CN204613148U - A kind of stirring-type electrochemical deposition analytical equipment - Google Patents

A kind of stirring-type electrochemical deposition analytical equipment Download PDF

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Publication number
CN204613148U
CN204613148U CN201520289715.3U CN201520289715U CN204613148U CN 204613148 U CN204613148 U CN 204613148U CN 201520289715 U CN201520289715 U CN 201520289715U CN 204613148 U CN204613148 U CN 204613148U
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China
Prior art keywords
electrolytic cell
stirring
electrode
analytical equipment
electrochemical deposition
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Expired - Fee Related
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CN201520289715.3U
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Chinese (zh)
Inventor
白红亮
王俊生
王艳
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Individual
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Individual
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Priority to CN201520289715.3U priority Critical patent/CN204613148U/en
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Publication of CN204613148U publication Critical patent/CN204613148U/en
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Anticipated expiration legal-status Critical

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Abstract

The utility model relates to a kind of stirring-type electrochemical deposition analytical equipment, comprise bearing, be arranged on electrolytic cell bearing with cylindrical structure and the capping being arranged on electrolytic cell peristome, also comprise the stirring apparatus and heating arrangement that are arranged on electrolytic cell inside, described electrolytic cell comprise evenly be arranged on sidewall be respectively used to installment work electrode, auxiliary electrode and contrast electrode three electrode installing ports, be arranged on turbination structure bottom electrolytic cell precipitation discharge side and with the escape hole valve be connected bottom precipitation discharge side; Described electrode installing port comprise be arranged on peristome gland bonnet, be arranged on gland bonnet lower surface for the draw-in groove of fixed electorde and be embedded in draw-in groove by conducting strip that wire and external power source are electrically connected to each other.A kind of stirring-type electrochemical deposition analytical equipment described in the utility model, it is rational in infrastructure, and electrode is installed stable, heats, stirs, and is easy to collect gas and discharge sediment.

Description

A kind of stirring-type electrochemical deposition analytical equipment
Technical field
The utility model relates to electrochemical analysis device field, especially a kind of stirring-type electrochemical deposition analytical equipment.
Background technology
Electrochemical analysis device is the ideal tools of electrochemical analysis, research and teaching, can be widely used in each fields such as environment, the energy, material, biology, pharmacy and metallurgy.There is no stable electrode installing port in existing electrochemical analysis device, easily cause electrode instability or come off, the result that impact analysis detects, and sediment is difficult to discharge, impact analysis result.Meanwhile, do not have stirring apparatus, heat is uneven, also can the result of direct impact analysis, makes reappearance result poor.
Summary of the invention
The technical problems to be solved in the utility model is: in order to overcome above-mentioned middle Problems existing, and provide a kind of stirring-type electrochemical deposition analytical equipment, it is rational in infrastructure, and electrode is installed stable, heats, stirs, and is easy to collect gas and discharge sediment.
The utility model solves the technical scheme that its technical matters adopts: a kind of stirring-type electrochemical deposition analytical equipment, comprise bearing, be arranged on electrolytic cell bearing with cylindrical structure and the capping being arranged on electrolytic cell peristome, also comprise the stirring apparatus and heating arrangement that are arranged on electrolytic cell inside, described electrolytic cell comprises and is evenly arranged on sidewall and is respectively used to installment work electrode, three electrode installing ports of auxiliary electrode and contrast electrode, be arranged on turbination structure bottom electrolytic cell precipitation discharge side and with the escape hole valve that is connected bottom precipitation discharge side,
Described electrode installing port comprise be arranged on peristome gland bonnet, be arranged on gland bonnet lower surface for the draw-in groove of fixed electorde and be embedded in draw-in groove by conducting strip that wire and external power source are electrically connected to each other;
Described capping comprises the air guide face being arranged on gas collection mouth and motor mount that one end, capping upper surface and the electrolytic cell inner space other end be communicated with extraneous gas gathering-device and being inclined at lower surface.
Further, described heating arrangement comprises the annular mount pad that is arranged on electrolytic cell intracavity sidewall and is filled in the spiral heating wire be electrically connected to each other with external power source in annular mount pad.
Further, described stirring apparatus comprise vertically be arranged on electrolytic cell inside puddler, arrange capping top be rotatably installed in by bearing the reducing motor that is in transmission connection with puddler in axis hole and be arranged on establish bottom puddler have blade.
As preferred scheme, described electrolytic cell sidewall is also provided with the liquid injection port with inner space.
The beneficial effects of the utility model are: a kind of stirring-type electrochemical deposition analytical equipment, electrode installing port comprise be arranged on peristome gland bonnet, for the draw-in groove of fixed electorde and conducting strip, electrode is installed stable, capping upper surface has gas collection mouth and motor mount, the air guide face that lower surface has, be easy to collect gas, electrolytic cell inside has stirring apparatus and heating arrangement, heat, stir, there is bottom electrolytic cell the precipitation discharge side of turbination structure, easily discharge sediment.
Accompanying drawing explanation
Below in conjunction with drawings and Examples, the utility model is further illustrated.
Fig. 1 is a kind of stirring-type electrochemical deposition analytical equipment one-piece construction schematic diagram described in the utility model;
Fig. 2 is the electrode installing port structural representation of a kind of stirring-type electrochemical deposition analytical equipment described in the utility model.
Accompanying drawing acceptance of the bid note is described below: 1, bearing, and 2, electrolytic cell, 21, liquid injection port, 3, electrode installing port, 31, gland bonnet, 32, draw-in groove, 33, conducting strip, 34, wire, 4, capping, 41, air guide face, 42, motor mount, 43, axis hole, 5, precipitation discharge side, 51, escape hole valve, 6, gas collection mouth, 71, puddler, 72, reducing motor, 81, annular mount pad, 82, spiral heating wire.
Embodiment
By reference to the accompanying drawings the utility model is described in further detail now.These accompanying drawings are the schematic diagram of simplification, only basic structure of the present utility model are described in a schematic way, and therefore it only shows the formation relevant with the utility model.
A kind of stirring-type electrochemical deposition analytical equipment as shown in Figure 1, comprise bearing 1, be arranged on the electrolytic cell 2 bearing 1 with cylindrical structure and the capping 4 being arranged on electrolytic cell 2 peristome, also comprise the stirring apparatus and heating arrangement that are arranged on electrolytic cell 2 inside, described electrolytic cell 2 comprise evenly be arranged on sidewall be respectively used to installment work electrode, auxiliary electrode and contrast electrode three electrode installing ports 3, be arranged on turbination structure bottom electrolytic cell 2 precipitation discharge side 5 and with the escape hole valve 51 be connected bottom precipitation discharge side 5; Described capping 4 comprises the air guide face 41 being arranged on gas collection mouth 6 and motor mount 42 that one end, capping 4 upper surface and the electrolytic cell 2 inner space other end be communicated with extraneous gas gathering-device and being inclined at lower surface.Described heating arrangement comprises the annular mount pad 81 that is arranged on electrolytic cell 2 intracavity sidewall and is filled in the spiral heating wire 82 be electrically connected to each other with external power source in annular mount pad 81.Described stirring apparatus comprise vertically be arranged on electrolytic cell 2 inside puddler 71, arrange capping 4 top be rotatably installed in by bearing the reducing motor that is in transmission connection with puddler 71 in axis hole 43 and be arranged on establish bottom puddler 71 have blade 72.Described electrolytic cell 2 sidewall is also provided with the liquid injection port 21 with inner space.
A kind of stirring-type electrochemical deposition analytical equipment as shown in Figure 2, described electrode installing port 3 comprise be arranged on peristome gland bonnet 31, be arranged on gland bonnet 31 lower surface for the draw-in groove 32 of fixed electorde and be embedded in draw-in groove 32 by conducting strip 33 that wire 34 and external power source are electrically connected to each other.
A kind of stirring-type electrochemical deposition analytical equipment described in the utility model, electrode installing port 3 comprise be arranged on peristome gland bonnet 31, for the draw-in groove 32 of fixed electorde and conducting strip 33, electrode is installed stable, capping 4 upper surface has gas collection mouth 6 and motor mount 42, the air guide face that lower surface has 41, be easy to collect gas, electrolytic cell 2 inside has stirring apparatus and heating arrangement, heat, stir, there is bottom electrolytic cell 2 the precipitation discharge side 5 of turbination structure, easily discharge sediment.
With above-mentioned according to desirable embodiment of the present utility model for enlightenment, by above-mentioned description, relevant staff in the scope not departing from this utility model technological thought, can carry out various change and amendment completely.The technical scope of this utility model is not limited to the content on instructions, must determine its technical scope according to right.

Claims (4)

1. a stirring-type electrochemical deposition analytical equipment, comprise bearing (1), be arranged on the electrolytic cell (2) bearing (1) with cylindrical structure and the capping (4) being arranged on electrolytic cell (2) peristome, it is characterized in that: also comprise and be arranged on the inner stirring apparatus of electrolytic cell (2) and heating arrangement
Described electrolytic cell (2) comprises and is evenly arranged on sidewall and is respectively used to installment work electrode, three electrode installing ports (3) of auxiliary electrode and contrast electrode, the precipitation discharge side (5) being arranged on electrolytic cell (2) bottom turbination structure and the escape hole valve (51) be connected with precipitation discharge side (5) bottom;
Described electrode installing port (3) comprise be arranged on peristome gland bonnet (31), be arranged on gland bonnet (31) lower surface be used for fixed electorde draw-in groove (32) and be embedded in draw-in groove (32) by conducting strip (33) that wire (34) and external power source are electrically connected to each other;
Described capping (4) comprises the air guide face (41) being arranged on gas collection mouth (6) and motor mount (42) that capping (4) one end, upper surface and electrolytic cell (2) the inner space other end be communicated with extraneous gas gathering-device and being inclined at lower surface.
2. a kind of stirring-type electrochemical deposition analytical equipment according to claim 1, is characterized in that: described heating arrangement comprises the annular mount pad (81) that is arranged on electrolytic cell (2) intracavity sidewall and is filled in the spiral heating wire (82) be electrically connected to each other with external power source in annular mount pad (81).
3. a kind of stirring-type electrochemical deposition analytical equipment according to claim 1, is characterized in that: described stirring apparatus comprise vertically be arranged on the inner puddler (71) of electrolytic cell (2), arrange that capping (4) top is rotatably installed in by bearing the reducing motor that is in transmission connection with puddler (71) in axis hole (43) and is arranged on that puddler (71) bottom establishes have blade (72).
4. a kind of stirring-type electrochemical deposition analytical equipment according to claim 1, is characterized in that: described electrolytic cell (2) sidewall is also provided with and the liquid injection port of inner space (21).
CN201520289715.3U 2015-05-07 2015-05-07 A kind of stirring-type electrochemical deposition analytical equipment Expired - Fee Related CN204613148U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520289715.3U CN204613148U (en) 2015-05-07 2015-05-07 A kind of stirring-type electrochemical deposition analytical equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520289715.3U CN204613148U (en) 2015-05-07 2015-05-07 A kind of stirring-type electrochemical deposition analytical equipment

Publications (1)

Publication Number Publication Date
CN204613148U true CN204613148U (en) 2015-09-02

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Application Number Title Priority Date Filing Date
CN201520289715.3U Expired - Fee Related CN204613148U (en) 2015-05-07 2015-05-07 A kind of stirring-type electrochemical deposition analytical equipment

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112305052A (en) * 2020-10-10 2021-02-02 荷贝克电源系统(武汉)有限公司 Measuring device and method for measuring hydrogen evolution characteristics of lead storage battery negative electrode material

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112305052A (en) * 2020-10-10 2021-02-02 荷贝克电源系统(武汉)有限公司 Measuring device and method for measuring hydrogen evolution characteristics of lead storage battery negative electrode material
CN112305052B (en) * 2020-10-10 2024-05-14 荷贝克电源系统(武汉)有限公司 Measuring device and method for measuring hydrogen evolution characteristics of negative electrode material of lead storage battery

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150902

Termination date: 20160507