CN204251357U - With the titanium tetrachloride mud treatment device of pressure tester - Google Patents
With the titanium tetrachloride mud treatment device of pressure tester Download PDFInfo
- Publication number
- CN204251357U CN204251357U CN201420668500.8U CN201420668500U CN204251357U CN 204251357 U CN204251357 U CN 204251357U CN 201420668500 U CN201420668500 U CN 201420668500U CN 204251357 U CN204251357 U CN 204251357U
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- Prior art keywords
- evaporation process
- process tank
- titanium tetrachloride
- gas
- pressure tester
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Abstract
The utility model discloses a kind of titanium tetrachloride mud treatment device with pressure tester, pipeline is established to extend in evaporation process tank bottom the thickener of chlorination system, dry slag collection bucket is provided with below evaporation process tank, evaporation process tank, gas-solid separating device, titanium tetrachloride eluting column is connected by the pipeline being provided with lagging material successively, be provided with pipeline bottom gas-solid separating device to be connected with dry slag collection bucket, agitator is provided with in evaporation process tank, agitator passes through axle, transmission mechanism is connected with the motor of evaporation process tank top, axle is being provided with dynamic seal ring through evaporation process tank place, main heating unit is provided with outside evaporation process tank, this device achieves the closed processes of titanium tetrachloride mud, the recovery utilization rate of valence component titanium tetrachloride is had to reach more than 95% in mud, the solid chloride dry powder residue dirt separated can carry out focusing on or being recycled, secondary pollution can not be caused to environment, this device does not affect the normal production of chlorination system.
Description
Technical field
The utility model belongs to titanium tetrachloride production technical field, and particularly fluidizing chlorination method produces the treatment unit producing mud in titanium tetrachloride process.
Background technology
Titanium tetrachloride is a kind of heavy chemical industry, metallurgic product, produce titanium dioxide, the main raw material of titanium sponge, at present, the production of titanium tetrachloride adopts fluidizing chlorination method to produce more, namely chlorine is adopted, rich titanium material, refinery coke carries out being obtained by reacting titanium tetrachloride gases in chlorination furnace, titanium tetrachloride gases is through drip washing, sedimentation, titanium tetrachloride liquid is obtained after filtration, a large amount of mud can be produced bottom the thickener of chlorination system in process of production, this mud is mainly the mixture of titanium tetrachloride and muriate dust, now conventional treatment process has airtight flushing or mud is melted down use, in flushing treating processes, not only cannot reclaim titanium tetrachloride in mud have valence component, and consume a large amount of clear water when rinsing, produce a large amount of acid gas, sour water, certain pollution is caused to environment, pollution plot costly, although mud melts down to use can reclaim valuable constituent in mud, easily affect the working of a furnace of boiling chloridizing furnace, cause the exception of chlorination reaction.
In recent years, the research how processed this mud is more, as 103121710A patent discloses Mud reclamation device in titanium tetrachloride production, comprise fluidizing furnace, dust-precipitator, described fluidizing furnace, a herring-bone mixing tube is provided with between dust-precipitator, herring-bone mixing tube one end is connected with fluidizing furnace air outlet, herring-bone mixing tube the other end is connected with dust-precipitator inlet mouth, herring-bone mixing tube round part is provided with mud admission port relative to the position of fluidizing furnace air outlet, mud admission port is connected with mud diffuser tube, mud diffuser tube and mud enter pipe and are connected, mud enters pipe and is connected with cooling threeway one end, the cooling threeway the other end is connected with the reverse jet pipe of mud, cooling threeway the 3rd end is connected with nitrogen tube, although this patent achieves mud melt down utilization, but solid chloride dust in mud is not separated by real realization from chlorination system, and this mode easily affects the rate of recovery of titanium tetrachloride in chlorination system.
Summary of the invention
The purpose of this utility model is to solve problems of the prior art, provide a kind of titanium tetrachloride mud treatment device with pressure tester, utilize this device can carry out the closed processes of titanium tetrachloride mud, in recycling mud, titanium tetrachloride has valence component, be separated the solid chloride dust in mud, do not affect the normal production of chlorination system, do not produce secondary pollution.
The technical solution of the utility model is:
A kind of titanium tetrachloride mud treatment device with pressure tester, primarily of evaporation process tank, gas-solid separating device, dry slag collection bucket composition, pipeline is established to extend in evaporation process tank bottom the thickener of chlorination system, dry slag collection bucket is provided with below evaporation process tank, evaporation process tank, gas-solid separating device, titanium tetrachloride eluting column is connected by the pipeline being provided with lagging material successively, be provided with pipeline bottom gas-solid separating device to be connected with dry slag collection bucket, agitator is provided with in evaporation process tank, agitator passes through axle, transmission mechanism is connected with the motor of evaporation process tank top, axle is being provided with dynamic seal ring through evaporation process tank place, main heating unit is provided with outside evaporation process tank.Particularly,
Gas percussion baffle plate, bagroom, eddy flow dust-precipitator is provided with from bottom to up successively in described gas-solid separating device; Eddy flow dust-precipitator is at least secondary;
The bottom of described gas-solid separating device is provided with assisted heating device, and the heating unit of assisted heating device, main heating unit is resistance wire, heating unit peripheral hardware heat-resistant insulation material;
The pipeline of described evaporation process tank, gas-solid separating device and dry slag collection bucket is provided with valve, and valve is magnetic valve;
Be provided with temperature measurer in described evaporation process tank, gas-solid separating device, temperature measurer is thermopair, and thermopair is connected with Controlling System by signal wire;
Be provided with pressure tester in described evaporation process tank, evaporation process tank top is provided with pressure relief opening and utilizes pipeline to be connected with titanium tetrachloride eluting column;
The body skin of described evaporation process tank, gas-solid separating device is provided with preservative coat;
Described titanium tetrachloride eluting column is the eluting column of chlorination system.
In the utility model: the titanium tetrachloride mud that chlorination system thickener bottom is precipitated is joined in evaporation process tank by pipeline, main heating unit is utilized to make temperature in evaporation process tank keep more than titanium tetrachloride boiling point, and by agitator, mud is stirred, the titanium tetrachloride liquid in mud is made to be evaporated to titanium tetrachloride gases, and through gas-solid separating device by after small solid dust separation, titanium tetrachloride gases is transported to drip washing recovery in the eluting column of chlorination system and obtains titanium tetrachloride, dry powder residue dirt after treatment send slag field to process or recycles after utilizing dry slag collection bucket to collect.
The beneficial effects of the utility model and advantage are:
This device achieves the closed processes of titanium tetrachloride mud, the recovery utilization rate of valence component titanium tetrachloride is had to reach more than 95% in mud, the solid chloride dry powder residue dirt separated can carry out focusing on or being recycled, can not cause secondary pollution to environment, this device does not affect the normal production of chlorination system.
Accompanying drawing explanation
Fig. 1 is the titanium tetrachloride mud treatment device structural representation with pressure tester of the present utility model;
In figure: 1-evaporation process tank, 2-thickener, 3-dynamic seal ring, 4-motor, 5-pressure relief opening, 6-agitator, 7-gas-solid separating device, 8-eddy flow dust-precipitator, 9-lagging material, 10-titanium tetrachloride eluting column, 11-bagroom, 12-assisted heating device, 13-heating unit, 14-gas percussion baffle plate, 15-valve, 16-dry slag collection bucket, the main heating unit of 17-.
Embodiment
Below in conjunction with accompanying drawing, the utility model is described in further detail, but should not be interpreted as that the scope of theme described in the utility model is only limitted to following embodiment at this point, do not departing from the above-mentioned technological thought situation of the utility model, all make according to ordinary skill knowledge and customary means various amendments, replacement and change, include in scope of the present utility model.
As shown in Figure 1, a kind of titanium tetrachloride mud treatment device with pressure tester, primarily of evaporation process tank 1, gas-solid separating device 7, dry slag collection bucket 16 forms, pipeline is established to extend in evaporation process tank 1 bottom the thickener 2 of chlorination system, dry slag collection bucket 16 is provided with below evaporation process tank 1, evaporation process tank 1, gas-solid separating device 7, titanium tetrachloride eluting column 10 is connected by the pipeline being provided with lagging material 9 successively, be provided with pipeline bottom gas-solid separating device 7 to be connected with dry slag collection bucket 16, agitator 6 is provided with in evaporation process tank 1, agitator 6 passes through axle, transmission mechanism is connected with the motor 4 at evaporation process tank 1 top, axle is being provided with dynamic seal ring 3 through evaporation process tank 1 place, main heating unit 17 is provided with outside evaporation process tank 1.
Further, be provided with gas percussion baffle plate 14, bagroom 11, eddy flow dust-precipitator 8 from bottom to up successively in described gas-solid separating device 7, eddy flow dust-precipitator 8 is at least secondary.
The bottom of described gas-solid separating device 7 is provided with assisted heating device 12, and the heating unit 13 of assisted heating device 12, main heating unit 17 is resistance wire, heating unit 13 peripheral hardware heat-resistant insulation material.
Described evaporation process tank 1, gas-solid separating device 7 are provided with valve 15 with the pipeline of dry slag collection bucket 16, and valve 15 is magnetic valve.
Be provided with temperature measurer in described evaporation process tank 1, gas-solid separating device 7, temperature measurer is thermopair, and thermopair is connected with Controlling System by signal wire.
Be provided with pressure tester in described evaporation process tank 1, evaporation process tank 1 top is provided with pressure relief opening 5 and utilizes pipeline to be connected with titanium tetrachloride eluting column 10.
The body skin of described evaporation process tank 1, gas-solid separating device 7 is provided with preservative coat.
Described titanium tetrachloride eluting column 10 is the eluting column of chlorination system.
The above is only a preferred embodiment of the present utility model, therefore all equivalences done according to structure, feature and the principle described in the utility model patent claim change or modify, and are included in the protection domain of the utility model patent application.
Claims (7)
1. the titanium tetrachloride mud treatment device with pressure tester, primarily of evaporation process tank (1), gas-solid separating device (7), dry slag collection bucket (16) composition, it is characterized in that thickener (2) bottom of chlorination system establishes pipeline to extend in evaporation process tank (1), evaporation process tank (1) below is provided with dry slag collection bucket (16), evaporation process tank (1), gas-solid separating device (7), titanium tetrachloride eluting column (10) is connected by the pipeline being provided with lagging material (9) successively, gas-solid separating device (7) bottom is provided with pipeline and is connected with dry slag collection bucket (16), agitator (6) is provided with in evaporation process tank (1), agitator (6) passes through axle, transmission mechanism is connected with the motor (4) at evaporation process tank (1) top, axle is being provided with dynamic seal ring (3) through evaporation process tank (1) place, main heating unit (17) is provided with outside evaporation process tank (1),
Be provided with pressure tester in described evaporation process tank (1), evaporation process tank (1) top is provided with pressure relief opening (5) and utilizes pipeline to be connected with titanium tetrachloride eluting column (10).
2. the titanium tetrachloride mud treatment device with pressure tester according to claim 1, is characterized in that being provided with gas percussion baffle plate (14), bagroom (11), eddy flow dust-precipitator (8) in described gas-solid separating device (7) from bottom to up successively.
3. the titanium tetrachloride mud treatment device with pressure tester according to claim 2, is characterized in that described eddy flow dust-precipitator (8) is at least secondary.
4. any one titanium tetrachloride mud treatment device with pressure tester according to claims 1 to 3, is characterized in that the bottom of described gas-solid separating device (7) is provided with assisted heating device (12),
The heating unit (13) of assisted heating device (12), main heating unit (17) is resistance wire, heating unit (13) peripheral hardware heat-resistant insulation material.
5. the titanium tetrachloride mud treatment device with pressure tester according to claim 1, is characterized in that described evaporation process tank (1), gas-solid separating device is provided with temperature measurer in (7).
6. the titanium tetrachloride mud treatment device with pressure tester according to claim 5, it is characterized in that described temperature measurer is thermopair, thermopair is connected with Controlling System by signal wire.
7. the titanium tetrachloride mud treatment device with pressure tester according to claim 1, is characterized in that the eluting column that described titanium tetrachloride eluting column (10) is chlorination system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420668500.8U CN204251357U (en) | 2014-11-11 | 2014-11-11 | With the titanium tetrachloride mud treatment device of pressure tester |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420668500.8U CN204251357U (en) | 2014-11-11 | 2014-11-11 | With the titanium tetrachloride mud treatment device of pressure tester |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204251357U true CN204251357U (en) | 2015-04-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420668500.8U Expired - Fee Related CN204251357U (en) | 2014-11-11 | 2014-11-11 | With the titanium tetrachloride mud treatment device of pressure tester |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204251357U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110330051A (en) * | 2019-08-15 | 2019-10-15 | 马汝普 | Waste residue recycle device in a kind of titanic chloride production process |
| CN114053739A (en) * | 2021-11-30 | 2022-02-18 | 攀钢集团钒钛资源股份有限公司 | Evaporation and deslagging device and method for refined vanadium-removing slurry |
-
2014
- 2014-11-11 CN CN201420668500.8U patent/CN204251357U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110330051A (en) * | 2019-08-15 | 2019-10-15 | 马汝普 | Waste residue recycle device in a kind of titanic chloride production process |
| CN114053739A (en) * | 2021-11-30 | 2022-02-18 | 攀钢集团钒钛资源股份有限公司 | Evaporation and deslagging device and method for refined vanadium-removing slurry |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Shao Jianxin Inventor after: Chai Lijun Inventor after: Chen Jianlin Inventor after: Xue Wenlong Inventor after: Zhou Haiyan Inventor before: Liu Chao |
|
| CB03 | Change of inventor or designer information | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170419 Address after: 314000 Zhejiang City, Jiaxing Province, the new meteorological Road, building 1080, No. four Patentee after: Jiaxing Ruixin Construction Engineering Co., Ltd. Address before: 518000 Guangdong city of Shenzhen province Futian District Fuhua Road No. 6 Building 1403 business tax Patentee before: Liu Chao |
|
| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150408 Termination date: 20171111 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |