CN204656520U - A kind of photochemical and thermal reaction device - Google Patents
A kind of photochemical and thermal reaction device Download PDFInfo
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- CN204656520U CN204656520U CN201520224506.0U CN201520224506U CN204656520U CN 204656520 U CN204656520 U CN 204656520U CN 201520224506 U CN201520224506 U CN 201520224506U CN 204656520 U CN204656520 U CN 204656520U
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Abstract
The utility model relates to a kind of photochemical and thermal reaction device, comprise reactor body, described reactor body is column, be provided with in described reactor body and be oppositely arranged every predeterminable range between the upper and lower by the first transparency glass plate and the second transparency glass plate and sealed with the inwall of described reactor body the reaction chamber formed by black box, the upper end of described reactor body is provided with the first light illuminator, the lower end of described reactor body is provided with the second light illuminator, the sidewall of described reactor body is provided with reaction material entrance, described reaction material entrance communicates with the inside of described reaction chamber, the sidewall of described reactor body is provided with the installation of TC mouth, cooling tracheae installing port and heater installing port, described the installation of TC mouth, cooling tracheae installing port and heater installing port are connected with described reaction chamber respectively, described reactor body is also connected with pressure test device.The utility model can meet the needs of Opto-thertnal detection.
Description
Technical field
The utility model belongs to photochemical and thermal reaction device technical field, is specifically related to a kind of photochemical and thermal reaction device.
Background technology
Photochemical and thermal reaction device is a kind of integration reaction unit, have a wide range of applications in catalyst reaction performance test, light is as the natural energy form of one, act on catalyst sample, particularly act on corresponding light activated catalyst, catalyst can be made to be in excitation state, thus to promote the generation of catalytic reaction process.Photocatalysis has the advantage of self uniqueness, and compared to heat energy, the huge energy that photon carries can complete the chemical reaction process that heat energy cannot realize.Another feature light-catalysed is the selective of energy in addition, in principle monochromatic light selectively provocative reaction thing be required excitation state and vibration mode, complete course of reaction.But the reaction compared with the light of macro-energy is needed for some, often conventional white light (390-780nm) and ultraviolet source (254nm) possibly cannot meet, and light not quite also limits its application in the utilization ratio of catalytic reaction in addition.
Photochemical and thermal reaction process is combined by both light and heats, and in certain reaction temperature, under the booster action of light, the reactivity worth of catalyst is generally far above single photocatalysis and thermocatalytic activity.Therefore to reach the identical clean property of reaction, under the participation role of light, the temperature of reaction can be reduced significantly, the selective of reaction can be improved like this.On the contrary, the existence of thermal source can lower the energy of required light source, namely at a certain temperature, make originally to need the reaction in very high-octane light source effect can complete at conventional white light (390-780nm) and ultraviolet source (254nm).Therefore photochemical and thermal reaction device has given full play to the synergy of light and heat, mutually promotes, and has larger using value.
Photoreactor is now mainly used in photodissociation hydrogen manufacturing and air pollutants, and in the light degradation processes such as poisonous organic wastewater, reaction is generally carried out at normal temperatures.Photochemical and thermal reaction device and related application thereof rarely have in patent at home and relate to.Disclose in prior art and use hot air circulating system to be incubated the liquid in the serpentine coil in light reaction district, realize the carrying out of material light reaction procedure in uniform temperature, and obviously this course of reaction is integral process.And for reactor, how to realize differential course of reaction in conjunction with light then becomes still an open question.Therefore, the development and application of photochemical and thermal reaction device seems extremely important, also very urgent.
Utility model content
The purpose of this utility model is solve above-mentioned technical problem and provide a kind of photochemical and thermal reaction device.
For achieving the above object, the utility model adopts following technical scheme:
A kind of photochemical and thermal reaction device, comprise reactor body, described reactor body is column, be provided with in described reactor body and be oppositely arranged every predeterminable range between the upper and lower by the first transparency glass plate and the second transparency glass plate and sealed with the inwall of described reactor body the reaction chamber formed by black box, the upper end of described reactor body is provided with the first light illuminator, the lower end of described reactor body is provided with the second light illuminator, the sidewall of described reactor body is provided with reaction material entrance, described reaction material entrance communicates with the inside of described reaction chamber, the sidewall of described reactor body is provided with the installation of TC mouth, cooling tracheae installing port and heater installing port, described the installation of TC mouth, cooling tracheae installing port and heater installing port are connected with described reaction chamber respectively, described reactor body is also connected with pressure test device.
First and second light illuminator described and described reactor body are for being threaded.
The inside of first and second light illuminator described is provided with lamp panel, and on described lamp panel, annular is furnished with multiple lamp.
Described lamp is LED.
Described reactor body comprises reactor pars intermedia and the reactor top that is connected with described reactor pars intermedia and reactor lower part, described reactor top and described reactor pars intermedia are that detachable is connected, be integral type structure in the middle part of described reactor lower part and described reactor, described cooling tracheae installing port is located on the sidewall of described reactor lower part.
The photochemical and thermal reaction that the utility model not only can realize liquid or gas detects, and above-mentioned be provided with light illuminator at the upper and lower end of reactor body owing to adopting, and be provided with on the sidewall of reactor body the installation of TC mouth, cooling tracheae installing port and heater installing port be connected with described reaction chamber respectively, and be provided with pressure test device, thus the needs of Opto-thertnal detection can be met.
Accompanying drawing explanation
Figure 1 shows that the structural representation of a kind of photochemical and thermal reaction device that the utility model embodiment provides.
Detailed description of the invention
Below, in conjunction with example, substantive distinguishing features of the present utility model and advantage are further described, but the utility model is not limited to listed embodiment.
Refer to shown in Fig. 1, a kind of photochemical and thermal reaction device, comprise reactor body 1, described reactor body is column, be provided with in described reactor body and be oppositely arranged every predeterminable range between the upper and lower by the first transparency glass plate and the second transparency glass plate and sealed with the inwall of described reactor body the reaction chamber formed by black box, the upper end of described reactor body is provided with the first light illuminator 2, the lower end of described reactor body is provided with the second light illuminator 3, the sidewall of described reactor body is provided with reaction material entrance 8, described reaction material entrance communicates with the inside of described reaction chamber, the sidewall of described reactor body is provided with the installation of TC mouth 9, cooling tracheae installing port 6 and heater installing port 11, described the installation of TC mouth 9, cooling tracheae installing port 6 and heater installing port 11 are connected with described reaction chamber respectively, described reactor body is also connected with pressure test device 4.
It should be noted that, described reaction material entrance 8 can pass into gas or liquid in reaction chamber, a three-way connection can be used to connect source of the gas respectively or liquid source realizes control inputs.
First and second vitreum described is transparent, when detecting, smearing catalyst ink inject row detection by heating and illumination at its outer surface.Due to be adopt by first and second vitreum is formed seal reaction chamber, described novel reactor can also directly to injecting gas phase to be detected or liquid phase substance in reactor, and by heating and illumination penetrate realize photochemical and thermal reaction after detect the catalytic performance of gas phase or liquid phase substance, there is the function that solid, liquid, gas three-phase carries out photochemical and thermal reaction detection.
As an embodiment, first and second light illuminator described and described reactor body, for being threaded, being convenient to like this install and being detected.
As an embodiment, the inside of first and second light illuminator described is provided with lamp panel, and on described lamp panel, annular is furnished with multiple lamp.
Wherein, described lamp is LED, and described LED can adopt the lamp sending different colours.
As an embodiment, described reactor body 1 comprises reactor pars intermedia and the reactor top 10 that is connected with described reactor pars intermedia and reactor lower part 5, described reactor top is connected to form as detachable is connected with described reactor pars intermedia by bolt 7, be integral type structure in the middle part of described reactor lower part 5 and described reactor, described cooling tracheae installing port 6 is located on the sidewall of described reactor lower part.
