CN204490774U - A kind of preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate - Google Patents

A kind of preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate Download PDF

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CN204490774U
CN204490774U CN201520162007.3U CN201520162007U CN204490774U CN 204490774 U CN204490774 U CN 204490774U CN 201520162007 U CN201520162007 U CN 201520162007U CN 204490774 U CN204490774 U CN 204490774U
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hollow
rotating shaft
methylthio
hydroxy
colter
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周建康
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NINGBO TASHIJIE BIOLOGICAL TECHNOLOGY Co Ltd
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NINGBO TASHIJIE BIOLOGICAL TECHNOLOGY Co Ltd
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Abstract

The utility model discloses a kind of preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate, comprise drying installation, the mixing device of carry liquid spraying plant, screening plant and control device; Described mixing device is located in described drying installation; Described liquid dispensing apparatus is connected on described mixing device; The downside of described drying installation is located at by described screening plant; Described control device controls the work of drying installation, liquid dispensing apparatus, mixing device and screening plant.This preparation facilities is swift in response thoroughly, and product yield is high, and dry fast effectively energy consumption is low, and product impurity is few, and purity is high, reduces refuse exhaust gas emission, safety and environmental protection, easy to operate easy, shortened process.

Description

A kind of preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate
Technical field
The utility model relates to mechanical means, relates to a kind of preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate or rather.
Background technology
2-2-hydroxy-4-methylthio-Calcium Butyrate trade(brand)name is methionine hydroxy calcium again, as amino acids fodder additives, it is a kind of origin of amino acid of brilliance, effectively can be converted into methionine(Met) in animal body, for the synthesis of protein, improve growth of animal rate and laying rate of poultry, and be again a kind of organic calcium of high-quality simultaneously, for animal growth provides the calcium source of high-quality, there is good economic benefit.The preparation method of this 2-2-hydroxy-4-methylthio-Calcium Butyrate has the advantages such as technical process is short, facility investment is few, production cost is low, and finished product is pressed powder, easy to use, wide application, without the need to Special feeding system, is a kind of excellent methionine(Met) substitute.At present, the preparation process of 2-2-hydroxy-4-methylthio-Calcium Butyrate has been come by combination drying machine, namely in combination drying machine, calcium oxide or calcium hydroxide is added, adopt continuous small dose to add 2-2-hydroxy-4-methylthio-butyric acid solution subsequently, make it that neutralization reaction occur and generate 2-2-hydroxy-4-methylthio-Calcium Butyrate.Prepare 2-2-hydroxy-4-methylthio-Calcium Butyrate by current combination drying machine and there is following defect: the calcium oxide of solid state or calcium hydroxide start to be difficult to mix with the 2-2-hydroxy-4-methylthio-butyric acid solution of liquid state, reaction is also difficult to, but once both react, reaction will be very violent, speed of response is very fast again, will increase sharply in reaction vessel can be made on the one hand, and produce a large amount of heats, thus cause speed of response, pressure and temperature is difficult to control, and after temperature is greater than 130 degree, product 2-2-hydroxy-4-methylthio-Calcium Butyrate can occur to decompose or coking, on the other hand, part material (as calcium oxide or calcium hydroxide or intermediate product etc.) is as easy as rolling off a log is packed to agglomerate or bulk, fully cannot participate in reaction, cause reaction raw materials amount relative deficiency, react insufficient, intermediate product is more, product purity is not high, thus affect efficiency of pcr product and quality.And after material is packed to agglomerate or bulk, the moisture of the inside is difficult to be evaporated when drying, affects material volume drying, makes the dry materials time greatly extend, and causes the whole production time long, affects output.
Utility model content
The technical problems to be solved in the utility model is, there is provided a kind of preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate, this preparation facilities is swift in response thoroughly, and product yield is high, dry effective fast, energy consumption is low, and product impurity is few, and purity is high, reduce refuse exhaust gas emission, safety and environmental protection, easy to operate easy, shortened process.
Technical solution of the present utility model is, provides a kind of preparation facilities with the 2-hydroxy-4-(methylthio) base-Calcium Butyrate of following structure, comprises drying installation, the mixing device of carry liquid spraying plant, screening plant and control device; Described mixing device is located in described drying installation; Described liquid dispensing apparatus is connected on described mixing device; The downside of described drying installation is located at by described screening plant; Described control device controls the work of drying installation, liquid dispensing apparatus, mixing device and screening plant.
After adopting above structure, the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate of the present utility model, compared with prior art, has the following advantages:
