CN204220138U - Stirred reactor - Google Patents
Stirred reactor Download PDFInfo
- Publication number
- CN204220138U CN204220138U CN201420593051.5U CN201420593051U CN204220138U CN 204220138 U CN204220138 U CN 204220138U CN 201420593051 U CN201420593051 U CN 201420593051U CN 204220138 U CN204220138 U CN 204220138U
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- CN
- China
- Prior art keywords
- sealing
- reactor
- chuck
- pond
- lid
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The open stirred reactor of the utility model, reactor monolith is arranged in chuck inner space, in the bottom of chuck and top, water inlet and delivery port are set, at the two ends of reactor, air inlet and gas outlet are set respectively, the sealing pond be connected with reactor opening is set between reactor open upper end and chuck, diaphragm seal is set in the bottom in sealing pond, the second sealing thread is set on the top in sealing pond; The described lid that tightens is arranged in sealing pond, described in tighten lid and matched with second sealing thread in sealing pond by the first sealing thread being arranged on its surface, to cover and the central authorities of diaphragm seal arrange installation passage tightening.The technical solution of the utility model utilization tightens lid and diaphragm seal seals, and Inlet and outlet water can be utilized to carry out temperature control, effectively prevents the volatilization of solvent, reaches good reaction effect.
Description
Technical field
The utility model belongs to chemical experiment field, more particularly, relates to a kind of stirred reactor.
Background technology
Often need stirred reactor in chemical experiment field, in course of reaction, namely utilize agitating device realization to the homogenising of reaction system and stabilisation.Agitating mode is often divided into two kinds, and one is mechanical agitation, adopts paddle and stirring sleeve to carry out sealing and fixing, and utilizes the stirring that motor Stirring oar realizes reaction system; Another kind is magnetic agitation, adopts additional field of magnetic forece to make the rotor in reaction system realize motion, to carry out homogenising and stabilisation to reaction system.In mechanical agitation, there are two kinds of forms in stirring sleeve: the sleeve pipe of glass material and the sleeve pipe of polytetrafluoroethylene (PTFE), these two kinds of stirring sleeves do not allow volatile chemical reaction more applicable for low temperature, solvent, because often there is gap between stirring sleeve and paddle, sealing effectiveness is bad, inapplicable for high temperature, back flow reaction and the reaction containing easy volatile solvent, the volatilization of partial solvent in course of reaction can be caused, thus affect reaction effect.
Utility model content
The purpose of this utility model is to overcome churned mechanically deficiency in prior art, provides a kind of stirred reactor, and enhanced leaktightness effect avoids the volatilization of reaction dissolvent in experimentation, makes reaction reach optimum efficiency.
Technical purpose of the present utility model is achieved by following technical proposals:
Stirred reactor, by chuck, reactor, tighten lid and mechanical stirring device form, wherein:
Described reactor monolith is arranged in chuck inner space, in the bottom of described chuck, water inlet is set, described water inlet and inlet channel are fixedly linked, the mouth of a river is set out at the top of described chuck, described delivery port and outlet conduit are fixedly linked, the two ends of described reactor arrange air inlet and gas outlet respectively, chuck is stretched out in described air inlet and gas outlet, and seal with chuck wall, described air inlet and admission line seal and are fixedly linked, described gas outlet and outlet pipe seal and are fixedly linked, set temperature harvester in described chuck, described temperature collecting device is connected with temperature control equipment, described temperature control equipment is connected with inlet channel, the flow of water inlet is controlled by the opening degree of pipe valve, so, whole reactor is all positioned within the space of chuck, and Inlet and outlet water can provide temperature to keep for reactor and regulate.
The sealing pond be connected with reactor opening is set between reactor open upper end and chuck, diaphragm seal is set in the bottom in sealing pond, the second sealing thread is set on the top in sealing pond; The described lid that tightens is arranged in sealing pond, described in tighten lid and matched with second sealing thread in sealing pond, to realize being tightly connected and fixing seal sheet by the first sealing thread being arranged on its surface; Installation passage is set in the described central authorities tightening lid and diaphragm seal, for the paddle of mechanical stirring device is incorporated in reactor, stirs to realize sealing.
Described mechanical stirring device is made up of the paddle being arranged on the stirring motor on top, the attaching parts be connected with stirring motor and being arranged on bottom, described paddle and attaching parts are through being arranged on the installation passage tightening lid and diaphragm seal central authorities, extend in reactor, the described size of installation passage is consistent with the radial dimension of the attaching parts of mechanical stirring device.
In technique scheme, described reactor bottom is spherical bottom, and top is cylinder, and material is glass.
In technique scheme, described chuck material is glass, thickness 10-15mm.
In technique scheme, the material in described sealing pond is glass, and the second sealing thread arranged on the top in sealing pond is internal thread.
In technique scheme, described in tighten lid material be polytetrafluoroethylene (PTFE), be external screw thread tightening the first sealing thread that cap surface arranges.
In technique scheme, described diaphragm seal and sealing pond fixed seal connection, material is lucite or rubber.
When using, utilization tightens lid and diaphragm seal seals, and Inlet and outlet water can be utilized to carry out temperature control, effectively prevents the volatilization of solvent, reaches good reaction effect.
Accompanying drawing explanation
Fig. 1 is the structural representation (1) of the utility model stirred reactor, and wherein 1 is chuck, and 1-1 is temperature control equipment, 1-2 is temperature collecting device, 2 is reactor, and 3-1 is air inlet, and 3-3 is admission line, 3-2 is gas outlet, 3-4 is outlet pipe, and 4 is water inlet, and 5 is delivery port, 6 for tightening lid, 7 is diaphragm seal, and 8 is sealing pond, and 9 is the first sealing thread, 10 for installing passage, 11 is the second sealing thread, and 12 is mechanical stirring device, and 12-1 is stirring motor, 12-2 is paddle, and 12-3 is attaching parts.
Fig. 2 is the structural representation (2) of the utility model stirred reactor, and wherein 1 is chuck, and 3-1 is air inlet, and 3-2 is gas outlet, 4 is water inlet, and 4-1 is inlet channel, and 5 is delivery port, 5-1 is outlet conduit, and 6 for tightening lid, and 10 for installing passage.
Detailed description of the invention
The technical solution of the utility model is further illustrated below in conjunction with specific embodiment.
As shown in accompanying drawing 1-2, the utility model stirred reactor, wherein 1 is chuck, 1-1 is temperature control equipment, 1-2 is temperature collecting device, 2 is reactor, 3-1 is air inlet, 3-3 is admission line, 3-2 is gas outlet, 3-4 is outlet pipe, 4 is water inlet, 4-1 is inlet channel, 5 is delivery port, 5-1 is outlet conduit, 6 for tightening lid, 7 is diaphragm seal, 8 is sealing pond, 9 is the first sealing thread, 10 for installing passage, 11 is the second sealing thread, 12 is mechanical stirring device, 12-1 is stirring motor, 12-2 is paddle, 12-3 is attaching parts.
Stirred reactor, by chuck, reactor, tighten lid and mechanical stirring device form, wherein:
Described reactor monolith is arranged in chuck inner space, in the bottom of described chuck, water inlet is set, described water inlet and inlet channel are fixedly linked, the mouth of a river is set out at the top of described chuck, described delivery port and outlet conduit are fixedly linked, the two ends of described reactor arrange air inlet and gas outlet respectively, chuck is stretched out in described air inlet and gas outlet, and seal with chuck wall, described air inlet and admission line seal and are fixedly linked, described gas outlet and outlet pipe seal and are fixedly linked, set temperature harvester in described chuck, described temperature collecting device is connected with temperature control equipment, described temperature control equipment is connected with inlet channel, the flow of water inlet is controlled by the opening degree of pipe valve, so, whole reactor is all positioned within the space of chuck, and Inlet and outlet water can provide temperature to keep for reactor and regulate.
The sealing pond be connected with reactor opening is set between reactor open upper end and chuck, diaphragm seal is set in the bottom in sealing pond, the second sealing thread is set on the top in sealing pond; The described lid that tightens is arranged in sealing pond, described in tighten lid and matched with second sealing thread in sealing pond, to realize being tightly connected and fixing seal sheet by the first sealing thread being arranged on its surface; Installation passage is set in the described central authorities tightening lid and diaphragm seal, for the paddle of mechanical stirring device is incorporated in reactor, stirs to realize sealing.
Described mechanical stirring device is made up of the paddle being arranged on the stirring motor on top, the attaching parts be connected with stirring motor and being arranged on bottom, described paddle and attaching parts are through being arranged on the installation passage tightening lid and diaphragm seal central authorities, extend in reactor, the described size of installation passage is consistent with the radial dimension of the attaching parts of mechanical stirring device.
In technique scheme, described reactor bottom is spherical bottom, and top is cylinder, and material is glass.
In technique scheme, described chuck material is glass, thickness 10-15mm.
In technique scheme, the material in described sealing pond is glass, and the second sealing thread arranged on the top in sealing pond is internal thread.
In technique scheme, described in tighten lid material be polytetrafluoroethylene (PTFE), be external screw thread tightening the first sealing thread that cap surface arranges.
In technique scheme, described diaphragm seal and sealing pond fixed seal connection, material is lucite or rubber.
When using, utilization tightens lid and diaphragm seal seals, and Inlet and outlet water can be utilized to carry out temperature control, effectively prevents the volatilization of solvent, reaches good reaction effect.
Above exemplary description is done to the utility model; should be noted that; when not departing from core of the present utility model, any simple distortion, amendment or other those skilled in the art can not spend the equivalent replacement of creative work all to fall into protection domain of the present utility model.
Claims (5)
1. stirred reactor, is characterized in that, by chuck, reactor, tighten lid and mechanical stirring device form, wherein:
Described reactor monolith is arranged in chuck inner space, in the bottom of described chuck, water inlet is set, described water inlet and inlet channel are fixedly linked, the mouth of a river is set out at the top of described chuck, described delivery port and outlet conduit are fixedly linked, the two ends of described reactor arrange air inlet and gas outlet respectively, chuck is stretched out in described air inlet and gas outlet, and seal with chuck wall, described air inlet and admission line seal and are fixedly linked, described gas outlet and outlet pipe seal and are fixedly linked, set temperature harvester in described chuck, described temperature collecting device is connected with temperature control equipment, described temperature control equipment is connected with inlet channel,
The sealing pond be connected with reactor opening is set between reactor open upper end and chuck, diaphragm seal is set in the bottom in sealing pond, the second sealing thread is set on the top in sealing pond; The described lid that tightens is arranged in sealing pond, described in tighten lid and matched with second sealing thread in sealing pond, to realize being tightly connected and fixing seal sheet by the first sealing thread being arranged on its surface; In the described central authorities tightening lid and diaphragm seal, installation passage is set;
Described mechanical stirring device is made up of the paddle being arranged on the stirring motor on top, the attaching parts be connected with stirring motor and being arranged on bottom, described paddle and attaching parts are through being arranged on the installation passage tightening lid and diaphragm seal central authorities, extend in reactor, the described size of installation passage is consistent with the radial dimension of the attaching parts of mechanical stirring device.
2. stirred reactor according to claim 1, is characterized in that, described reactor bottom is spherical bottom, and top is cylinder, and material is glass.
3. stirred reactor according to claim 1, is characterized in that, described chuck material is glass, thickness 10-15mm.
4. stirred reactor according to claim 1, is characterized in that, the material in described sealing pond is glass, and the second sealing thread arranged on the top in sealing pond is internal thread; The described material tightening lid is polytetrafluoroethylene (PTFE), tighten cap surface arrange the first sealing thread be external screw thread.
5. stirred reactor according to claim 1, is characterized in that, described diaphragm seal and sealing pond fixed seal connection, material is lucite or rubber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420593051.5U CN204220138U (en) | 2014-10-14 | 2014-10-14 | Stirred reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420593051.5U CN204220138U (en) | 2014-10-14 | 2014-10-14 | Stirred reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204220138U true CN204220138U (en) | 2015-03-25 |
Family
ID=52918284
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420593051.5U Expired - Fee Related CN204220138U (en) | 2014-10-14 | 2014-10-14 | Stirred reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204220138U (en) |
-
2014
- 2014-10-14 CN CN201420593051.5U patent/CN204220138U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150325 Termination date: 20161014 |