The photochemical and thermal reaction that the utility model not only can realize liquid or gas detects, and above-mentioned be provided with light illuminator at the upper and lower end of reactor body owing to adopting, and be provided with on the sidewall of reactor body the installation of TC mouth, cooling tracheae installing port and heater installing port be connected with described reaction chamber respectively, and be provided with pressure test device, thus the needs of Opto-thertnal detection can be met.
It should be noted that, spoken of in this manual " embodiment ", " another embodiment ", " embodiment " etc., refer to the specific features, structure or the feature that describe in conjunction with this embodiment and be included at least one embodiment of the application's generality description.Multiple place occurs that statement of the same race is not one necessarily refer to same embodiment in the description.Furthermore, when describing specific features, structure or a feature in conjunction with any embodiment, what advocate is also drop in scope of the present utility model to realize this feature, structure or feature in conjunction with other embodiments.
Although be described the utility model with reference to multiple explanatory embodiment of the present utility model here, but, should be appreciated that, those skilled in the art can design a lot of other amendment and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit.
More particularly, in the scope of, accompanying drawing open in the application and claim, multiple modification and improvement can be carried out to the building block of subject combination layout and/or layout.Except the modification of carrying out building block and/or layout is with except improvement, to those skilled in the art, other purposes also will be obvious.
Claims (5)
1. a photochemical and thermal reaction device, it is characterized in that, comprise reactor body, described reactor body is column, be provided with in described reactor body and be oppositely arranged every predeterminable range between the upper and lower by the first transparency glass plate and the second transparency glass plate and sealed with the inwall of described reactor body the reaction chamber formed by black box, the upper end of described reactor body is provided with the first light illuminator, the lower end of described reactor body is provided with the second light illuminator, the sidewall of described reactor body is provided with reaction material entrance, described reaction material entrance communicates with the inside of described reaction chamber, the sidewall of described reactor body is provided with the installation of TC mouth, cooling tracheae installing port and heater installing port, described the installation of TC mouth, cooling tracheae installing port and heater installing port are connected with described reaction chamber respectively, described reactor body is also connected with pressure test device.
2. photochemical and thermal reaction device as claimed in claim 1, it is characterized in that, first and second light illuminator described and described reactor body are for being threaded.
3. photochemical and thermal reaction device as claimed in claim 2, it is characterized in that, the inside of first and second light illuminator described is provided with lamp panel, and on described lamp panel, annular is furnished with multiple lamp.
4. photochemical and thermal reaction device as claimed in claim 3, it is characterized in that, described lamp is LED.
5. photochemical and thermal reaction device as described in any one of Claims 1 to 4, it is characterized in that, described reactor body comprises reactor pars intermedia and the reactor top that is connected with described reactor pars intermedia and reactor lower part, described reactor top and described reactor pars intermedia are that detachable is connected, be integral type structure in the middle part of described reactor lower part and described reactor, described cooling tracheae installing port is located on the sidewall of described reactor lower part.
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CN201520224506.0U CN204656520U (en) | 2015-04-10 | 2015-04-10 | A kind of photochemical and thermal reaction device |
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CN201520224506.0U CN204656520U (en) | 2015-04-10 | 2015-04-10 | A kind of photochemical and thermal reaction device |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108261985A (en) * | 2018-01-17 | 2018-07-10 | 天津中环电炉股份有限公司 | A kind of horizontal-type high temperature photo-thermal catalytic reaction device |
CN110801788A (en) * | 2019-11-27 | 2020-02-18 | 北京昆仑永泰科技有限公司 | High-temperature high-pressure fixed bed reactor |
-
2015
- 2015-04-10 CN CN201520224506.0U patent/CN204656520U/en not_active Expired - Fee Related
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108261985A (en) * | 2018-01-17 | 2018-07-10 | 天津中环电炉股份有限公司 | A kind of horizontal-type high temperature photo-thermal catalytic reaction device |
CN110801788A (en) * | 2019-11-27 | 2020-02-18 | 北京昆仑永泰科技有限公司 | High-temperature high-pressure fixed bed reactor |
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GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150923 Termination date: 20190410 |
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CF01 | Termination of patent right due to non-payment of annual fee |