Because the preparation facilities collection of 2-hydroxy-4-(methylthio) base-Calcium Butyrate of the present utility model reacts, mixing, dry, the several functions such as screening are in one, during use, solid materials calcium oxide or calcium hydroxide are joined in drying installation in advance, during the work of this preparation facilities, liquid material 2-2-hydroxy-4-methylthio-butyric acid solution is injected in drying installation by liquid dispensing apparatus, and the solid materials drive in drying installation also can be flown upward by mixing device work, thus make solid materials and object material form spray in drying installation, carry out abundant hybrid reaction, add the point of contact between reaction mass and contact surface, thus can make to react more fully and completely between reaction mass.Reaction mass forms raw product after reacting in drying installation, then the effect by drying installation and mixing device is carried out fully and mixing and drying rapidly, highly purified 2-hydroxy-4-(methylthio) base-Calcium Butyrate product can be made, last again by the sieving action of screening plant, finally obtain 2-hydroxy-4-(methylthio) base-Calcium Butyrate finished product.Preparing 2-hydroxy-4-(methylthio) base-Calcium Butyrate by the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate of the present utility model makes reactant reaction thorough rapidly, and product yield is high; Dry effective fast, energy consumption is low; Product impurity is few, and purity is high, effectively improves the quality of products; Reduce the discharge of waste gas and wastes, effectively can alleviate environmental pollution; Working method is easy, shortened process, can reduce facility investment, reduces production cost.
Improve as one of the present utility model, described drying installation comprises dry cylindrical shell; The barrel of described dry cylindrical shell comprises stainless-steel sheet layer, steel plate layer and heating jacket from inside to outside.After adopting this kind of structure, described stainless-steel sheet layer has corrosion resistant effect; Described steel plate layer can increase mechanical rigid and intensity; Described heating jacket has heating and regulates the effect of temperature.
Improve as another kind of the present utility model, described mixing device comprises hollow rotating shaft and rotating shaft driving device; Described hollow rotating shaft is connected with described rotating shaft driving device, and this rotating shaft driving device is electrically connected with described control device; Described hollow rotating shaft is axially located in described dry cylindrical shell along dry cylindrical shell; On described hollow rotating shaft, radial direction is provided with multiple hollow colter; The inner chamber of described hollow rotating shaft and the intracavity inter-connection of described hollow colter; Described hollow rotating shaft is connected with described liquid dispensing apparatus; Several spray holes are equipped with on the sidewall of described hollow rotating shaft and on the sidewall of hollow colter.After adopting this kind of structure, material is ejected in dry housing by liquid dispensing apparatus and material spray hole and forms spray, increase the point of contact between material and contact surface, reaction mass epidemic situation comparison is loose, can not form or be packed to agglomerate or bulk, thus can make to react between reaction mass more thorough more rapidly, also reduce the heat in dry housing and pressure simultaneously, also can improve the quality of product.In addition, adopt plough coulter type mixing device stirring intensity higher, make the effect of mixing better.
Also have a kind of improvement as of the present utility model, described hollow colter comprises the bright and hollow coulter of hollow colter; One end that described hollow colter is bright is connected with hollow rotating shaft; The other end that described hollow colter is bright is connected with hollow coulter; Described hollow coulter is berrette file shape or flat ellipse shape; The described bright inner chamber of hollow colter, hollow coulter inner chamber and hollow rotating shaft inner chamber are interconnected; The spray holes described in several is equipped with on the sidewall that described hollow colter is bright and on the sidewall of hollow coulter.After adopting this kind of structure, effectively can strengthen the bright physical strength of colter, greatly reduce the resistance that in mixing process, colter produces, solve the problems such as the bending or fracture of colter in mixing or drying process, increase again the different flow direction of material, material is constantly stirred, convection current and diffusion, thus increased substantially material point of contact each other and contact surface, improve the effect of mixing of materials reaction and follow-up drying.
Also have a kind of improvement as of the present utility model, described screening plant comprises screening housing; Described screening housing is located at the downside of described drying installation; At least one deck sieve plate or screen cloth is provided with in this screening housing.After adopting this kind of structure, globule size and the screening speed of material can be controlled.
Also have a kind of improvement as of the present utility model, the upside of described dry cylindrical shell is provided with liquid spray room; The sidewall of described liquid spray room is provided with multiple fog-spray nozzle and the fog nozzle of the plurality of fog-spray nozzle is indoor towards liquid spray; Multiple described fog-spray nozzle is all connected with atomizing pump by pipeline.After adopting this kind of structure, part liquid material sprays from the liquid spray room of the upside of dry cylindrical shell, mix with the solid materials in dry cylindrical shell, can further improve material point of contact each other and contact surface like this, improve the effect of mixing of materials reaction and follow-up drying further.
Accompanying drawing explanation
Fig. 1 is the structural representation of the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate of the present utility model.
Fig. 2 is the structural representation of the liquid spray room of the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate of the present utility model.
Shown in figure: 1, dry cylindrical shell, 2, hollow rotating shaft, 3, rotating shaft driving device, 4, hollow colter, 4.1, hollow coulter shank, 4.2, hollow coulter, 5, material spray hole, 6, housing is sieved, 7, sieve plate/screen cloth, 8, liquid spray room, 9, fog-spray nozzle, 10, atomizing pump, 11, water evaporation device, 12, gas collector.
Embodiment
Below in conjunction with the drawings and specific embodiments, the utility model is described in further detail.
Refer to shown in Fig. 1, the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate of the present utility model, is characterized in that: comprise drying installation, the mixing device of carry liquid spraying plant, screening plant and control device; Described mixing device is located in described drying installation; Described liquid dispensing apparatus is connected on described mixing device; The downside of described drying installation is located at by described screening plant; Described control device controls the work of drying installation, liquid dispensing apparatus, mixing device and screening plant.
Described drying installation comprises dry cylindrical shell 1; The barrel of described dry cylindrical shell 1 comprises stainless-steel sheet layer, steel plate layer and heating jacket from inside to outside.Described stainless-steel sheet layer is rolled by stainless-steel sheet and forms.Described steel plate layer is rolled by steel plate and forms.
Described mixing device comprises hollow rotating shaft 2 and rotating shaft driving device 3; Described hollow rotating shaft 2 is connected with described rotating shaft driving device 3, and this rotating shaft driving device 3 is electrically connected with described control device; Described hollow rotating shaft is axially located in described dry cylindrical shell along dry cylindrical shell; On described hollow rotating shaft 2, radial direction is provided with multiple hollow colter 4; The inner chamber of described hollow rotating shaft 2 and the intracavity inter-connection of described hollow colter 4; Described hollow rotating shaft 2 is connected with described liquid dispensing apparatus 8; Several spray holes 5 are equipped with on the sidewall of described hollow rotating shaft 2 and on the sidewall of hollow colter 4.The flow of described liquid dispensing apparatus 8 controllable liquid, speed and state, thus control the speed of whole reaction, intensity and state.
Described hollow colter 4 comprises hollow colter bright 4.1 and hollow coulter 4.2; One end of described hollow colter bright 4.1 is connected with hollow rotating shaft 2; The other end of described hollow colter bright 4.1 is connected with hollow coulter 4.2; Described hollow coulter 4.2 is berrette file shape or flat ellipse shape; Bright 4.1 inner chambers of described hollow colter, hollow coulter 4.2 inner chamber and hollow rotating shaft 2 inner chamber are interconnected; The spray holes 5 described in several is equipped with on the sidewall of described hollow colter bright 4.1 and on the sidewall of hollow coulter 4.2.
Described screening plant comprises screening housing 6; Described screening housing 6 is located at the downside of described dry cylindrical shell 1; At least one deck sieve plate or screen cloth 7 is provided with in this screening housing 6.
See also shown in Fig. 2, the upside of described dry cylindrical shell 1 is provided with liquid spray room 8; The sidewall of described liquid spray room 8 be provided with multiple fog-spray nozzle 9 and the fog nozzle of the plurality of fog-spray nozzle 9 towards in liquid spray room 8; Multiple described fog-spray nozzle 9 is all connected with atomizing pump 10 by pipeline.
The upside of the drying installation of the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate of the present utility model is also provided with water evaporation device 11, gas collector 12 and well heater, react and the water evaporation that produces or other gas in drying process for controlling, thus indirectly control speed and the intensity of reaction.Described water evaporation device is connected respectively at described drying installation with gas collector.Described well heater is for heating heat-conducting medium.
The working process of the preparation facilities of the utility model 2-hydroxy-4-(methylthio) base-Calcium Butyrate is as follows: solid materials calcium oxide or calcium hydroxide are joined in advance in drying installation in advance before use.During the work of this preparation facilities, liquid material 2-2-hydroxy-4-methylthio-butyric acid solution is injected in dry cylindrical shell by liquid dispensing apparatus, and the solid materials drive in dry cylindrical shell also can be flown upward by hollow rotating shaft work, thus make solid materials and object material form spray in dry cylindrical shell, carry out abundant hybrid reaction, the 2-hydroxy-4-(methylthio) base-Calcium Butyrate raw product of production high density; Raw product carries out short mix and rapid drying through dry cylindrical shell and mixing device again, makes highly purified 2-hydroxy-4-(methylthio) base-Calcium Butyrate product; Again by the sieving action of screening plant, finally obtain 2-hydroxy-4-(methylthio) base-Calcium Butyrate finished product.

Claims (6)

1. a preparation facilities for 2-hydroxy-4-(methylthio) base-Calcium Butyrate, is characterized in that: comprise drying installation, the mixing device of carry liquid spraying plant, screening plant and control device; Described mixing device is located in described drying installation; Described liquid dispensing apparatus is connected on described mixing device; The downside of described drying installation is located at by described screening plant; Described control device controls the work of drying installation, liquid dispensing apparatus, mixing device and screening plant.
2. the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate according to claim 1, is characterized in that: described drying installation comprises dry cylindrical shell (1); The barrel of described dry cylindrical shell (1) comprises stainless-steel sheet layer, steel plate layer and heating jacket from inside to outside.
3. the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate according to claim 2, is characterized in that: described mixing device comprises hollow rotating shaft (2) and rotating shaft driving device (3); Described hollow rotating shaft (2) is connected with described rotating shaft driving device (3), and this rotating shaft driving device (3) is electrically connected with described control device; Described hollow rotating shaft is axially located in described dry cylindrical shell along dry cylindrical shell; The upper radial direction of described hollow rotating shaft (2) is provided with multiple hollow colter (4); The inner chamber of described hollow rotating shaft (2) and the intracavity inter-connection of described hollow colter (4); Described hollow rotating shaft (2) is connected with described liquid dispensing apparatus (8); Several spray holes (5) are equipped with on the sidewall of described hollow rotating shaft (2) and on the sidewall of hollow colter (4).
4. the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate according to claim 3, is characterized in that: described hollow colter (4) comprises hollow colter bright (4.1) and hollow coulter (4.2); One end of described hollow colter bright (4.1) is connected with hollow rotating shaft (2); The other end of described hollow colter bright (4.1) is connected with hollow coulter (4.2); Described hollow coulter (4.2) is berrette file shape or flat ellipse shape; Described hollow colter bright (4.1) inner chamber, hollow coulter (4.2) inner chamber and hollow rotating shaft (2) inner chamber are interconnected; The spray holes (5) described in several is equipped with on the sidewall of described hollow colter bright (4.1) and on the sidewall of hollow coulter (4.2).
5. the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate according to claim 1, is characterized in that: described screening plant comprises screening housing (6); Described screening housing (6) is located at the downside of described drying installation; At least one deck sieve plate or screen cloth (7) is provided with in this screening housing (6).
6. the preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate according to claim 3, is characterized in that: the upside of described dry cylindrical shell (1) is provided with liquid spray room (8); The sidewall of described liquid spray room (8) be provided with multiple fog-spray nozzle (9) and the fog nozzle of the plurality of fog-spray nozzle (9) towards in liquid spray room (8); Multiple described fog-spray nozzle (9) is all connected with atomizing pump (10) by pipeline.
CN201520162007.3U 2015-03-20 2015-03-20 A kind of preparation facilities of 2-hydroxy-4-(methylthio) base-Calcium Butyrate Active CN204490774U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104725290A (en) * 2015-03-20 2015-06-24 宁波它世界生物科技有限公司 Preparation device of calcium 2-hydroxy-4-methylthio-butyrate
CN106839700A (en) * 2017-02-10 2017-06-13 徐州新南湖科技有限公司 A kind of dendrobium candidum screw propulsion solid dielectric drying unit
CN113171705A (en) * 2020-11-22 2021-07-27 湖南贝爱成食品有限公司 Workshop is with mixed machine of flavouring of fast food

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104725290A (en) * 2015-03-20 2015-06-24 宁波它世界生物科技有限公司 Preparation device of calcium 2-hydroxy-4-methylthio-butyrate
CN106839700A (en) * 2017-02-10 2017-06-13 徐州新南湖科技有限公司 A kind of dendrobium candidum screw propulsion solid dielectric drying unit
CN113171705A (en) * 2020-11-22 2021-07-27 湖南贝爱成食品有限公司 Workshop is with mixed machine of flavouring of fast food

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