving flask is facilitated to collect, described condenser is communicated with rotating shaft, described condenser pipe is spiral cold-finger, described condenser pipe is provided with water inlet and delivery port, water inlet and delivery port can keep water cooling, reduce cool time, described condenser one end is provided with valve charge pipe.
As preferably, described receiving flask is provided with ball milling mouth folder, prevents interface from revealing.
As preferably, described receiving flask is connected with condenser by ball milling mouth folder, prevents interface from revealing.
As preferably, described rotating shaft is fixedly connected with support, keeps stable when moving of rotating shaft.
As preferably, described support bottom is provided with fixing sucking disk, can fixed base, more stable during use.
This technical scheme has high-efficiency evaporating, to the concentrated purification of medicine, easy to use, effectively avoids the feature revealed.
The beneficial effects of the utility model are: the revolving bottle of setting can rotary heating, greatly improve evaporation efficiency, lock nut prevents from occurring when heating revealing, and heating water bath can provide heating for revolving bottle, condenser pipe can high efficiency cooling, facilitate receiving flask to collect, water inlet and delivery port can keep water cooling, reduce cool time, ball milling mouth folder prevents interface from revealing, fixing sucking disk, can fixed base, more stable during use.
Accompanying drawing explanation
In order to be illustrated more clearly in the utility model embodiment or technical scheme of the prior art, be briefly described to the accompanying drawing used required in embodiment or description of the prior art below, apparently, accompanying drawing in the following describes is only embodiments more of the present utility model, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to these accompanying drawings.
Fig. 1 is the structure chart of a kind of pharmacology experimental provision of the present utility model.
Detailed description of the invention
Consult shown in Fig. 1, a kind of pharmacology experimental provision, comprise revolving bottle 1, support 2, rotating shaft 3, condenser 4 and receiving flask 5, described rotating shaft 3 is located at support 2 top, described rotating shaft 3 is hollow setting, described revolving bottle 1 includes heated water bath and crosses pot 6 and lock nut 7, in use, by vacuum orifice 8 by evacuating air in condenser 4, the rate of recovery and evaporation rate can be improved, in revolving bottle 1, liquid material is added by valve charge pipe 12, described revolving bottle 1 is located at above heating water bath 6, described lock nut 7 is threaded with revolving bottle 1, described rotating shaft 3 is rotationally connected with lock nut 7, described condenser 4 is located at above receiving flask 5, vacuum orifice 8 and condenser pipe 9 is provided with in described condenser 4, described condenser 4 is communicated with rotating shaft 3, described condenser pipe 9 is spiral cold-finger, in use, regulate heated water bath to cross pot 6 and heat revolving bottle 1, start rotating shaft 3 to rotate simultaneously, liquid after condenser pipe 9 arrives in receiving flask 5, described condenser pipe 9 is provided with water inlet 10 and delivery port 11, described condenser 4 one end is provided with valve charge pipe 12.
Described receiving flask 5 is provided with ball milling mouth folder 13, in use, fixes ball milling mouth folder 13 at interface.
Described receiving flask 5 is connected with condenser 4 by ball milling mouth folder 13, prevents interface from revealing.
Described rotating shaft 3 is fixedly connected with support 2, in use, keeps rotating shaft 3 stablizing when moving.
Described support 2 bottom is provided with fixing sucking disk 14, can fix support 2 and can not produce vibrations because rotating shaft 3 rotates.
In use, by vacuum orifice 8 by evacuating air in condenser 4, the rate of recovery and evaporation rate can be improved, in revolving bottle 1, liquid material is added by valve charge pipe 12, regulate heated water bath to cross pot 6 and heat revolving bottle 1, start rotating shaft 3 to rotate, the liquid after condenser pipe 9 arrives in receiving flask 5 simultaneously.
The beneficial effects of the utility model are: the revolving bottle of setting can rotary heating, greatly improve evaporation efficiency, lock nut prevents from occurring when heating revealing, and heating water bath can provide heating for revolving bottle, condenser pipe can high efficiency cooling, facilitate receiving flask to collect, water inlet and delivery port can keep water cooling, reduce cool time, ball milling mouth folder prevents interface from revealing, fixing sucking disk, can fixed base, more stable during use.
The above; be only detailed description of the invention of the present utility model; but protection domain of the present utility model is not limited thereto; any change of expecting without creative work or replacement; all should be encompassed within protection domain of the present utility model; therefore, the protection domain that protection domain of the present utility model should limit with claims is as the criterion.
Claims (5)
1. a pharmacology experimental provision, it is characterized in that: comprise revolving bottle, support, rotating shaft, condenser and receiving flask, described rotating shaft is located at support top, described rotating shaft is that hollow is arranged, described revolving bottle includes heated water bath and crosses pot and lock nut, described revolving bottle is located at above heating water bath, described lock nut is threaded with revolving bottle, described rotating shaft and lock nut are rotationally connected, described condenser is located at above receiving flask, vacuum orifice and condenser pipe is provided with in described condenser, described condenser is communicated with rotating shaft, described condenser pipe is spiral cold-finger, described condenser pipe is provided with water inlet and delivery port, described condenser one end is provided with valve charge pipe.
2. pharmacology experimental provision according to claim 1, is characterized in that: described receiving flask is provided with ball milling mouth folder.
3. pharmacology experimental provision according to claim 1, is characterized in that: described receiving flask is connected with condenser by ball milling mouth folder.
4. pharmacology experimental provision according to claim 1, is characterized in that: described rotating shaft is fixedly connected with support.
5. pharmacology experimental provision according to claim 1, is characterized in that: described support bottom is provided with fixing sucking disk.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520214010.5U CN204709819U (en) | 2015-04-10 | 2015-04-10 | A kind of pharmacology experimental provision |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520214010.5U CN204709819U (en) | 2015-04-10 | 2015-04-10 | A kind of pharmacology experimental provision |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204709819U true CN204709819U (en) | 2015-10-21 |
Family
ID=54308852
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520214010.5U Expired - Fee Related CN204709819U (en) | 2015-04-10 | 2015-04-10 | A kind of pharmacology experimental provision |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204709819U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106512448A (en) * | 2017-01-19 | 2017-03-22 | 江苏新思维信息系统工程有限公司 | Safe and efficient rotatory evaporator |
| CN106693424A (en) * | 2015-11-13 | 2017-05-24 | 步建设 | Western medicine distillation agent purification device |
| CN109464822A (en) * | 2018-12-13 | 2019-03-15 | 浙江电商检测有限公司 | Constant-temperature vacuum purifying plant |
| CN112716804A (en) * | 2020-12-17 | 2021-04-30 | 李成哲 | Refining equipment and processing technology for refining soft extract by adding into particulate matter |
-
2015
- 2015-04-10 CN CN201520214010.5U patent/CN204709819U/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106693424A (en) * | 2015-11-13 | 2017-05-24 | 步建设 | Western medicine distillation agent purification device |
| CN106512448A (en) * | 2017-01-19 | 2017-03-22 | 江苏新思维信息系统工程有限公司 | Safe and efficient rotatory evaporator |
| CN109464822A (en) * | 2018-12-13 | 2019-03-15 | 浙江电商检测有限公司 | Constant-temperature vacuum purifying plant |
| CN109464822B (en) * | 2018-12-13 | 2023-12-15 | 浙江电商检测有限公司 | Constant temperature vacuum purification device |
| CN112716804A (en) * | 2020-12-17 | 2021-04-30 | 李成哲 | Refining equipment and processing technology for refining soft extract by adding into particulate matter |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20151224 Address after: 1, Building 102, building 1, 528400 health Road, Torch Development Zone, Zhongshan, Guangdong, Zhongshan Patentee after: ZHONGSHAN DINGSHENG BIOTECHNOLOGY CO., LTD. Address before: 510850 Guangdong city in Guangzhou Province, Xinhua Street, Huadu District of Binhu Road No. 12, room 101 No. 7 Bay Patentee before: Xia Fangjun |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151021 Termination date: 20160410 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |