CN204369708U - A kind of device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water - Google Patents

A kind of device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water Download PDF

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CN204369708U
CN204369708U CN201420781302.2U CN201420781302U CN204369708U CN 204369708 U CN204369708 U CN 204369708U CN 201420781302 U CN201420781302 U CN 201420781302U CN 204369708 U CN204369708 U CN 204369708U
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ultrasonic
tank
ultrasonic heating
ultrasonic tank
water
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樊栓狮
张雯翔
王燕鸿
郎雪梅
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South China University of Technology SCUT
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South China University of Technology SCUT
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Abstract

The utility model discloses a kind of device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water.Described device comprises water inlet pipe, raw water pump, deionization apparatus, Ultrasonic Heating equipment, rising pipe; Water inlet pipe is connected in turn with raw water pump, deionization apparatus, Ultrasonic Heating equipment, rising pipe; Described deionization apparatus is made up of activated charcoal filter, reverse osmosis membrane assembly and mixed bed, and described activated charcoal filter is connected in turn with reverse osmosis membrane assembly, mixed bed; Ultrasonic Heating equipment is made up of the first ultrasonic tank, the second ultrasonic tank, Ultrasonic Heating groove, hot bath device and the 3rd ultrasonic tank, wherein the first ultrasonic tank is connected in turn with the second ultrasonic tank, Ultrasonic Heating groove and the 3rd ultrasonic tank, and hot bath device and Ultrasonic Heating groove to be connected the utility model preparation method simple, energy operate continuously, circulation is large, good economy performance; The small-micelle water cluster molecule of preparation is few, and rate of permeation is high, is easy to absorb, and can keep the characteristic of small-micelle water for a long time, good stability simultaneously.

Description

A kind of device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water
Technical field
The utility model relates to the device preparing small-micelle water, is specifically related to a kind of device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water.
Background technology
Water is elementary composition by hydrogen-oxygen two kinds, and it is the valuable source comprising inorganic chemical, all life existence of the mankind, is also the most important integral part of organism.For human body, water is the important substance being only second to oxygen.Glassware for drinking water have dissolve digestion, participate in metabolism, carrier transport, regulate suppress, lubrication is moistened, dilution and the function such as toxin expelling.Water exists with cluster form, its cluster number of the most of water of nature is 10-13, and only have when the cluster molecule number of water reduces to 5-9, just form our said small-micelle water, result of study is had to show: to only have small-micelle water just by the human body cell ionic channel of 2 nanometers, enter nucleus and DNA, active cells enzyme tissue, excite vitality, and other tap water, pure water all cannot be entered in cell by ionic channel.Each Cell uptake and utilization in the easy body of micromolecular water; Strengthen metabolic efficiency and function; Strengthen each cell and the inter-agency information transmission of surrounding tissue; The obvious nutrition of whole body material that improves transmits supply; Improve the transportcapacity of whole body oxygen; Promote the discharge of refuse and toxin in cell; Promote the transmission of normal gene information.Small-micelle water is healthy water, the water of life.
Hydrogen bond is a kind of slightly stronger than Intermolecular Forces (Van der Waals force), than covalent linkage and the weak interaction much of ionic linkage.Its stability is weaker than covalent linkage and ionic linkage.In liquid water, combined by stronger hydrogen bond action between several water molecules, namely molecular association occurs, form the molecular cluster of (H2O) n.Between water molecules, hydrogen bond Average bond energy is 21kJ/mol, when temperature, pressure change or by External Force Acting, provide the hydrogen bond between extra energy damages water molecules, and the chemical bond in water molecules is not destroyed, and can obtain the small-micelle water that cluster number is less.
Pass through external energy, realize the change of water molecule cluster number, at present, some investigators utilize electrolysis tech, far-infrared technique, nanotechnology, Refrigeration Technique to produce micromolecular water, its micromolecular water poor stability prepared, returns to again macromolecular mass tufted state after long-time placement; Can not continuity operation, production efficiency is low, less economical, prepares length consuming time, day can treatment capacity little.
Utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art, by ultrasonic and heat effect, provides a kind of and continuity operation, formation efficiency high, good economy performance, day output small-micelle water that is large, good stability can make device and method.
The purpose of this utility model is reached by following measure:
Utilize Ultrasonic Heating technology to prepare a device for stable micro-molecular group water, described device comprises water inlet pipe, raw water pump, deionization apparatus, Ultrasonic Heating equipment and rising pipe; Described water inlet pipe is connected in turn with raw water pump, deionization apparatus, Ultrasonic Heating equipment, rising pipe; Described deionization apparatus is made up of activated charcoal filter, reverse osmosis membrane assembly and mixed bed, and described activated charcoal filter is connected in turn with reverse osmosis membrane assembly, mixed bed; Described Ultrasonic Heating equipment is made up of the first ultrasonic tank, the second ultrasonic tank, Ultrasonic Heating groove, hot bath device and the 3rd ultrasonic tank, wherein the first ultrasonic tank is connected in turn with the second ultrasonic tank, Ultrasonic Heating groove and the 3rd ultrasonic tank, and hot bath device is connected with Ultrasonic Heating groove.
In said apparatus, described device also comprises magnetic valve and controlling box; Described magnetic valve is connected between raw water pump and deionization apparatus; Described controlling box is connected with raw water pump, magnetic valve, activated charcoal filter, reverse osmosis membrane assembly, mixed bed, the first ultrasonic tank, the second ultrasonic tank, Ultrasonic Heating groove, hot bath device, the 3rd ultrasonic tank respectively by signal wire; Described controlling box, by regulation and control raw water pump, magnetic valve, controls raw water flow; Described controlling box, by activated charcoal filter, reverse osmosis membrane assembly, mixed bed in regulation and control deionization apparatus, controls the conductivity value of deionized water; Described controlling box is by regulating and controlling the ultrasound resonance frequency of the first ultrasonic tank, the second ultrasonic tank, Ultrasonic Heating groove, the 3rd ultrasonic tank in Ultrasonic Heating equipment and ultrasonic duration, and the heating ramp rate of regulation and control hot bath device, controls Ultrasonic Heating process.
In said apparatus, the first described ultrasonic tank, the second ultrasonic tank, Ultrasonic Heating groove, the 3rd ultrasonic tank volume are 5 ~ 100L.
Utilize Ultrasonic Heating technology to prepare a using method for the device of stable micro-molecular group water, comprise the following steps:
A. pass in described device by former water by water inlet pipe, water, sequentially by raw water pump and magnetic valve, flows through deionization apparatus and Ultrasonic Heating equipment, is flowed out by rising pipe;
B. controlling box electromagnetic valve for adjusting, raw water pump draws water, and controls at 0.5 ~ 10L/min by the volumetric flow rate of water in water inlet pipe;
C. controlling box regulation and control deionization apparatus, the conductivity value controlling deionized water is less than 10 us/cm;
D. controlling box regulation and control Ultrasonic Heating equipment, the resonant frequency controlling supersound process is 20 ~ 20000kHz, and total ultrasonic duration is 8 ~ 800min/L;
E. controlling box regulation and control hot bath device, controlling Ultrasonic Heating groove temperature rise rate is 0.5 ~ 15 K/min, is down to room temperature rapidly after the 2 ~ 140min that heats up, and again with the heating of the temperature rise rate of 0.5 ~ 15 K/min, heat-processed so circulates;
F. Ultrasonic Heating equipment water outlet is connected with rising pipe, and water outlet naturally cools to room temperature, the obtained small-micelle water with small molecules clustering properties.
In aforesaid method, deionization apparatus water outlet gained deionization electrical conductivity of water is less than 10 us/cm.
In aforesaid method, the molecular cluster of described small-micelle water is 4 ~ 8 water moleculess.
In aforesaid method, described small-micelle water at room temperature places 12 months, and its water molecule cluster still remains on 4 ~ 8 water moleculess.
The beneficial effects of the utility model are:
The utility model apparatus structure is simple, fully utilize ultrasonic and heat effect, have can continuity operation, the advantage such as formation efficiency is high, good economy performance, day output are large, solve other device and prepare the bad defect of products obtained therefrom (small-micelle water) stability.Under heating acts on mutually with ultrasonic friendship, the energy outside the amount of imports, the hydrogen bond between water molecules is destroyed, and makes the small-micelle water had good stability, and the utility model small-micelle water making method simply, can consecutive production, and energy consumption is low, good economy performance; The small-micelle water that the utility model makes, water sample 17o NMR peak width at half height numerical value is low, good stability, can maintain micromolecular water characteristic for a long time, can be used for the condition that need keep small-micelle water characteristic for a long time, as makeup, bottled canned tap water, medical in.
Accompanying drawing explanation
Fig. 1 is that the utility model utilizes Ultrasonic Heating technology to prepare the structural representation of stable micro-molecular group water device.
Water inlet pipe 1, raw water pump 2, magnetic valve 3, activated charcoal filter 4, reverse osmosis membrane assembly 5, mixed bed 6, first ultrasonic tank 7, second ultrasonic tank 8, Ultrasonic Heating groove 9, hot bath device 10, the 3rd ultrasonic tank 11, controlling box 12, rising pipe 13.
Embodiment
Following examples are to the further detailed analysis of the utility model, but embodiment of the present utility model is not limited thereto.
As shown in Figure 1, its annexation for: a kind of utilize Ultrasonic Heating technology prepare stable micro-molecular group water device described in device comprise water inlet pipe 1, raw water pump 2, deionization apparatus, Ultrasonic Heating equipment, rising pipe 13; Described water inlet pipe 1 is connected in turn with raw water pump 2, deionization apparatus, Ultrasonic Heating equipment, rising pipe 13; Described deionization apparatus is made up of activated charcoal filter 4, reverse osmosis membrane assembly 5 and mixed bed 6, and described activated charcoal filter 4 is connected in turn with reverse osmosis membrane assembly 5, mixed bed 6; Described Ultrasonic Heating equipment is made up of the first ultrasonic tank 7, second ultrasonic tank 8, Ultrasonic Heating groove 9, hot bath device 10 and the 3rd ultrasonic tank 11, wherein the first ultrasonic tank 7 is connected in turn with the second ultrasonic tank 8, Ultrasonic Heating groove 9 and the 3rd ultrasonic tank 11, and hot bath device 10 is connected with Ultrasonic Heating groove 9.Described device also comprises magnetic valve 3 and controlling box 12; Described magnetic valve 3 is connected between raw water pump 2 and deionization apparatus; Described controlling box 12 is connected with raw water pump 2, magnetic valve 3, activated charcoal filter 4, reverse osmosis membrane assembly 5, mixed bed 6, first ultrasonic tank 7, second ultrasonic tank 8, Ultrasonic Heating groove 9, hot bath device 10, the 3rd ultrasonic tank 11 respectively by signal wire; Described controlling box 12, by regulation and control raw water pump 2, magnetic valve 3, controls raw water flow; Described controlling box 12, by activated charcoal filter 4, reverse osmosis membrane assembly 5, mixed bed 6 in regulation and control deionization apparatus, controls the conductivity value of deionized water; Described controlling box 12 is by regulating and controlling the ultrasound resonance frequency of the first ultrasonic tank 7, second ultrasonic tank 8, Ultrasonic Heating groove 9, the 3rd ultrasonic tank 11 in Ultrasonic Heating equipment and ultrasonic duration, and the heating ramp rate of regulation and control hot bath device 10, controls Ultrasonic Heating process.
Utilize said apparatus to prepare the method for stable micro-molecular group water, it comprises the following steps: former water passes in described device by water inlet pipe by a., and water, sequentially by raw water pump and magnetic valve, flows through deionization apparatus and Ultrasonic Heating equipment, flowed out by rising pipe; B. controlling box electromagnetic valve for adjusting, raw water pump draws water, and controls at 0.5 ~ 10L/min by the volumetric flow rate of water in water inlet pipe; C. controlling box regulation and control deionization apparatus, the conductivity value controlling deionized water is less than 10 us/cm; D. controlling box regulation and control Ultrasonic Heating equipment, the resonant frequency controlling supersound process is 20 ~ 20000kHz, and total ultrasonic duration is 8 ~ 800min/L; E. controlling box regulation and control hot bath device, controlling Ultrasonic Heating groove temperature rise rate is 0.5 ~ 15 K/min, is down to room temperature rapidly after the 2 ~ 140min that heats up, and again with the heating of the temperature rise rate of 0.5 ~ 15 K/min, heat-processed so circulates; F. Ultrasonic Heating equipment water outlet is connected with rising pipe, and water outlet naturally cools to room temperature, the obtained small-micelle water with small molecules clustering properties.
Embodiment 1
By controlling box 12, regulation and control raw water pump 2 and magnetic valve 3, former water is passed into deionization apparatus with 1L/min, obtain the deionized water that specific conductivity is 8us/cm, then the first ultrasonic tank 7 is passed into successively, second ultrasonic tank 8, Ultrasonic Heating groove 9 and the 3rd ultrasonic tank 11, regulation and control ultrasonic tank 7, 8, in 11, direct insertion ultrasonic power instrument resonant frequency is respectively 20KHz, 30KHz, 50KHz, in Ultrasonic Heating groove 9, resonant frequency is 40 KHz, heating bath 10 heating ramp rate is 2K/min, room temperature is down to rapidly after intensification 20min, again heat with the temperature rise rate of 2 K/min, heat-processed circulates successively, water peak width at half height can be made to drop in rising pipe 13 60.54Hz when leaving standstill room temperature (290K) from the 113.69Hz water inlet pipe 1, by 17the data of O NMR gained, can draw the product of preparation, and its cluster number becomes 6 from 11, leave standstill 10 days, peak width at half height becomes 73.76Hz, by 17the data of O NMR gained, after can drawing 10 days, the cluster number of product becomes 7.
Embodiment 2
By controlling box 12, regulation and control raw water pump 2 and magnetic valve 3, former water is passed into deionization apparatus with 4L/min, obtain the deionized water that specific conductivity is 5us/cm, then the first ultrasonic tank 7 is passed into successively, second ultrasonic tank 8, Ultrasonic Heating groove 9 and the 3rd ultrasonic tank 11, regulation and control ultrasonic tank 7, 8, in 11, direct insertion ultrasonic power instrument resonant frequency is respectively 200KHz, 300KHz, 500KHz, in Ultrasonic Heating groove 9, resonant frequency is 400 KHz, heating ramp rate is 10K/min, room temperature is down to rapidly after intensification 5min, again heat with the temperature rise rate of 10K/min, heat-processed circulates successively, water peak width at half height can be made to drop to rising pipe 13 from the 113.65Hz water inlet pipe 1 and to leave standstill the 61.68Hz after room temperature (303K), by 17the data of O NMR gained, can draw the product of preparation, and its cluster number becomes 6 from 11, leave standstill 10 days, peak width at half height becomes 73.88Hz, by 17the data of O NMR gained, after can drawing 10 days, the cluster number of product becomes 7.
Embodiment 3
By controlling box 12, regulation and control raw water pump 2 and magnetic valve 3, former water is passed into deionization apparatus with 7L/min, obtain the deionized water that specific conductivity is 2us/cm, then the first ultrasonic tank 7 is passed into successively, second ultrasonic tank 8, Ultrasonic Heating groove 9 and the 3rd ultrasonic tank 11, regulation and control ultrasonic tank 7, 8, in 11, direct insertion ultrasonic power instrument resonant frequency is respectively 2000KHz, 3000KHz, 5000KHz, in Ultrasonic Heating groove 9, resonant frequency is 4000 KHz, heating ramp rate is 15K/min, room temperature is down to rapidly after intensification 3min, again heat with the temperature rise rate of 15K/min, heat-processed circulates successively, water peak width at half height can be made to drop to rising pipe 13 from the 113.54Hz water inlet pipe 1 and to leave standstill the 60.67Hz after room temperature (303K), by 17the data of O NMR gained, can draw the product of preparation, and its cluster number becomes 6 from 11, leave standstill 10 days, peak width at half height becomes 72.12Hz, by 17the data of O NMR gained, after can drawing 10 days, the cluster number of product becomes 7.
Embodiment 4
By controlling box 12, regulation and control raw water pump 2 and magnetic valve 3, former water is passed into deionization apparatus with 2L/min, obtain the deionized water that specific conductivity is 2us/cm, then the first ultrasonic tank 7 is passed into successively, second ultrasonic tank 8, Ultrasonic Heating groove 9 and the 3rd ultrasonic tank 11, regulation and control ultrasonic tank 7, 8, in 11, direct insertion ultrasonic power instrument resonant frequency is respectively 1000KHz, 2000KHz, 4000KHz, in Ultrasonic Heating groove 9, resonant frequency is 3000 KHz, heating ramp rate is 6K/min, room temperature is down to rapidly after intensification 10min, again heat with the temperature rise rate of 6 K/min, heat-processed circulates successively, water peak width at half height can be made to drop to rising pipe 13 from the 113.54Hz of water inlet pipe 1 and to leave standstill the 61.13Hz after room temperature (303K), by 17the data of O NMR gained, can draw the product of preparation, and its cluster number becomes 6 from 11, leave standstill 10 days, peak width at half height becomes 73.33Hz, by 17the data of O NMR gained, after can drawing 10 days, the cluster number of product becomes 7, leave standstill 60 days, peak width at half height becomes 73.53Hz, by 17the data of O NMR gained, after can drawing 60 days, the cluster number of product is still 7, leave standstill 300 days, peak width at half height becomes 73.55Hz, by 17the data of O NMR gained, after can drawing 300 days, the cluster number of product is still 7.
Embodiment 5
By controlling box 12, regulation and control raw water pump 2 and magnetic valve 3, former water is passed into deionization apparatus with 3L/min, obtain the deionized water that specific conductivity is 5us/cm, then the first ultrasonic tank 7 is passed into successively, second ultrasonic tank 8, Ultrasonic Heating groove 9 and the 3rd ultrasonic tank 11, regulation and control ultrasonic tank 7, 8, in 11, direct insertion ultrasonic power instrument resonant frequency is respectively 500KHz, 600KHz, 800KHz, in Ultrasonic Heating groove 9, resonant frequency is 700 KHz, heating ramp rate is 7K/min, room temperature is down to rapidly after intensification 7min, again heat with the temperature rise rate of 7 K/min, heat-processed circulates successively, water peak width at half height can be made to drop to rising pipe 13 from the 113.66Hz of water inlet pipe 1 and to leave standstill the 62.16Hz after room temperature (303K), by 17the data of O NMR gained, can draw the product of preparation, and its cluster number becomes 6 from 11, leave standstill 10 days, peak width at half height becomes 73.56Hz, by 17the data of O NMR gained, after can drawing 10 days, the cluster number of product becomes 7, leave standstill 60 days, peak width at half height becomes 73.58Hz, by 17the data of O NMR gained, after can drawing 60 days, the cluster number of product is still 7, leave standstill 300 days, peak width at half height becomes 73.59Hz, by 17the data of O NMR gained, after can drawing 300 days, the cluster number of product is still 7.
Above-described embodiment of the present utility model is only for the utility model example is clearly described, and is not the restriction to embodiment of the present utility model.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here exhaustive without the need to also giving all embodiments.All do within spirit of the present utility model and principle any amendment, equivalent to replace and improvement etc., within the protection domain that all should be included in the utility model claim.

Claims (3)

1. utilize Ultrasonic Heating technology to prepare a device for stable micro-molecular group water, it is characterized in that, described device comprises water inlet pipe (1), raw water pump (2), deionization apparatus, Ultrasonic Heating equipment and rising pipe (13); Described water inlet pipe (1) is connected in turn with raw water pump (2), deionization apparatus, Ultrasonic Heating equipment, rising pipe (13); Described deionization apparatus is made up of activated charcoal filter (4), reverse osmosis membrane assembly (5) and mixed bed (6), and described activated charcoal filter (4) is connected in turn with reverse osmosis membrane assembly (5), mixed bed (6); Described Ultrasonic Heating equipment is made up of the first ultrasonic tank (7), the second ultrasonic tank (8), Ultrasonic Heating groove (9), hot bath device (10) and the 3rd ultrasonic tank (11), wherein the first ultrasonic tank (7) is connected in turn with the second ultrasonic tank (8), Ultrasonic Heating groove (9) and the 3rd ultrasonic tank (11), and hot bath device (10) is connected with Ultrasonic Heating groove (9).
2. the device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water according to claim 1, it is characterized in that, described device also comprises magnetic valve (3) and controlling box (12); Described magnetic valve (3) is connected between raw water pump (2) and deionization apparatus; Described controlling box (12) is connected with raw water pump (2), magnetic valve (3), activated charcoal filter (4), reverse osmosis membrane assembly (5), mixed bed (6), the first ultrasonic tank (7), the second ultrasonic tank (8), Ultrasonic Heating groove (9), hot bath device (10), the 3rd ultrasonic tank (11) respectively by signal wire; Described controlling box (12), by regulation and control raw water pump (2), magnetic valve (3), controls raw water flow; Described controlling box (12), by activated charcoal filter (4), reverse osmosis membrane assembly (5), mixed bed (6) in regulation and control deionization apparatus, controls the conductivity value of deionized water; Described controlling box (12) is by regulating and controlling the ultrasound resonance frequency of the first ultrasonic tank (7), the second ultrasonic tank (8), Ultrasonic Heating groove (9), the 3rd ultrasonic tank (11) in Ultrasonic Heating equipment and ultrasonic duration, the heating ramp rate of regulation and control hot bath device (10), controls Ultrasonic Heating process.
3. according to a kind of device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water shown in claim 1, it is characterized in that, described the first ultrasonic tank (7), the second ultrasonic tank (8), Ultrasonic Heating groove (9), the 3rd ultrasonic tank (11) volume are 5 ~ 100L.
CN201420781302.2U 2014-12-12 2014-12-12 A kind of device utilizing Ultrasonic Heating technology to prepare stable micro-molecular group water Active CN204369708U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104556517A (en) * 2014-12-12 2015-04-29 华南理工大学 Device and method for preparing stable microcluster water by use of ultrasonic heating technology

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104556517A (en) * 2014-12-12 2015-04-29 华南理工大学 Device and method for preparing stable microcluster water by use of ultrasonic heating technology

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