CN204417390U - A kind of PAM reactor - Google Patents

A kind of PAM reactor Download PDF

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Publication number
CN204417390U
CN204417390U CN201420867371.5U CN201420867371U CN204417390U CN 204417390 U CN204417390 U CN 204417390U CN 201420867371 U CN201420867371 U CN 201420867371U CN 204417390 U CN204417390 U CN 204417390U
Authority
CN
China
Prior art keywords
tank
reactor
reactive tank
reactive
pam
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420867371.5U
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Chinese (zh)
Inventor
马帅
尹楠
郭超
董本芬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui University of Science and Technology
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Anhui University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui University of Science and Technology filed Critical Anhui University of Science and Technology
Priority to CN201420867371.5U priority Critical patent/CN204417390U/en
Application granted granted Critical
Publication of CN204417390U publication Critical patent/CN204417390U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of PAM reactor, belong to macromolecule synthesising technology field, be specifically related to a kind of laboratory that solves at synthesis polyacrylamide poor product quality, the unmanageable reactor of experiment condition.This reactor mainly comprises tank body, reactive tank, ultraviolet lamp, vacuum orifice, tail gas mouth.This reactor is according to light-initiated aqueous solution polymerization method, first the test tube that reaction stoste is housed is added in reactive tank, synthesis polyacrylamide is caused by illumination in airtight vacuum environment, overcome product in conventional synthesis process easily oxidized, reactant is volatile, the shortcoming of toxic gas diffusion, thus improve the quality product of polyacrylamide.

Description

A kind of PAM reactor
Technical field
The utility model relates to a kind of light-initiated synthesis device, particularly relates to the light-initiated synthesizer of a kind of polyacrylamide.
Background technology:
Along with industrial development, water pollution problems is further serious, current water treatment procedure many employings polyacrylamide is as flocculation agent, and the character of polyacrylamide directly affects industrial production efficiency and economic benefit, so the synthesis condition improving polyacrylamide is an important step of improving the quality of products.
But the production technique of polyacrylamide falls behind at present, poor product quality is low in economic efficiency, and reason is a series of defects such as the synthesis condition of polyacrylamide is difficult to control, and process is unstable, generation toxic gas is difficult.
Real novel content:
It is simple that the purpose of this utility model is to provide a kind of structure, and the polyacrylamide amine reactor of operating aspect, this reactor building-up process is easy to control, and environmental pollution is little, sintetics steady quality.
For achieving the above object, the technical solution adopted in the utility model is: a kind of PAM reactor, is characterized in that:
Tank body (1) is hollow cylinder shape, for providing reacting environment;
Reactive tank one (2), reactive tank two (3), reactive tank three (4), reactive tank four (5), four hollow cylinder shape reactive tanks are evenly fixed on tank interior, for placing glass test tube;
Sealing cover (6), circular sealing cover is connected to vessel edge, for sealed shell of tank by bolt able to turn on or off;
Vacuum orifice (7), for hollow circuit cylinder pipeline is laterally fixed on tank body upper center, for being evacuated by reactor;
Ultraviolet lamp (8), cylindrical ultraviolet lamp tube, can put in the middle part of tank body, provide light source.
Preferably, reactive tank one (2), reactive tank two (3), reactive tank three (4), reactive tank four (5) that distribution four internal diameters in described tank body (1) inside are identical, upper right side is venting port (9);
Preferably, be vacuum orifice (7) in the middle of described sealing cover (6) upper end, ultraviolet lamp tube (8) is installed in inner side.Principle of work:
The utility model is the polyacrylamide reaction solution initiated polymerization utilizing UV-irradiation to add light trigger, for preventing being oxidized in reaction process, carrying out, stablize reaction conditions in the environment vacuumized, and collects obnoxious flavour at venting port.
Compared with prior art, the utility model has the advantages that:
By the irradiation synthesis polyacrylamide of ultraviolet lamp in airtight vacuum environment, overcome traditional product easily oxidized, reactant is volatile, the shortcoming of the toxic gas diffusion that product generates, thus substantially increase the quality product of polyacrylamide, reduce the injury to experimenter and environmental pollution simultaneously.
Accompanying drawing explanation
Fig. 1 is a kind of PAM reactor schematic diagram of the present utility model.
Fig. 2 is reactor tank body inside top figure of the present utility model.
In Fig. 1: tank body-1, reactive tank-2,3, sealing cover-6, vacuum orifice-7, ultraviolet lamp-8, venting port-9.
In Fig. 2: reactive tank-2,3,4,5, ultraviolet lamp-8.
Embodiment
For making the purpose of this utility model, technical scheme and advantage clearly, below in conjunction with the drawings and specific embodiments, the utility model is described in further detail:
As shown in Figure 1, a kind of PAM reactor, it comprises following integral part:
Tank body 1 is hollow cylinder shape, for providing reacting environment;
Reactive tank 1, reactive tank 23, reactive tank 34, reactive tank 45, four hollow cylinder shape reactive tanks are evenly fixed on tank interior, for placing glass test tube;
Sealing cover 6, circular sealing cover is connected to vessel edge, for sealed shell of tank by bolt able to turn on or off;
Vacuum orifice 7, for hollow circuit cylinder pipeline is laterally fixed on tank body upper center, for being evacuated by reactor;
Ultraviolet lamp 8, cylindrical ultraviolet lamp tube, can put in the middle part of tank body, provide light source.
Preferably, reactive tank 1, reactive tank 23, reactive tank 34, reactive tank 45 that distribution four internal diameters in tank body 1 inside are identical, upper right side is venting port 9;
Preferably, be vacuum orifice 7 in the middle of sealing cover 6 upper end, ultraviolet lamp tube 8 is installed in inner side.
Middle Fig. 1 is described working process of the present utility model by reference to the accompanying drawings:
First, open sealing cover 6, added by the test tube that polyacrylamide reaction solution is housed in reactive tank 2,3,4,5, close upper right side venting port 9, to be connected with vacuum orifice 7 by vacuum pump and to be evacuated by tank body 1, unlatching ultraviolet lamp 8 carries out light-induced polymerization.After for some time, question response terminates, and closes ultraviolet lamp 8, is connected by venting port 9 and carries out vent gas treatment, open sealing cover 6 and take out product with air-washer, and reaction terminates.
The above is illustrative instead of determinate, therefore in the change do not departed under the utility model overall structure and amendment, should belong within protection domain of the present utility model.

Claims (3)

1. PAM reactor mainly comprises a following integral part, it is characterized in that:
Tank body (1) is hollow cylinder shape, for providing reacting environment;
Reactive tank one (2), reactive tank two (3), reactive tank three (4), reactive tank four (5), four hollow cylinder shape reactive tanks are evenly fixed on tank interior, for placing glass test tube;
Sealing cover (6), circular sealing cover is connected to vessel edge, for sealed shell of tank by bolt able to turn on or off;
Vacuum orifice (7), for hollow circuit cylinder pipeline is laterally fixed on tank body upper center, for being evacuated by reactor;
Ultraviolet lamp (8), cylindrical ultraviolet lamp tube, can put in the middle part of tank body, provide light source.
2. a kind of PAM reactor according to claim 1, it is characterized in that: the distribution of described tank body (1) inside reactive tank one (2), reactive tank two (3), reactive tank three (4), reactive tank four (5), upper right side is venting port (9).
3. a kind of PAM reactor according to claim 1, is characterized in that: be vacuum orifice (7) in the middle of described sealing cover (6) upper end, ultraviolet lamp tube (8) is installed in inner side.
CN201420867371.5U 2014-12-31 2014-12-31 A kind of PAM reactor Expired - Fee Related CN204417390U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420867371.5U CN204417390U (en) 2014-12-31 2014-12-31 A kind of PAM reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420867371.5U CN204417390U (en) 2014-12-31 2014-12-31 A kind of PAM reactor

Publications (1)

Publication Number Publication Date
CN204417390U true CN204417390U (en) 2015-06-24

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201420867371.5U Expired - Fee Related CN204417390U (en) 2014-12-31 2014-12-31 A kind of PAM reactor

Country Status (1)

Country Link
CN (1) CN204417390U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108607487A (en) * 2018-04-03 2018-10-02 安徽理工大学 A kind of New Polyacrylamide synthesizer
CN109053954A (en) * 2018-05-31 2018-12-21 义乌市鹏之友新材料有限公司 A kind of visible light Photoreactor and its application method being exclusively used in cationic polyacrylamide polymerization

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108607487A (en) * 2018-04-03 2018-10-02 安徽理工大学 A kind of New Polyacrylamide synthesizer
CN109053954A (en) * 2018-05-31 2018-12-21 义乌市鹏之友新材料有限公司 A kind of visible light Photoreactor and its application method being exclusively used in cationic polyacrylamide polymerization

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150624

Termination date: 20151231

EXPY Termination of patent right or utility model